JP5782038B2 - 等温多管式反応器及び該反応器を組み込んだプロセス - Google Patents

等温多管式反応器及び該反応器を組み込んだプロセス Download PDF

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JP5782038B2
JP5782038B2 JP2012533363A JP2012533363A JP5782038B2 JP 5782038 B2 JP5782038 B2 JP 5782038B2 JP 2012533363 A JP2012533363 A JP 2012533363A JP 2012533363 A JP2012533363 A JP 2012533363A JP 5782038 B2 JP5782038 B2 JP 5782038B2
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reactor
reaction
temperature
heat transfer
design
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JP2013507393A5 (2
JP2013507393A (ja
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マーカス ティルトウィッドジョジョ マックス
マーカス ティルトウィッドジョジョ マックス
フア バイ
フア バイ
チャクラボーティー デバシス
チャクラボーティー デバシス
アイフラー ユールゲン
アイフラー ユールゲン
グローネワルト ハインツ
グローネワルト ハインツ
フレデリック ヒルセコーン カート
フレデリック ヒルセコーン カート
ココット マンフレット
ココット マンフレット
ジェイ．クルーパー，ジュニア ウィリアム
ジェイ．クルーパー，ジュニア ウィリアム
ウルリッヒ ルエベ トマス
ウルリッヒ ルエベ トマス
モーリック パテル アバニ
モーリック パテル アバニ
ショー セクストン シャーリー
ショー セクストン シャーリー
ベンツェル ペーター
ベンツェル ペーター
ボブサー マルクス
ボブサー マルクス
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Dow Global Technologies LLC
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Dow Global Technologies LLC
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/2425—Tubular reactors in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • B01J19/0026—Avoiding carbon deposits
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2405—Stationary reactors without moving elements inside provoking a turbulent flow of the reactants, such as in cyclones, or having a high Reynolds-number
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/269—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/17—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing iodine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B01J2219/00063—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00247—Fouling of the reactor or the process equipment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0227—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of graphite

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
JP2012533363A 2009-10-09 2010-10-08 等温多管式反応器及び該反応器を組み込んだプロセス Expired - Fee Related JP5782038B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US25003009P 2009-10-09 2009-10-09
US61/250,030 2009-10-09
PCT/US2010/052073 WO2011044514A2 (en) 2009-10-09 2010-10-08 Isothermal multitube reactors and processes incorporating the same

Publications (3)

Publication Number Publication Date
JP2013507393A JP2013507393A (ja) 2013-03-04
JP2013507393A5 JP2013507393A5 (2) 2013-11-21
JP5782038B2 true JP5782038B2 (ja) 2015-09-24

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JP2012533363A Expired - Fee Related JP5782038B2 (ja) 2009-10-09 2010-10-08 等温多管式反応器及び該反応器を組み込んだプロセス

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US (2) US8558041B2 (2)
EP (1) EP2485832B1 (2)
JP (1) JP5782038B2 (2)
KR (1) KR20120091192A (2)
CN (1) CN102596387B (2)
BR (1) BR112012007914A2 (2)
WO (1) WO2011044514A2 (2)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102665890B (zh) * 2009-10-09 2016-02-24 蓝立方知识产权公司 生产氯化和/或氟化丙烯和高级烯烃的绝热活塞流反应器及方法
CN103717557A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
CN108929192A (zh) 2011-08-07 2018-12-04 蓝立方知识产权有限责任公司 生产氯化的丙烯的方法
