JP2907962B2 - 高感度ハロゲン化銀写真感光材料 - Google Patents

高感度ハロゲン化銀写真感光材料

Info

Publication number: JP2907962B2
Authority: JP; Japan
Prior art keywords: emulsion; silver halide; agx; particles; grains
Prior art date: 1990-06-19
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

JP2160954A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0451141A (ja

Inventor

博史大谷

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Konica Minolta Inc

Original Assignee

Konica Minolta Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-06-19

Filing date

1990-06-19

Publication date

1999-06-21

1990-06-19 Application filed by Konica Minolta Inc filed Critical Konica Minolta Inc

1990-06-19 Priority to JP2160954A priority Critical patent/JP2907962B2/ja

1991-06-15 Priority to DE69127404T priority patent/DE69127404T2/de

1991-06-15 Priority to EP91109834A priority patent/EP0462528B1/de

1992-02-19 Publication of JPH0451141A publication Critical patent/JPH0451141A/ja

1993-09-29 Priority to US08/129,026 priority patent/US5358841A/en

1999-06-21 Application granted granted Critical

1999-06-21 Publication of JP2907962B2 publication Critical patent/JP2907962B2/ja

2014-06-21 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

-1 silver halide Chemical class 0.000 title claims description 55
229910052709 silver Inorganic materials 0.000 title claims description 46
239000004332 silver Substances 0.000 title claims description 46
239000000463 material Substances 0.000 title claims description 26
230000035945 sensitivity Effects 0.000 title description 13
239000000839 emulsion Substances 0.000 claims description 87
229910021612 Silver iodide Inorganic materials 0.000 claims description 54
239000013078 crystal Substances 0.000 claims description 36
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 claims description 19
229940045105 silver iodide Drugs 0.000 claims description 19
239000002245 particle Substances 0.000 description 55
238000000034 method Methods 0.000 description 48
239000000243 solution Substances 0.000 description 24
239000007864 aqueous solution Substances 0.000 description 18
239000010410 layer Substances 0.000 description 18
239000010419 fine particle Substances 0.000 description 17
239000000203 mixture Substances 0.000 description 13
108010010803 Gelatin Proteins 0.000 description 11
150000001875 compounds Chemical class 0.000 description 11
229920000159 gelatin Polymers 0.000 description 11
239000008273 gelatin Substances 0.000 description 11
235000019322 gelatine Nutrition 0.000 description 11
235000011852 gelatine desserts Nutrition 0.000 description 11
238000004519 manufacturing process Methods 0.000 description 11
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Inorganic materials [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 9
238000002360 preparation method Methods 0.000 description 9
230000001235 sensitizing effect Effects 0.000 description 9
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 8
239000003795 chemical substances by application Substances 0.000 description 8
238000011161 development Methods 0.000 description 8
238000004090 dissolution Methods 0.000 description 8
239000012452 mother liquor Substances 0.000 description 8
206010070834 Sensitisation Diseases 0.000 description 7
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 7
230000000694 effects Effects 0.000 description 7
239000012071 phase Substances 0.000 description 7
230000008313 sensitization Effects 0.000 description 7
229910052717 sulfur Inorganic materials 0.000 description 7
239000011593 sulfur Substances 0.000 description 7
238000002156 mixing Methods 0.000 description 6
230000008569 process Effects 0.000 description 6
238000012545 processing Methods 0.000 description 6
239000000126 substance Substances 0.000 description 6
238000005406 washing Methods 0.000 description 6
150000002344 gold compounds Chemical class 0.000 description 5
239000011859 microparticle Substances 0.000 description 5
CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 4
239000000654 additive Substances 0.000 description 4
239000012153 distilled water Substances 0.000 description 4
238000009826 distribution Methods 0.000 description 4
BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 4
230000005070 ripening Effects 0.000 description 4
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 4
239000000725 suspension Substances 0.000 description 4
101710134784 Agnoprotein Proteins 0.000 description 3
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 3
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 3
229960000583 acetic acid Drugs 0.000 description 3
230000002776 aggregation Effects 0.000 description 3
238000004061 bleaching Methods 0.000 description 3
238000005345 coagulation Methods 0.000 description 3
230000015271 coagulation Effects 0.000 description 3
238000009792 diffusion process Methods 0.000 description 3
DROMNWUQASBTFM-UHFFFAOYSA-N dinonyl benzene-1,2-dicarboxylate Chemical compound CCCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCCC DROMNWUQASBTFM-UHFFFAOYSA-N 0.000 description 3
