CS258112B2 - Method of vanilin-positive ionoforming substance quantity determination - Google Patents

Method of vanilin-positive ionoforming substance quantity determination Download PDF

Info

Publication number: CS258112B2
Authority: CS; Czechoslovakia
Prior art keywords: vanillin; feed; acid; positive; solution
Prior art date: 1982-05-26

Application number

CS833610A

Other languages

Czech (cs)

English (en)

Other versions

CS361083A2 (en

Inventor

Gunter H W Marten

Original Assignee

Lilly Industries Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-05-26

Filing date

1983-05-20

Publication date

1988-07-15

1983-05-20 Application filed by Lilly Industries Ltd filed Critical Lilly Industries Ltd

1987-12-17 Publication of CS361083A2 publication Critical patent/CS361083A2/cs

1988-07-15 Publication of CS258112B2 publication Critical patent/CS258112B2/cs

Links

MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims description 25
FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 claims description 25
235000012141 vanillin Nutrition 0.000 claims description 25
238000000034 method Methods 0.000 claims description 15
230000000236 ionophoric effect Effects 0.000 claims description 14
239000002904 solvent Substances 0.000 claims description 12
239000002555 ionophore Substances 0.000 claims description 11
YCPXWRQRBFJBPZ-UHFFFAOYSA-N 5-sulfosalicylic acid Chemical compound OC(=O)C1=CC(S(O)(=O)=O)=CC=C1O YCPXWRQRBFJBPZ-UHFFFAOYSA-N 0.000 claims description 7
229930191564 Monensin Natural products 0.000 claims description 7
GAOZTHIDHYLHMS-UHFFFAOYSA-N Monensin A Natural products O1C(CC)(C2C(CC(O2)C2C(CC(C)C(O)(CO)O2)C)C)CCC1C(O1)(C)CCC21CC(O)C(C)C(C(C)C(OC)C(C)C(O)=O)O2 GAOZTHIDHYLHMS-UHFFFAOYSA-N 0.000 claims description 7
230000001476 alcoholic effect Effects 0.000 claims description 7
229960005358 monensin Drugs 0.000 claims description 7
GAOZTHIDHYLHMS-KEOBGNEYSA-N monensin A Chemical compound C([C@@](O1)(C)[C@H]2CC[C@@](O2)(CC)[C@H]2[C@H](C[C@@H](O2)[C@@H]2[C@H](C[C@@H](C)[C@](O)(CO)O2)C)C)C[C@@]21C[C@H](O)[C@@H](C)[C@@H]([C@@H](C)[C@@H](OC)[C@H](C)C(O)=O)O2 GAOZTHIDHYLHMS-KEOBGNEYSA-N 0.000 claims description 7
238000002156 mixing Methods 0.000 claims description 6
239000002253 acid Substances 0.000 description 17
239000000243 solution Substances 0.000 description 14
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
239000000126 substance Substances 0.000 description 7
239000006228 supernatant Substances 0.000 description 7
239000000203 mixture Substances 0.000 description 6
239000007787 solid Substances 0.000 description 6
150000001299 aldehydes Chemical class 0.000 description 4
239000007788 liquid Substances 0.000 description 4
HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
241001465754 Metazoa Species 0.000 description 3
239000003674 animal food additive Substances 0.000 description 3
239000000463 material Substances 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
LWRSYTXEQUUTKW-UHFFFAOYSA-N 2,4-dimethoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C(OC)=C1 LWRSYTXEQUUTKW-UHFFFAOYSA-N 0.000 description 2
229910002012 Aerosil® Inorganic materials 0.000 description 2
241000283690 Bos taurus Species 0.000 description 2