US9540295B2 (en) 2011-09-30 2017-01-10 Honeywell International Inc. Process for producing 2-chloro-3,3,3-trifluoropropene and 2,3,3,3-tetrafluoropropene
KR20140104947A (ko) 2011-10-14 2014-08-29 셀마 벡터세빅 2,3,3,3-테트라플루오로프로펜의 제조 방법
JP6050375B2 (ja) 2011-12-02 2016-12-21 ブルー キューブ アイピー エルエルシー クロロアルカンの製造方法
CA2856545A1 (en) 2011-12-02 2013-06-06 Dow Global Technologies Llc Process for the production of chlorinated alkanes
DE102011121930A1 (de) * 2011-12-22 2013-06-27 Solarfuel Gmbh Methanisierungsreaktor
WO2013096706A1 (en) 2011-12-23 2013-06-27 Dow Global Technologies, Llc Process for the production of alkenes and/or aromatic compounds
US9598334B2 (en) 2012-09-20 2017-03-21 Blue Cube Ip Llc Process for the production of chlorinated propenes
EP2897930A1 (en) 2012-09-20 2015-07-29 Dow Global Technologies LLC Process for the production of chlorinated propenes
CA2885329A1 (en) 2012-09-30 2014-03-04 Dow Global Technologies Llc Weir quench and processes incorporating the same
US10065157B2 (en) 2012-10-26 2018-09-04 Blue Cube Ip Llc Mixer and processes incorporating the same
JP6247311B2 (ja) 2012-12-18 2017-12-13 ブルー キューブ アイピー エルエルシー 塩素化プロペンを生成するための方法
CA2894168C (en) 2012-12-19 2018-04-24 Dow Global Technologies Llc Process for the production of chlorinated propenes
US8889930B2 (en) 2013-01-22 2014-11-18 Axiall Ohio, Inc. Process for producing chlorinated hydrocarbons
US9289758B2 (en) 2013-01-22 2016-03-22 Axiall Ohio, Inc. Processes for producing chlorinated hydrocarbons and methods for recovering polyvalent antimony catalysts therefrom
CA2901450A1 (en) 2013-02-27 2014-09-04 Blue Cube Ip Llc Process for the production of chlorinated propenes
CA2903760C (en) 2013-03-09 2018-02-20 Blue Cube Ip Llc Process for the production of chlorinated alkanes
US9353029B2 (en) 2013-03-14 2016-05-31 Honeywell International, Inc. Fluorination process and reactor
US9139497B2 (en) 2013-10-23 2015-09-22 Axiall Ohio, Inc. Process for producing chlorinated hydrocarbons in the presence of a polyvalent bismuth compound
MX2016010294A (es) * 2014-02-10 2016-10-17 Honeywell Int Inc Diseño de reactor para la fluoracion en fase liquida.
JP2019522000A (ja) * 2016-06-23 2019-08-08 ブルー キューブ アイピー エルエルシー クロロアルカンの脱塩化水素化のためのプロセス
CN115635609A (zh) * 2022-10-25 2023-01-24 上海瑞宝造粒机有限公司 一种可流动物质的溢流堰装置

Family Cites Families (191)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2630461A (en) * 1953-03-03 Production of acetylene by incom
US2119484A (en) * 1935-05-06 1938-05-31 Du Pont Chlorination of propylene dichloride
GB471186A (en) 1936-02-28 1937-08-30 Du Pont Improvements in or relating to the manufacture of chlorine derivatives of unsaturated hydrocarbons
GB471188A (en) 1936-02-28 1937-08-30 Du Pont Improvements in or relating to the manufacture of chlorinated hydrocarbons
GB471187A (en) 1936-02-28 1937-08-30 Du Pont Improvements in or relating to the manufacture of chlorinated hydrocarbons
US2179378A (en) * 1936-07-18 1939-11-07 Air Reduction Production of acetylene
US2207193A (en) 1937-09-14 1940-07-09 Shell Dev Production of allyl type halides
US2299441A (en) * 1939-09-02 1942-10-20 Shell Dev Catalytic halo-substitution of saturated organic compounds
US2302228A (en) * 1940-04-02 1942-11-17 Du Pont Method of chlorination with sulphuryl chloride and production of monochloro-trimethyl acetic acid
