ES483285A1 - Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas - Google Patents

Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas

Info

Publication number
ES483285A1
ES483285A1 ES483285A ES483285A ES483285A1 ES 483285 A1 ES483285 A1 ES 483285A1 ES 483285 A ES483285 A ES 483285A ES 483285 A ES483285 A ES 483285A ES 483285 A1 ES483285 A1 ES 483285A1
Authority
ES
Spain
Prior art keywords
hydrogen
methyl
formula
benzyl
compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES483285A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Merck and Co Inc
Original Assignee
Merck and Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Merck and Co Inc filed Critical Merck and Co Inc
Publication of ES483285A1 publication Critical patent/ES483285A1/es
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D295/00Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
    • C07D295/096Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P21/00Drugs for disorders of the muscular or neuromuscular system
    • A61P21/02Muscle relaxants, e.g. for tetanus or cramps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • A61P25/20Hypnotics; Sedatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • A61P25/22Anxiolytics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P43/00Drugs for specific purposes, not provided for in groups A61P1/00-A61P41/00
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D295/00Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/10Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms
    • C07D295/112Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms with the ring nitrogen atoms and the doubly bound oxygen or sulfur atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings
    • C07D295/116Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms with the ring nitrogen atoms and the doubly bound oxygen or sulfur atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings with the doubly bound oxygen or sulfur atoms directly attached to a carbocyclic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D451/00Heterocyclic compounds containing 8-azabicyclo [3.2.1] octane, 9-azabicyclo [3.3.1] nonane, or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane or granatane alkaloids, scopolamine; Cyclic acetals thereof
    • C07D451/02Heterocyclic compounds containing 8-azabicyclo [3.2.1] octane, 9-azabicyclo [3.3.1] nonane, or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane or granatane alkaloids, scopolamine; Cyclic acetals thereof containing not further condensed 8-azabicyclo [3.2.1] octane or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane; Cyclic acetals thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Engineering & Computer Science (AREA)
  • Public Health (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Neurology (AREA)
  • Biomedical Technology (AREA)
  • Neurosurgery (AREA)
  • Anesthesiology (AREA)
  • Pain & Pain Management (AREA)
  • Orthopedic Medicine & Surgery (AREA)
  • Physical Education & Sports Medicine (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1. Un procedimiento para la preparación de nuevas dibenzo [a,d] ciclohepten-5,10-iminas sustituidas de fórmula: **(Fórmula-01)** en el que R es hidrógeno, metilo, estilo o bencilo; y R2 es hidrógeno, metilo o -CH2OH, caracterizado porque consiste en: a) someter a reacción de reducción un compuesto de fórmula: **(Fórmula-02)** en el que X, Y y Z son, independientemente, hidrógeno, cloro o bromo; R infinito es hidrógeno, hidroxilo, metilo, etilo, bencilo, o benzoilo; b) si se desea, someter a reacción de N-alquilación el producto procedente de la etapa anterior donde R es hidrógeno para producir el compuesto donde R es metilo, etilo o bencilo; y c) a continuación, si se desea, resolver el compuesto obtenido en un enantiómetro dextrógiro.
ES483285A 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas Expired ES483285A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US83463977A 1977-09-19 1977-09-19

Publications (1)

Publication Number Publication Date
ES483285A1 true ES483285A1 (es) 1980-09-01

Family

ID=25267426

Family Applications (7)

Application Number Title Priority Date Filing Date
ES473492A Expired ES473492A1 (es) 1977-09-19 1978-09-19 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas.sustituidas.
ES483286A Expired ES483286A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483285A Expired ES483285A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483287A Expired ES483287A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483288A Expired ES483288A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483284A Expired ES483284A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483283A Expired ES483283A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas (a,d) ciclo- hepten-5,10, sustituidas.

Family Applications Before (2)

Application Number Title Priority Date Filing Date
ES473492A Expired ES473492A1 (es) 1977-09-19 1978-09-19 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas.sustituidas.
ES483286A Expired ES483286A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas

Family Applications After (4)

Application Number Title Priority Date Filing Date
ES483287A Expired ES483287A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483288A Expired ES483288A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483284A Expired ES483284A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
ES483283A Expired ES483283A1 (es) 1977-09-19 1979-08-09 Un procedimiento para la preparacion de nuevas (a,d) ciclo- hepten-5,10, sustituidas.