VHKXXVVRRDYCIK-CWCPJSEDSA-N Narasin Chemical compound C[C@H]1C[C@H](C)[C@H]([C@@H](CC)C(O)=O)O[C@H]1[C@@H](C)[C@H](O)[C@H](C)C(=O)[C@H](CC)[C@@H]1[C@@H](C)C[C@@H](C)[C@@]2(C=C[C@@H](O)[C@@]3(O[C@@](C)(CC3)[C@@H]3O[C@@H](C)[C@@](O)(CC)CC3)O2)O1 VHKXXVVRRDYCIK-CWCPJSEDSA-N 0.000 description 2
VHKXXVVRRDYCIK-UHFFFAOYSA-N Narasin Natural products CC1CC(C)C(C(CC)C(O)=O)OC1C(C)C(O)C(C)C(=O)C(CC)C1C(C)CC(C)C2(C=CC(O)C3(OC(C)(CC3)C3OC(C)C(O)(CC)CC3)O2)O1 VHKXXVVRRDYCIK-UHFFFAOYSA-N 0.000 description 2
KQXDHUJYNAXLNZ-XQSDOZFQSA-N Salinomycin Chemical compound O1[C@@H]([C@@H](CC)C(O)=O)CC[C@H](C)[C@@H]1[C@@H](C)[C@H](O)[C@H](C)C(=O)[C@H](CC)[C@@H]1[C@@H](C)C[C@@H](C)[C@@]2(C=C[C@@H](O)[C@@]3(O[C@@](C)(CC3)[C@@H]3O[C@@H](C)[C@@](O)(CC)CC3)O2)O1 KQXDHUJYNAXLNZ-XQSDOZFQSA-N 0.000 description 2
239000004189 Salinomycin Substances 0.000 description 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
238000003556 assay Methods 0.000 description 2
238000004040 coloring Methods 0.000 description 2
CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 description 2
238000000605 extraction Methods 0.000 description 2
235000019359 magnesium stearate Nutrition 0.000 description 2
229960001851 narasin Drugs 0.000 description 2
229960001548 salinomycin Drugs 0.000 description 2
235000019378 salinomycin Nutrition 0.000 description 2
239000011973 solid acid Substances 0.000 description 2
JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 2
WJUFSDZVCOTFON-UHFFFAOYSA-N veratraldehyde Chemical compound COC1=CC=C(C=O)C=C1OC WJUFSDZVCOTFON-UHFFFAOYSA-N 0.000 description 2
KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 description 1
IAJBQAYHSQIQRE-UHFFFAOYSA-N 2,4,5-trimethoxybenzaldehyde Chemical compound COC1=CC(OC)=C(C=O)C=C1OC IAJBQAYHSQIQRE-UHFFFAOYSA-N 0.000 description 1
-1 5-sulfosalicyl Chemical group 0.000 description 1
AXMVYSVVTMKQSL-UHFFFAOYSA-N UNPD142122 Natural products OC1=CC=C(C=CC=O)C=C1O AXMVYSVVTMKQSL-UHFFFAOYSA-N 0.000 description 1
239000003377 acid catalyst Substances 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
230000002411 adverse Effects 0.000 description 1
DQPBABKTKYNPMH-UHFFFAOYSA-N amino hydrogen sulfate Chemical compound NOS(O)(=O)=O DQPBABKTKYNPMH-UHFFFAOYSA-N 0.000 description 1
DNAVOCNYHNNEQI-UHFFFAOYSA-N asaronaldehyde Natural products COC1=CC(OC)=C(C=CC=O)C=C1OC DNAVOCNYHNNEQI-UHFFFAOYSA-N 0.000 description 1
229940117916 cinnamic aldehyde Drugs 0.000 description 1
KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
229940073505 ethyl vanillin Drugs 0.000 description 1
239000000945 filler Substances 0.000 description 1
239000007952 growth promoter Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
230000003993 interaction Effects 0.000 description 1
LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 description 1
235000016709 nutrition Nutrition 0.000 description 1
244000144977 poultry Species 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
239000013049 sediment Substances 0.000 description 1
238000010186 staining Methods 0.000 description 1
239000012086 standard solution Substances 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1
239000010414 supernatant solution Substances 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
238000010998 test method Methods 0.000 description 1