US2370342A (en) * 1940-04-30 1945-02-27 Tide Water Associated Oil Comp Halogenation
US2378859A (en) 1941-08-08 1945-06-19 Distillers Co Yeast Ltd Splitting-off of hydrogen halide from halogenated hydrocarbons
US2449286A (en) * 1945-07-16 1948-09-14 Shell Dev Production of 1, 3-dihalopropylenes
US2435983A (en) * 1945-12-01 1948-02-17 Universal Oil Prod Co Production of liquid hydrocarbons
US2588867A (en) 1948-10-25 1952-03-11 Dow Chemical Co Pyrolytic production of chlorohydrocarbons
US2688592A (en) * 1950-10-21 1954-09-07 Diamond Alkali Co Photochemical process for preparing carbon tetrachloride
DE857955C (de) 1951-03-23 1952-12-04 Basf Ag Verfahren zur Herstellung von Tetrachloraethylen neben Tetrachlorkohlenstoff
US2762611A (en) * 1952-02-28 1956-09-11 Pfaudler Co Inc Tubular heat exchangers
US2765359A (en) * 1953-02-10 1956-10-02 Hydrocarbon Research Inc Production of acetylene
GB857086A (en) 1956-08-30 1960-12-29 Hoechst Ag Process for the manufacture of carbon tetrachloride
US3000980A (en) * 1958-04-07 1961-09-19 Dow Chemical Co Preparation of alkyl bromides
US2973393A (en) * 1958-10-02 1961-02-28 Dow Chemical Co Chlorination of acetylenes
US2964579A (en) * 1958-10-09 1960-12-13 Houdry Process Corp Selective hydrogenation of diolefins with copper chromite catalyst
US3094567A (en) * 1960-02-25 1963-06-18 Monsanto Chemicals Chlorination of propynes
US3112988A (en) 1960-02-26 1963-12-03 Sheil Oil Company Mixing gases at supersonic velocity
US3819731A (en) * 1960-03-23 1974-06-25 Stauffer Chemical Co Production of chlorinated unsaturated hydrocarbons
BE622939A (2) * 1961-09-28
US3446859A (en) * 1962-06-11 1969-05-27 Hooker Chemical Corp Vapor phase condensation process
US3502734A (en) * 1966-05-11 1970-03-24 Du Pont Process for partially chlorinating methyl chloride and/or methylene chloride
ES332724A1 (es) 1966-06-07 1967-12-01 El Paso Products Co Un procedimiento para la produccion de diolefinas.
DE1568921A1 (de) 1966-07-22 1970-03-26 Knapsack Ag Verfahren zur gemeinsamen Herstellung von 2,2,3- und 1,2,3-Trichlorbutan
US3444263A (en) * 1966-11-09 1969-05-13 Gulf Research Development Co Method for converting ethylene to alpha olefins in the presence of an organic sulfide
CH526333A (de) 1967-05-19 1972-08-15 Bayer Ag Verfahren und Vorrichtung zur Durchführung von Reaktionen zwischen Gasen
FR1546709A (fr) 1967-10-10 1968-11-22 Mini Ind Chimice Procédé et appareil pour la fabrication en système continu de nitrosodérivés d'hydrocarbures
DE1904426C3 (de) * 1969-01-30 1974-02-28 Farbwerke Hoechst Ag, Vormals Meister Lucius & Bruening, 6000 Frankfurt Verfahren zur Herstellung von Tetrachlorkohlenstoff aus Benzol und Chlor
US3558438A (en) * 1968-10-30 1971-01-26 Du Pont Distillation process and apparatus
US3551512A (en) * 1968-11-01 1970-12-29 Diamond Shamrock Corp Pressure process for preparing acetylene
US4513154A (en) * 1971-07-30 1985-04-23 Allied Corporation Process for consecutive competitive gas phase reaction
US3823195A (en) * 1971-12-27 1974-07-09 Monsanto Co Preparation of 1,1,2,3-tetrachloropropene from 1,2,3-trichloropropane
NL160542C (nl) 1971-12-17 1979-11-15 Monsanto Co Werkwijze voor het bereiden van 1,1,2,3,-tetrachloorpro- peen.