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 3
229910052737 gold Inorganic materials 0.000 description 3
239000010931 gold Substances 0.000 description 3
239000002609 medium Substances 0.000 description 3
229910000510 noble metal Inorganic materials 0.000 description 3
229910052711 selenium Inorganic materials 0.000 description 3
239000011669 selenium Substances 0.000 description 3
ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 3
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 3
239000006104 solid solution Substances 0.000 description 3
239000003381 stabilizer Substances 0.000 description 3
238000012546 transfer Methods 0.000 description 3
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
230000000274 adsorptive effect Effects 0.000 description 2
238000005054 agglomeration Methods 0.000 description 2
ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 description 2
230000008901 benefit Effects 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
239000003638 chemical reducing agent Substances 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
238000000576 coating method Methods 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
238000007796 conventional method Methods 0.000 description 2
238000011033 desalting Methods 0.000 description 2
239000006185 dispersion Substances 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
239000007788 liquid Substances 0.000 description 2
229910052943 magnesium sulfate Inorganic materials 0.000 description 2
235000019341 magnesium sulphate Nutrition 0.000 description 2
150000002736 metal compounds Chemical class 0.000 description 2
239000011591 potassium Substances 0.000 description 2
229910052700 potassium Inorganic materials 0.000 description 2
229910000027 potassium carbonate Inorganic materials 0.000 description 2
239000000047 product Substances 0.000 description 2
230000009467 reduction Effects 0.000 description 2
229910001961 silver nitrate Inorganic materials 0.000 description 2
HAAYBYDROVFKPU-UHFFFAOYSA-N silver;azane;nitrate Chemical compound N.N.[Ag+].[O-][N+]([O-])=O HAAYBYDROVFKPU-UHFFFAOYSA-N 0.000 description 2
230000006641 stabilisation Effects 0.000 description 2
238000011105 stabilization Methods 0.000 description 2
239000006228 supernatant Substances 0.000 description 2
UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 2
TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 description 1
CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 1
GGZHVNZHFYCSEV-UHFFFAOYSA-N 1-Phenyl-5-mercaptotetrazole Chemical compound SC1=NN=NN1C1=CC=CC=C1 GGZHVNZHFYCSEV-UHFFFAOYSA-N 0.000 description 1
QTLHLXYADXCVCF-UHFFFAOYSA-N 2-(4-amino-n-ethyl-3-methylanilino)ethanol Chemical compound OCCN(CC)C1=CC=C(N)C(C)=C1 QTLHLXYADXCVCF-UHFFFAOYSA-N 0.000 description 1
CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical compound NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 1
RYYXDZDBXNUPOG-UHFFFAOYSA-N 4,5,6,7-tetrahydro-1,3-benzothiazole-2,6-diamine;dihydrochloride Chemical compound Cl.Cl.C1C(N)CCC2=C1SC(N)=N2 RYYXDZDBXNUPOG-UHFFFAOYSA-N 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
PQUCIEFHOVEZAU-UHFFFAOYSA-N Diammonium sulfite Chemical compound [NH4+].[NH4+].[O-]S([O-])=O PQUCIEFHOVEZAU-UHFFFAOYSA-N 0.000 description 1
AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 description 1
LEVWYRKDKASIDU-IMJSIDKUSA-N L-cystine Chemical compound [O-]C(=O)[C@@H]([NH3+])CSSC[C@H]([NH3+])C([O-])=O LEVWYRKDKASIDU-IMJSIDKUSA-N 0.000 description 1
101150006989 NDEL1 gene Proteins 0.000 description 1
238000001016 Ostwald ripening Methods 0.000 description 1
239000004698 Polyethylene Substances 0.000 description 1
229910021607 Silver chloride Inorganic materials 0.000 description 1
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 description 1
229910021626 Tin(II) chloride Inorganic materials 0.000 description 1
XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
XCFIVNQHHFZRNR-UHFFFAOYSA-N [Ag].Cl[IH]Br Chemical compound [Ag].Cl[IH]Br XCFIVNQHHFZRNR-UHFFFAOYSA-N 0.000 description 1
XEIPQVVAVOUIOP-UHFFFAOYSA-N [Au]=S Chemical compound [Au]=S XEIPQVVAVOUIOP-UHFFFAOYSA-N 0.000 description 1
KWEGYAQDWBZXMX-UHFFFAOYSA-N [Au]=[Se] Chemical compound [Au]=[Se] KWEGYAQDWBZXMX-UHFFFAOYSA-N 0.000 description 1
230000009471 action Effects 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
239000003463 adsorbent Substances 0.000 description 1
230000002411 adverse Effects 0.000 description 1
239000006687 ag medium Substances 0.000 description 1
230000004931 aggregating effect Effects 0.000 description 1
238000004220 aggregation Methods 0.000 description 1
235000016720 allyl isothiocyanate Nutrition 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
XYXNTHIYBIDHGM-UHFFFAOYSA-N ammonium thiosulfate Chemical compound [NH4+].[NH4+].[O-]S([O-])(=O)=S XYXNTHIYBIDHGM-UHFFFAOYSA-N 0.000 description 1
229940101006 anhydrous sodium sulfite Drugs 0.000 description 1
229920006318 anionic polymer Polymers 0.000 description 1
239000003945 anionic surfactant Substances 0.000 description 1
150000001450 anions Chemical class 0.000 description 1