Classifications

- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food

Landscapes

Engineering & Computer Science (AREA)
Food Science & Technology (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Chemical & Material Sciences (AREA)
Biochemistry (AREA)
Physics & Mathematics (AREA)
Analytical Chemistry (AREA)
Medicinal Chemistry (AREA)
General Health & Medical Sciences (AREA)
General Physics & Mathematics (AREA)
Immunology (AREA)
Pathology (AREA)
Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Investigating Or Analysing Biological Materials (AREA)
Fodder In General (AREA)
Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)

CS833610A 1982-05-26 1983-05-20 Method of vanilin-positive ionoforming substance quantity determination CS258112B2 (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GB8215419		1982-05-26

Publications (2)

Publication Number	Publication Date
CS361083A2 CS361083A2 (en)	1987-12-17
CS258112B2 true CS258112B2 (en)	1988-07-15

Family

ID=10530654

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS833610A CS258112B2 (en)	1982-05-26	1983-05-20	Method of vanilin-positive ionoforming substance quantity determination

Country Status (22)

Country	Link
JP (1)	JPS58223753A (fr)
AT (1)	AT391760B (fr)
BE (1)	BE896809A (fr)
CH (1)	CH656959A5 (fr)
CS (1)	CS258112B2 (fr)
DD (1)	DD209914A5 (fr)
DE (1)	DE3318597A1 (fr)
DK (1)	DK157713C (fr)
ES (1)	ES522640A0 (fr)
FI (1)	FI76643C (fr)
FR (1)	FR2527777B1 (fr)
GR (1)	GR79289B (fr)
HU (1)	HU185599B (fr)
IE (1)	IE54906B1 (fr)
IL (1)	IL68741A0 (fr)
IT (1)	IT1203653B (fr)
LU (1)	LU84814A1 (fr)
NL (1)	NL8301798A (fr)
NO (1)	NO163507C (fr)
PL (1)	PL136878B1 (fr)
RO (1)	RO86696B (fr)
SE (1)	SE8302832L (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US20090232949A1 (en) *	2008-03-12	2009-09-17	Zinpro Corporation	Fluorescent dye tracer method for animal feed supplement products

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CA998873A (en) *	1972-11-17	1976-10-26	Naremco	Prevention of fungi and molds in poultry and animal feedstuffs
US3915637A (en) *	1973-03-16	1975-10-28	A H P Inc	Analysis for water and feed additives

1983
- 1983-03-19 RO RO110998A patent/RO86696B/ro unknown
- 1983-05-19 FI FI831773A patent/FI76643C/fi not_active IP Right Cessation
- 1983-05-19 CH CH2740/83A patent/CH656959A5/fr not_active IP Right Cessation
- 1983-05-19 SE SE8302832A patent/SE8302832L/ unknown
- 1983-05-20 NL NL8301798A patent/NL8301798A/nl not_active Application Discontinuation
- 1983-05-20 BE BE6/47829A patent/BE896809A/fr not_active IP Right Cessation
- 1983-05-20 CS CS833610A patent/CS258112B2/cs unknown
- 1983-05-20 PL PL1983242095A patent/PL136878B1/pl unknown
- 1983-05-20 IL IL68741A patent/IL68741A0/xx not_active IP Right Cessation
- 1983-05-20 LU LU84814A patent/LU84814A1/fr unknown
- 1983-05-21 DE DE19833318597 patent/DE3318597A1/de not_active Withdrawn
- 1983-05-23 IE IE1212/83A patent/IE54906B1/en not_active IP Right Cessation
- 1983-05-24 DK DK231483A patent/DK157713C/da not_active IP Right Cessation
- 1983-05-24 ES ES522640A patent/ES522640A0/es active Granted
- 1983-05-24 NO NO831836A patent/NO163507C/no unknown
- 1983-05-24 IT IT48357/83A patent/IT1203653B/it active
- 1983-05-24 AT AT0187683A patent/AT391760B/de not_active IP Right Cessation
- 1983-05-24 GR GR71443A patent/GR79289B/el unknown
- 1983-05-25 FR FR8308588A patent/FR2527777B1/fr not_active Expired
- 1983-05-25 DD DD83251247A patent/DD209914A5/de not_active IP Right Cessation
- 1983-05-25 HU HU831848A patent/HU185599B/hu not_active IP Right Cessation
- 1983-05-25 JP JP58092209A patent/JPS58223753A/ja active Granted