US3926758A (en) * 1971-12-27 1975-12-16 Monsanto Co Preparation of 1,1,2,3-tetrachloropropene from 2,3-trichloropropane
DE2257005A1 (de) * 1972-11-21 1974-05-22 Merck Patent Gmbh Loesungsmittel fuer die kernresonanzspektroskopie
CH609022A5 (en) 1973-06-12 1979-02-15 Monsanto Co Process for the preparation of 1,2,3-trichloropropene from 1,2,3-trichloropropane
NL7313098A (2) * 1973-09-22 1974-03-25
US3872664A (en) * 1973-10-15 1975-03-25 United Aircraft Corp Swirl combustor with vortex burning and mixing
US3914167A (en) * 1974-08-26 1975-10-21 Dow Chemical Co Process for making cis-1,3-dichloropropene
US4051182A (en) * 1976-04-12 1977-09-27 Stauffer Chemical Company Process for the manufacture of α-chloropropionyl chloride
US4038372A (en) 1976-05-05 1977-07-26 The United States Of America As Represented By The Secretary Of The Navy Process for manufacturing chloramine
US4319062A (en) 1976-08-02 1982-03-09 The Dow Chemical Company Allyl chloride process
JPS5479207U (2) 1977-11-14 1979-06-05
JPS5720859Y2 (2) 1978-03-14 1982-05-06
SU899523A1 (ru) 1979-07-03 1982-01-23 Уфимский Нефтяной Институт Способ получени 1,1,2,3-тетрахлорпропена
JPS58501376A (ja) 1981-09-01 1983-08-18 オラ−，ジヨ−ジ　アンドル− メタンからハロゲン化メチル類およびメチルアルコ−ル
US4650914A (en) * 1983-07-06 1987-03-17 Monsanto Company Process for producing 1,1,2,3-tetrachloropropene
US4535194A (en) * 1983-07-06 1985-08-13 Monsanto Co. Process for producing 1,1,2,3-tetrachloropropene
DE3415334A1 (de) * 1983-08-25 1985-03-14 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von 1,1,2-trichlor-2-methyl-propan
DE3415337A1 (de) * 1983-08-25 1985-03-14 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von 3,3-dichlor-2-methyl-propen
DE3415336A1 (de) * 1984-04-25 1985-10-31 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von 1,2,3-trichlor-2-methyl-propan
FR2569182B1 (fr) * 1984-08-20 1986-12-05 Solvay Procede pour effectuer des reactions de chloration substitutive de composes organiques au moyen de chlore moleculaire en presence d'un produit chlore servant d'initiateur radicalaire et initiateurs radicalaires utilises dans un tel procede
DE3432720A1 (de) * 1984-09-06 1986-03-06 Hüls AG, 4370 Marl Verfahren zur herstellung von 1,2,3-trichlorpropan
US4614572A (en) * 1985-07-08 1986-09-30 The Dow Chemical Company Liquid phase chlorination of chlorinated methanes
DE3681768D1 (de) * 1985-07-30 1991-11-07 Hartmut Wolf Zerstaeubungsvorrichtung.
US4644907A (en) * 1985-11-29 1987-02-24 Hunter Edward H Boiler tubes of enhanced efficiency and method of producing same
US4727181A (en) * 1986-04-21 1988-02-23 The Dow Chemical Company Process for the preparation of α-halocinnamate esters
GB8708618D0 (en) 1987-04-10 1987-05-13 Ici Plc Production process
GB8721964D0 (en) * 1987-09-18 1987-10-28 Shell Int Research Multitube reactor
US5171899A (en) * 1988-05-17 1992-12-15 Daikin Industries Ltd. Process for production of 1,1,1-trifluoro-2,2-dichloroethane
JPH01290639A (ja) * 1988-05-17 1989-11-22 Daikin Ind Ltd １，１，１−トリフルオロ−２，２−ジクロロエタンの製造法
US4999102A (en) * 1988-12-16 1991-03-12 The Amalgamated Sugar Company Liquid transfer manifold system for maintaining plug flow
US5254771A (en) * 1989-07-14 1993-10-19 Hoechst Aktiengesellschaft Process for the preparation of 1,1,1-trifluoro-2-2-dichloroethane under elevated pressure