238000000137 annealing Methods 0.000 description 1
239000002216 antistatic agent Substances 0.000 description 1
UMEAURNTRYCPNR-UHFFFAOYSA-N azane;iron(2+) Chemical compound N.[Fe+2] UMEAURNTRYCPNR-UHFFFAOYSA-N 0.000 description 1
150000001540 azides Chemical class 0.000 description 1
239000007844 bleaching agent Substances 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
229910052798 chalcogen Inorganic materials 0.000 description 1
150000001787 chalcogens Chemical class 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
238000010411 cooking Methods 0.000 description 1
229960003067 cystine Drugs 0.000 description 1
230000007547 defect Effects 0.000 description 1
238000013461 design Methods 0.000 description 1
KYQODXQIAJFKPH-UHFFFAOYSA-N diazanium;2-[2-[bis(carboxymethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [NH4+].[NH4+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O KYQODXQIAJFKPH-UHFFFAOYSA-N 0.000 description 1
125000004177 diethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
230000008034 disappearance Effects 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000001804 emulsifying effect Effects 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
ALCDAWARCQFJBA-UHFFFAOYSA-N ethylselanylethane Chemical class CC[Se]CC ALCDAWARCQFJBA-UHFFFAOYSA-N 0.000 description 1
239000010946 fine silver Substances 0.000 description 1
229940050521 gelatin agent Drugs 0.000 description 1
239000012362 glacial acetic acid Substances 0.000 description 1
RJHLTVSLYWWTEF-UHFFFAOYSA-K gold trichloride Chemical compound Cl[Au](Cl)Cl RJHLTVSLYWWTEF-UHFFFAOYSA-K 0.000 description 1
150000004820 halides Chemical class 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
229910001385 heavy metal Inorganic materials 0.000 description 1
ZMZDMBWJUHKJPS-UHFFFAOYSA-N hydrogen thiocyanate Natural products SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 description 1
SSBBQNOCGGHKJQ-UHFFFAOYSA-N hydroxy-(4-methylphenyl)-oxo-sulfanylidene-$l^{6}-sulfane Chemical compound CC1=CC=C(S(S)(=O)=O)C=C1 SSBBQNOCGGHKJQ-UHFFFAOYSA-N 0.000 description 1
230000001969 hypertrophic effect Effects 0.000 description 1
230000001771 impaired effect Effects 0.000 description 1
229910017053 inorganic salt Inorganic materials 0.000 description 1
239000004816 latex Substances 0.000 description 1
229920000126 latex Polymers 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
239000000314 lubricant Substances 0.000 description 1
239000006224 matting agent Substances 0.000 description 1
230000010534 mechanism of action Effects 0.000 description 1
239000004530 micro-emulsion Substances 0.000 description 1
239000011259 mixed solution Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
150000002941 palladium compounds Chemical class 0.000 description 1
WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
229920000172 poly(styrenesulfonic acid) Polymers 0.000 description 1
229920000768 polyamine Polymers 0.000 description 1
229920000573 polyethylene Polymers 0.000 description 1
229940005642 polystyrene sulfonic acid Drugs 0.000 description 1
QUCBOTJDQJBEPB-KVVVOXFISA-M potassium (Z)-2-iodooctadec-9-enoate Chemical compound IC(C(=O)[O-])CCCCCC\C=C/CCCCCCCC.[K+] QUCBOTJDQJBEPB-KVVVOXFISA-M 0.000 description 1
238000000634 powder X-ray diffraction Methods 0.000 description 1
150000003142 primary aromatic amines Chemical class 0.000 description 1
239000011241 protective layer Substances 0.000 description 1
238000012552 review Methods 0.000 description 1
KIWUVOGUEXMXSV-UHFFFAOYSA-N rhodanine Chemical compound O=C1CSC(=S)N1 KIWUVOGUEXMXSV-UHFFFAOYSA-N 0.000 description 1
238000004062 sedimentation Methods 0.000 description 1
229940065287 selenium compound Drugs 0.000 description 1
150000003343 selenium compounds Chemical class 0.000 description 1
150000003346 selenoethers Chemical class 0.000 description 1
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 1
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
239000001509 sodium citrate Substances 0.000 description 1
NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
230000003595 spectral effect Effects 0.000 description 1
238000003892 spreading Methods 0.000 description 1
230000007480 spreading Effects 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
239000001119 stannous chloride Substances 0.000 description 1
235000011150 stannous chloride Nutrition 0.000 description 1
239000000758 substrate Substances 0.000 description 1
230000000153 supplemental effect Effects 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
XGMYMWYPSYIPQB-UHFFFAOYSA-J tetrasodium;2-(1,2-dicarboxylatoethoxy)butanedioate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CC(C([O-])=O)OC(C([O-])=O)CC([O-])=O XGMYMWYPSYIPQB-UHFFFAOYSA-J 0.000 description 1
DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical compound [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 description 1
HERBOKBJKVUALN-UHFFFAOYSA-K trisodium;2-[bis(carboxylatomethyl)amino]acetate;hydrate Chemical compound O.[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CC([O-])=O HERBOKBJKVUALN-UHFFFAOYSA-K 0.000 description 1