Country Status (33)

Country Link
JP (1) JPS5463100A (es)
AR (1) AR231544A1 (es)
AT (1) AT370103B (es)
AU (1) AU520178B2 (es)
BE (1) BE870562A (es)
CA (1) CA1129850A (es)
CH (1) CH637954A5 (es)
CY (1) CY1283A (es)
DE (1) DE2840786A1 (es)
DK (1) DK153843C (es)
ES (7) ES473492A1 (es)
FI (1) FI65618C (es)
FR (1) FR2403334A1 (es)
GB (2) GB2061947B (es)
GR (1) GR65703B (es)
HK (1) HK30885A (es)
HU (1) HU180868B (es)
IE (1) IE47355B1 (es)
IL (1) IL55521A0 (es)
IT (1) IT1113279B (es)
KE (1) KE3501A (es)
LU (1) LU80262A1 (es)
NL (1) NL191488C (es)
NO (1) NO151861C (es)
NZ (1) NZ188361A (es)
PH (1) PH15920A (es)
PL (3) PL112834B1 (es)
PT (1) PT68544A (es)
SE (1) SE437520B (es)
SG (1) SG9585G (es)
SU (2) SU895288A3 (es)
YU (1) YU41432B (es)
ZA (1) ZA785291B (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4232158A (en) * 1979-06-04 1980-11-04 Merck & Co., Inc. 10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5,10-imines
US4477668A (en) * 1982-04-07 1984-10-16 Merck & Co., Inc. Process for 5-methyl-10,11-dihydro-5H-dibenzo[a,d]-cyclohepten-5,10-imine
GB8719199D0 (en) * 1987-08-13 1987-09-23 Merck Sharp & Dohme Chemical compounds
US5686614A (en) * 1995-04-11 1997-11-11 Neurogen Corporation Preparation of chiral 5-aminocarbonyl-5H-dibenzo a,d!cyclohepten-5,10-imines by optical resolution
US5739337A (en) * 1996-03-08 1998-04-14 Neurogen Corporation Process for preparing dibenzo-1-carboxamido-1,4-azabicyclo 3.2.1!octanes
EP3383429B1 (en) 2015-11-30 2020-10-14 INSERM - Institut National de la Santé et de la Recherche Médicale Nmdar antagonists for the treatment of tumor angiogenesis

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE794904A (fr) * 1972-02-04 1973-08-02 Roussel Uclaf Nouveaux derives du dibenzocycloheptene et leur preparation
BE829075A (fr) * 1974-05-15 1975-11-14 9,10-dihydroanthracen-9,10-imines substituees et leurs analogues heterocycliques (aza)

Also Published As

Publication number Publication date
ATA669778A (de) 1982-07-15
GB2061947B (en) 1982-08-04
AT370103B (de) 1983-03-10
YU219678A (en) 1983-02-28
NO151861C (no) 1985-06-19
FI65618C (fi) 1984-06-11
NL191488C (nl) 1995-08-04
AR231544A1 (es) 1984-12-28
ES483283A1 (es) 1980-04-16
IL55521A0 (en) 1978-12-17
HK30885A (en) 1985-04-26
SG9585G (en) 1985-08-08
JPS5463100A (en) 1979-05-21
AU3966878A (en) 1980-03-13
AU520178B2 (en) 1982-01-21
PT68544A (en) 1978-10-01
NO151861B (no) 1985-03-11
SE7809187L (sv) 1979-03-20
DE2840786A1 (de) 1979-03-22
CY1283A (en) 1985-07-05
DK153843C (da) 1989-01-23
KE3501A (en) 1985-02-22
DK389978A (da) 1979-03-20
LU80262A1 (fr) 1979-06-01
DE2840786C2 (es) 1987-05-21
NL7808847A (nl) 1979-03-21
GB2004872A (en) 1979-04-11
ES483284A1 (es) 1980-09-01
ES483288A1 (es) 1980-04-16
BE870562A (fr) 1979-03-19
NZ188361A (en) 1982-06-29
ZA785291B (en) 1980-04-30
FR2403334B1 (es) 1982-11-19
SU915800A3 (en) 1982-03-23
YU41432B (en) 1987-06-30
DK153843B (da) 1988-09-12
NO783017L (no) 1979-03-20
PL118478B1 (en) 1981-10-31
PL121605B1 (en) 1982-05-31
PL112834B1 (en) 1980-11-29
GR65703B (en) 1980-10-22
PL209632A1 (pl) 1979-06-04
CA1129850A (en) 1982-08-17
SU895288A3 (ru) 1981-12-30
IE47355B1 (en) 1984-02-22
GB2004872B (en) 1982-04-15
ES473492A1 (es) 1980-07-16
HU180868B (en) 1983-04-29
CH637954A5 (de) 1983-08-31
FR2403334A1 (fr) 1979-04-13
NL191488B (nl) 1995-04-03
PH15920A (en) 1983-04-22
IT7851126A0 (it) 1978-09-18
SE437520B (sv) 1985-03-04
FI782680A7 (fi) 1979-03-20
IE781866L (en) 1979-03-19
ES483286A1 (es) 1980-04-16
ES483287A1 (es) 1980-04-16
FI65618B (fi) 1984-02-29
JPS5639315B2 (es) 1981-09-11
GB2061947A (en) 1981-05-20
IT1113279B (it) 1986-01-20