US5057634A (en) * 1989-12-19 1991-10-15 E. I. Du Pont De Nemours And Company Multistep synthesis of hexafluoropropylene
US5178844A (en) 1990-04-03 1993-01-12 Phillips Petroleum Company Method and apparatus for producing nitride products
DE4012007A1 (de) 1990-04-13 1991-10-17 Erdoelchemie Gmbh Verfahren zur reduktiven dehydrohalogenierung von halogenkohlenwasserstoffen und halogenethern
GB9105167D0 (en) * 1991-03-12 1991-04-24 Ici Plc Chemical process
US5254788A (en) * 1991-09-10 1993-10-19 Stone And Webster Engineering Corporation Process for the production of olefins from light paraffins
US5262575A (en) 1992-08-04 1993-11-16 The Dow Chemical Company Production of allylic chlorides
GB9315450D0 (en) * 1993-07-26 1993-09-08 Zeneca Ltd Chlorination process
US5414166A (en) * 1993-11-29 1995-05-09 Korea Institute Of Science And Technology Process for the preparation of 1,1,1-trifluoro-2,2-dichloroethane
US5504266A (en) 1995-05-24 1996-04-02 The Dow Chemical Company Process to make allyl chloride and reactor useful in that process
US5616819A (en) * 1995-08-28 1997-04-01 Laroche Industries Inc. Process for preparing fluorinated aliphatic compounds
US5689020A (en) * 1996-03-11 1997-11-18 Laroche Industries Inc. High temperature chlorination process for the preparation of polychloroolefins
US6111150A (en) * 1996-06-20 2000-08-29 Central Glass Company, Limited Method for producing 1,1,1,3,3,-pentafluoropropane
US6538167B1 (en) * 1996-10-02 2003-03-25 Exxonmobil Chemical Patents Inc. Process for producing light olefins
US5986151A (en) * 1997-02-05 1999-11-16 Alliedsignal Inc. Fluorinated propenes from pentafluoropropane
US5811605A (en) * 1997-02-19 1998-09-22 Ppg Industries, Inc. Preparation of 1,2,3,3-tetrachloropropene
US5912309A (en) 1997-07-16 1999-06-15 Union Carbide Chemicals & Plastics Technology Corporation Gas phase fluidized bed polymerization process using sonic cleaner with optimum design and operation
US5895825A (en) * 1997-12-01 1999-04-20 Elf Atochem North America, Inc. Preparation of 1,1,1,3,3-pentafluoropropane
CN1143842C (zh) * 1997-12-18 2004-03-31 陶氏环球技术公司 在绝热反应器系统中制造二醇的方法
JP3518321B2 (ja) * 1998-03-23 2004-04-12 ダイキン工業株式会社 １，１，１，３，３−ペンタフルオロプロパンの製造方法
US6187976B1 (en) * 1998-04-09 2001-02-13 Alliedsignal Inc. Process for the preparation of fluorine containing hydrohalocarbons
ATE220657T1 (de) * 1998-11-04 2002-08-15 Rohm & Haas Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure
US6273180B1 (en) * 1998-12-23 2001-08-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'eploitation Des Procedes Georges Claude Heat exchanger for preheating an oxidizing gas
TW527218B (en) * 1999-03-16 2003-04-11 Basf Ag Multitube reactor, especially for catalytic gas-phase reactions
EP1060788A1 (en) * 1999-06-15 2000-12-20 Methanol Casale S.A. Isothermal catalytic reactor for exothermic or endothermic heterogeneous reactions
JP4891503B2 (ja) * 1999-06-16 2012-03-07 ゾルファイ フルーオル ゲゼルシャフト ミット ベシュレンクテル ハフツング Ｕｖ−活性化塩素化
DE19952754A1 (de) 1999-11-02 2001-05-10 Krc Umwelttechnik Gmbh Verfahren und Vorrichtung zur Kühlung und Reinigung von Vergasungsgasen
MXPA02005142A (es) 1999-11-22 2002-11-07 Dow Chemical Co Un proceso para la conversion de etileno en cloruro de vinilo, y composiciones catalizadoras novedosas utiles para este proceso.