Classifications

- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/015—Apparatus or processes for the preparation of emulsions

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Physics & Mathematics (AREA)
General Physics & Mathematics (AREA)
Silver Salt Photography Or Processing Solution Therefor (AREA)

JP2160954A 1990-06-19 1990-06-19 高感度ハロゲン化銀写真感光材料 Expired - Fee Related JP2907962B2 (ja)

Priority Applications (4)

Application Number	Priority Date	Filing Date	Title
JP2160954A JP2907962B2 (ja)	1990-06-19	1990-06-19	高感度ハロゲン化銀写真感光材料
DE69127404T DE69127404T2 (de)	1990-06-19	1991-06-15	Verfahren zur Herstellung einer Silberhalogenidemulsion
EP91109834A EP0462528B1 (de)	1990-06-19	1991-06-15	Verfahren zur Herstellung einer Silberhalogenidemulsion
US08/129,026 US5358841A (en)	1990-06-19	1993-09-29	Method for preparing a silver halide emulsion

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP2160954A JP2907962B2 (ja)	1990-06-19	1990-06-19	高感度ハロゲン化銀写真感光材料

Publications (2)

Publication Number	Publication Date
JPH0451141A JPH0451141A (ja)	1992-02-19
JP2907962B2 true JP2907962B2 (ja)	1999-06-21

Family

ID=15725790

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP2160954A Expired - Fee Related JP2907962B2 (ja)	1990-06-19	1990-06-19	高感度ハロゲン化銀写真感光材料

Country Status (4)