Also Published As

Publication number	Publication date
RO86696A (fr)	1985-04-17
IT8348357A0 (it)	1983-05-24
DK157713B (da)	1990-02-05
LU84814A1 (fr)	1985-03-21
FI76643C (fi)	1988-11-10
DD209914A5 (de)	1984-05-23
FI831773L (fi)	1983-11-27
PL136878B1 (en)	1986-03-31
NL8301798A (nl)	1983-12-16
SE8302832L (sv)	1983-11-27
FI76643B (fi)	1988-07-29
FI831773A0 (fi)	1983-05-19
NO163507C (no)	1990-06-06
NO163507B (no)	1990-02-26
JPH0449654B2 (fr)	1992-08-12
GR79289B (fr)	1984-10-22
ES8407588A1 (es)	1984-10-01
AT391760B (de)	1990-11-26
DK231483A (da)	1983-11-27
IE54906B1 (en)	1990-03-14
DE3318597A1 (de)	1983-12-01
FR2527777A1 (fr)	1983-12-02
NO831836L (no)	1983-11-28
JPS58223753A (ja)	1983-12-26
IT1203653B (it)	1989-02-15
BE896809A (fr)	1983-11-21
IE831212L (en)	1983-11-26
FR2527777B1 (fr)	1986-03-21
RO86696B (ro)	1985-05-02
ATA187683A (de)	1990-05-15
PL242095A1 (en)	1983-12-05
HU185599B (en)	1985-02-28
SE8302832D0 (sv)	1983-05-19
IL68741A0 (en)	1983-09-30
DK157713C (da)	1990-07-16
CH656959A5 (fr)	1986-07-31
DK231483D0 (da)	1983-05-24
CS361083A2 (en)	1987-12-17
ES522640A0 (es)	1984-10-01

Publication	Publication Date	Title
Reid et al.	1951	Separation and estimation of saturated C2–C7 fatty acids by paper partition chromatography
US3212855A (en)	1965-10-19	Diagnostic device
US4003706A (en)	1977-01-18	Method and reagents for the detection, estimation and quantitative determination of nitrate ions
US3630680A (en)	1971-12-28	Diagnostic agents for the detection of urobilinogen materials in body fluids
US3016292A (en)	1962-01-09	Diagnostic composition
Edgar	1953	The chemical assay of progesterone
US3446599A (en)	1969-05-27	Method and composition for the detection of urobilinogen in fluids
CS258112B2 (en)	1988-07-15	Method of vanilin-positive ionoforming substance quantity determination
JPH0146029B2 (fr)	1989-10-05
US3771964A (en)	1973-11-13	Test composition and device for ascorbic acid determination
DE1773920A1 (de)	1971-12-02	Laboratoriumsreagens zur Bestimmung von AEthanol in Fluessigkeiten
GB2120787A (en)	1983-12-07	Method of estimating feed additives
JPH0257673B2 (fr)	1990-12-05
McNaught	1939	The determination of cobalt in animal tissues
Keng et al.	1992	High performance liquid chromatographic determination of tylosin in bovine muscle, kidney and liver
MacDonald et al.	1949	Spectrophotometric Method for Following Perodate Oxidations
FI88310C (fi)	1993-04-26	Foerfarande och medel foer bestaemning av urea
US3351431A (en)	1967-11-07	Formula and method for determining the proportion of fat in dairy products
SU1684661A1 (ru)	1991-10-15	Способ количественного определени витамина А
Coe	1936	Photochemical studies of rancidity: Induction period of protected and non‐protected oils
SU445749A1 (ru)	1974-10-05	Способ определени уреазной активности почвы
Borfitz et al.	1967	Determination of Buquinolate in Chicken Feeds by Thin Layer Chromatography and Fluorometry
Golden	1946	Peroxide test for mineral oils
McDaniel et al.	1973	The clearance of purines from the haemolymph of the cecropia silkmoth
Allen et al.	1962	The colorimetric determination of phenolphthalein