JP3869170B2 (ja) 1999-11-22 2007-01-17 セントラル硝子株式会社 １，１，１，３，３−ペンタクロロプロパンの製造方法
CN1297999A (zh) 1999-11-24 2001-06-06 上海博容基因开发有限公司 一种新的多肽——人谷氨酰转移核糖核酸合成酶58和编码这种多肽的多核苷酸
US6118018A (en) * 1999-12-06 2000-09-12 Occidental Chemical Corporation Chlorination and bromination of aromatic compounds at atmospheric pressure
JP2001213820A (ja) 2000-01-31 2001-08-07 Central Glass Co Ltd １，１，１，３，３−ペンタクロロプロパンの製造方法
US6613127B1 (en) 2000-05-05 2003-09-02 Dow Global Technologies Inc. Quench apparatus and method for the reformation of organic materials
DE10054840A1 (de) * 2000-11-04 2002-08-08 Xcellsis Gmbh Verfahren und Vorrichtung zum Starten eines Reaktors in einem Gaserzeugungssystem
US6551469B1 (en) * 2001-11-27 2003-04-22 Honeywell International Photochlorination of 1,1,1,3,3-pentafluoropropane
EP2361899B1 (en) * 2002-01-11 2015-07-22 Mitsubishi Chemical Corporation Vapor phase catalytic oxidation method using a multitube reactor of the heat-exchange type
US7117934B2 (en) * 2002-03-15 2006-10-10 H2Gen Innovations, Inc. Method and apparatus for minimizing adverse effects of thermal expansion in a heat exchange reactor
US6924403B2 (en) 2002-06-26 2005-08-02 E. I. Du Pont De Nemours And Company Synthesis of hexafluoropropylene
US6683216B1 (en) * 2002-11-06 2004-01-27 Eastman Chemical Company Continuous process for the preparation of amines
GB0301660D0 (en) * 2003-01-24 2003-02-26 Redding John Dredging scouring & excavation
WO2004067164A1 (de) * 2003-01-31 2004-08-12 Man Dwe Gmbh Mantelrohrreaktor zur durchführung katalytischer gasphasenreaktionen und verfahren zum betreiben eines solchen
EP1603965B1 (en) * 2003-03-07 2007-02-07 Dow Global Technologies Inc. Continuous process and system of producing polyether polyols
US7588739B2 (en) * 2003-07-14 2009-09-15 Mitsubishi Rayon Co., Ltd. Fixed bed multitube reactor
US7880040B2 (en) 2004-04-29 2011-02-01 Honeywell International Inc. Method for producing fluorinated organic compounds
US20060292046A1 (en) * 2003-07-31 2006-12-28 Dow Global Technologies Inc. Oxidation process and reactor with modified feed system
CN1819869A (zh) * 2003-07-31 2006-08-16 陶氏环球技术公司 氧化方法和具有改良进料系统的反应器
US6825383B1 (en) * 2003-09-22 2004-11-30 Council Of Scientific And Industrial Research Catalytic process for regiospecific chlorination of alkanes, alkenes and arenes
US7371904B2 (en) * 2004-04-29 2008-05-13 Honeywell International Inc. Processes for synthesis of 1,3,3,3-tetrafluoropropene
MXPA06012466A (es) * 2004-04-29 2007-01-31 Honeywell Int Inc Procesos para la sintesis de 1,3,3,3-tetrafluoropropeno y 2,3,3,3-tetrafluoropropeno.
CN1972887B (zh) * 2004-04-29 2010-10-13 霍尼韦尔国际公司 1,3,3,3-四氟丙烯的合成方法
US8084653B2 (en) * 2004-04-29 2011-12-27 Honeywell International, Inc. Method for producing fluorinated organic compounds
US7951982B2 (en) 2004-04-29 2011-05-31 Honeywell International Inc. Method for producing fluorinated organic compounds
US7674939B2 (en) * 2004-04-29 2010-03-09 Honeywell International Inc. Method for producing fluorinated organic compounds
US9102579B2 (en) * 2004-04-29 2015-08-11 Honeywell International Inc. Method for producing fluorinated organic compounds
US8383867B2 (en) * 2004-04-29 2013-02-26 Honeywell International Inc. Method for producing fluorinated organic compounds
US7659434B2 (en) * 2004-04-29 2010-02-09 Honeywell International Inc. Method for producing fluorinated organic compounds
US8058486B2 (en) 2004-04-29 2011-11-15 Honeywell International Inc. Integrated process to produce 2,3,3,3-tetrafluoropropene