Similar Documents

Publication Publication Date Title
DE69023934D1 (de) Substanz PF 1022, Verfahren zu ihrer Herstellung und diese Substanz enthaltende anthelmintische Zusammensetzung.
SE7707633L (sv) Forfarande for stereoselektiv framstellning av hexahydrodibensopyranoner smat mellanprodukter derfor
ATE18054T1 (de) Derivate und reduktionsprodukte der dglucopyranosyl-alpha(1-5)-d-arabonsaeure, deren herstellung und verwendung.
HUT48878A (en) Process for producing neopodophyllotoxin-benzylether derivatives
ES483285A1 (es) Un procedimiento para la preparacion de nuevas dibenzo (a,d)ciclohepten-5,10-iminas sustituidas
DE3576952D1 (de) Verfahren zur herstellung von 4-phenyl-pyrrol-derivaten.
NL186866C (nl) Werkwijze voor de bereiding van een waardevolle hoogaromatische pekachtige stof uit kool.
DE2860560D1 (en) 5-substituted-1,2-dihydro-3h-pyrrolo(1,2-a)pyrrole-1-carbonitriles and process for their conversion to the corresponding 1-carboxylic acids
PT68087A (en) Process for production of maleic anhydride from four-carbon hidrocarbons using catalysts preparared by hydrothermal techniques.
EP0152965A3 (en) Process for preparing 2,6-substituted-9-(1,3-dihydroxy-2-propoxy-menthyl)-purines and certain derivatives
JPS54119499A (en) Triazolobenzodiazepin derivative
FR2381733A1 (fr) Procede de preparation de m-bromo-a,a,a-trifluorotoluenes
DE3855002D1 (de) Verfahren zur Herstellung von Dodecahydro-3a,6,6,9a-tetramethylnaphto(2,1-b)furan
ATE5077T1 (de) 22-arylsulfonyl-24,25-dihydroxy-cholestane und verfahren zu ihrer herstellung.
JPS5423184A (en) Fermentor of organic waste
JPS5259111A (en) Process for preparation of acid-fluoride-containing fluoride having an ester group
ATE8638T1 (de) Verfahren zur herstellung von 17-alpha-hydroxy17beta-hydroxyacetyl-steroiden und die erhaltenen entsprechenden zwischenprodukte.
IL65664A0 (en) 5-(4-phenyl 1-piperidinyl)methyl-2,3-dihydro-2-oxo-1h-imidazole-4-carboxylic acid derivatives
GB1552166A (en) Polycyclic scents
JPS54145293A (en) Organic compound * method for producing same by microorganism and use
KR830007592A (ko) 약리활성체 4-[2-히드록시-4-(치환)페닐]나프탈렌-2(1h)-온 및 2-올, 이들 유도체 및 이들 중간체의 제조방법
US4094884A (en) 4α-Hydroxy-6-oxo-2β-arylmethoxy-methyl-3α-tetrahydropyranacetic acid γ-lactones
AU2172688A (en) Preparation of dien-1-ols, 9-hydroxydodec-10-enyl 1-tert-butyl ether and use thereof as an intermediate for synthesizing, 8,10-dodecadienol
US4094883A (en) 5-Iodo-6-oxo-3-(2&#39;-arylmethoxy-1&#39;-hydroxyethyl)-4-hydroxy-hexanoic acid, γ-lactone dialkyl acetals
PL296513A1 (en) Method of obtaining 20-oxo-17 alpha,21-dihydroxyl derivatives of pregnane and novel intermediate products