Country	Link
US (1)	US5358841A (de)
EP (1)	EP0462528B1 (de)
JP (1)	JP2907962B2 (de)
DE (1)	DE69127404T2 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2992720B2 (ja) *	1992-01-31	1999-12-20	コニカ株式会社	ハロゲン化銀写真感光材料
DE10018934A1 (de) *	2000-04-17	2001-10-31	Agfa Gevaert Ag	Fotografische Silberhalogenidemulsion
CN112746268B (zh) *	2020-12-29	2023-04-25	武汉理工大学	一种具有偏光效应薄膜镀制的方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB1150013A (en) *	1965-09-22	1969-04-30	Fuji Photo Film Co Ltd	A Process for the Production of a Silver Halide Emulsion
US4459353A (en) *	1982-12-20	1984-07-10	Eastman Kodak Company	Gamma phase silver iodide emulsions, photographic elements containing these emulsions, and processes for their use
JPS616643A (ja) *	1984-06-20	1986-01-13	Konishiroku Photo Ind Co Ltd	ハロゲン化銀写真乳剤の製造方法
US4672026A (en) *	1985-10-04	1987-06-09	Eastman Kodak Company	Photographic elements containing bright yellow silver iodide
JP2670847B2 (ja) *	1988-04-11	1997-10-29	富士写真フイルム株式会社	ハロゲン化銀写真乳剤およびその製造方法
GB8821425D0 (en) *	1988-09-13	1988-10-12	Ciba Geigy Ag	Film halide emulsions
GB8821427D0 (en) *	1988-09-13	1988-10-12	Ciba Geigy Ag	Silver halide emulsions
JP2719540B2 (ja) *	1989-06-27	1998-02-25	コニカ株式会社	高感度ハロゲン化銀写真感光材料
US5262294A (en) *	1990-02-19	1993-11-16	Konica Corporation	Silver halide photographic light sensitive material

1990
- 1990-06-19 JP JP2160954A patent/JP2907962B2/ja not_active Expired - Fee Related
1991
- 1991-06-15 DE DE69127404T patent/DE69127404T2/de not_active Expired - Fee Related
- 1991-06-15 EP EP91109834A patent/EP0462528B1/de not_active Expired - Lifetime
1993
- 1993-09-29 US US08/129,026 patent/US5358841A/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
US5358841A (en)	1994-10-25
DE69127404T2 (de)	1998-01-02
EP0462528A1 (de)	1991-12-27
DE69127404D1 (de)	1997-10-02
JPH0451141A (ja)	1992-02-19
EP0462528B1 (de)	1997-08-27

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Publication	Publication Date	Title
US4349622A (en)	1982-09-14	Photographic silver halide emulsion comprising epitaxial composite silver halide crystals, silver iodobromide emulsion and process for preparing the same
US4610958A (en)	1986-09-09	Process of preparing a silver halide emulsion
JP2907962B2 (ja)	1999-06-21	高感度ハロゲン化銀写真感光材料
JP2719540B2 (ja)	1998-02-25	高感度ハロゲン化銀写真感光材料
JP2530843B2 (ja)	1996-09-04	ハロゲン化銀乳剤の製造方法
JP2864246B2 (ja)	1999-03-03	高画質画像の得られるハロゲン化銀写真感光材料
JPH09114030A (ja)	1997-05-02	臭化銀系感光性乳剤及びその製造方法
JPS6342769B2 (de)	1988-08-25
JPH05313273A (ja)	1993-11-26	ハロゲン化銀乳剤
JPH07113738B2 (ja)	1995-12-06	経時カブリ等の少ない改良されたハロゲン化銀写真感光材料
JPH0451140A (ja)	1992-02-19	圧力かぶり特性の良好なハロゲン化銀写真感光材料
JP2681172B2 (ja)	1997-11-26	ハロゲン化銀写真感光材料
JP2894612B2 (ja)	1999-05-24	薄膜化されたハロゲン化銀写真感光材料
US5362619A (en)	1994-11-08	High-speed halide photographic light-sensitive material
JP2929330B2 (ja)	1999-08-03	ハロゲン化銀写真乳剤の製造方法
JP2829620B2 (ja)	1998-11-25	ハロゲン化銀カラー写真感光材料
JP2907964B2 (ja)	1999-06-21	高感度で現像性が良好なハロゲン化銀乳剤
JPH03182738A (ja)	1991-08-08	感光性ハロゲン化銀乳剤
JPH06102604A (ja)	1994-04-15	ハロゲン化銀乳剤及びハロゲン化銀写真感光材料
JPH10293374A (ja)	1998-11-04	ハロゲン化銀写真乳剤
JPH0391736A (ja)	1991-04-17	ハロゲン化銀写真乳剤の化学増感法
JPH0442223A (ja)	1992-02-12	現像性と経時保存性の改良されたハロゲン化銀乳剤の製造方法及び該ハロゲン化銀乳剤を用いたハロゲン化銀写真感光材料
JPH10228069A (ja)	1998-08-25	ハロゲン化銀写真用乳剤及び写真感光材料
JPH02120849A (ja)	1990-05-08	ハロゲン化銀結晶粒子及びハロゲン化銀感光材料
JPH03235937A (ja)	1991-10-21	感度及び粒状性の改良された感光性ハロゲン化銀乳剤