US20080021229A1 (en) * 2004-05-21 2008-01-24 Maughon Bob R Process for Preparing Epichlorhydrin from Ethane
MY142153A (en) * 2004-12-10 2010-09-30 Shell Int Research Reactor tube apparatus
CN101090767A (zh) * 2004-12-22 2007-12-19 纳幕尔杜邦公司 用于光化学反应的末端官能化全氟(烷基乙烯基醚)的官能化共聚物的反应器壁、增加烃和卤代烃的氟含量的方法和烯烃的制备
JP4501158B2 (ja) 2005-03-30 2010-07-14 富士フイルム株式会社 マイクロ化学装置の運転方法
US7396965B2 (en) * 2005-05-12 2008-07-08 Honeywell International Inc. Method for producing fluorinated organic compounds
US7511101B2 (en) * 2005-05-13 2009-03-31 Fina Technology, Inc. Plug flow reactor and polymers prepared therewith
JP2007021396A (ja) 2005-07-19 2007-02-01 Japan Science & Technology Agency 重金属の除去方法
WO2007018298A1 (en) 2005-08-09 2007-02-15 Canon Kabushiki Kaisha Fluid-processing device and fluid-processing method
DE102005044501A1 (de) 2005-09-16 2007-03-22 Roquette, Eberhard, Dipl.-Ing. Veresterungsdüse
CA2635806C (en) 2006-01-03 2015-03-31 Honeywell International, Inc. Method for producing fluorinated organic compounds
US8071825B2 (en) * 2006-01-03 2011-12-06 Honeywell International Inc. Method for producing fluorinated organic compounds
ES3036520T3 (en) 2006-01-03 2025-09-19 Honeywell Int Inc Method for producing fluorinated organic compounds
US7695695B2 (en) * 2006-01-18 2010-04-13 Lg Chem, Ltd. Reactor or heat exchanger with improved heat transfer performance
DE102007008876A1 (de) 2006-02-21 2007-12-27 Sachtleben Chemie Gmbh Verfahren zur Durchführung chemischer und physikalischer Prozesse und Reaktionszelle
EP2001828B1 (en) * 2006-03-31 2012-08-22 E.I. Du Pont De Nemours And Company Coproduction of hydrofluoroolefins
US7836941B2 (en) * 2006-05-19 2010-11-23 Exxonmobil Research And Engineering Company Mitigation of in-tube fouling in heat exchangers using controlled mechanical vibration
US20080073063A1 (en) * 2006-06-23 2008-03-27 Exxonmobil Research And Engineering Company Reduction of fouling in heat exchangers
FR2902785B1 (fr) * 2006-06-26 2008-08-08 Solvay Procede de fabrication de 1,2-dichloroethane
JP2008063314A (ja) 2006-09-04 2008-03-21 Tokyo Kasei Kogyo Kk 環境調和型超原子価ヨウ素試剤
CN101578252B (zh) * 2006-09-05 2013-11-27 纳幕尔杜邦公司 1,2,3,3,3-五氟丙烯生产方法
CN103483140B (zh) 2006-10-31 2015-09-09 纳幕尔杜邦公司 氟丙烷、卤代丙烯以及2-氯-3,3,3-三氟-1-丙烯与hf的共沸组合物和1,1,1,2,2-五氟丙烷与hf的共沸组合物的制备方法
US20080207962A1 (en) * 2007-02-23 2008-08-28 Velliyur Nott Mallikarjuna Rao Compositions containing chromium, oxygen, and at least two modifier metals selected the group consisting of gold, silver, and palladium, their preparation, and their use as catalysts and catalyst precursors
EP2135888A4 (en) 2007-04-10 2014-10-01 Asahi Glass Co Ltd COMPOUND CATALYST OF METAL CYANIDE COMPLEX WITH ORGANIC LIGAND, METHOD OF MANUFACTURING THEREOF, AND METHOD FOR PRODUCING POLYETHEREPOLYOLE
JP2009000592A (ja) 2007-06-19 2009-01-08 Hitachi Ltd 反応器および反応システム
KR101550250B1 (ko) 2007-06-27 2015-09-04 알케마 인코포레이티드 하이드로플루오로올레핀의 제조 방법
JP2010531897A (ja) 2007-06-27 2010-09-30 アーケマ・インコーポレイテッド ヒドロフルオロオレフィンを製造する２段階法
US20090018377A1 (en) * 2007-07-09 2009-01-15 Boyce C Bradford Catalytic process for the preparation of fluorinated halocarbons
JP5339229B2 (ja) 2007-07-24 2013-11-13 ナガセケムテックス株式会社 超原子価ヨウ素反応剤を用いる芳香族化合物および複素環式芳香族化合物のポリマーの製造方法
US8258355B2 (en) * 2007-07-25 2012-09-04 Honeywell International Inc. Processes for preparing 1,1,2,3-tetrachloropropene
US7795480B2 (en) 2007-07-25 2010-09-14 Honeywell International Inc. Method for producing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf)
US9035111B2 (en) * 2007-08-22 2015-05-19 Honeywell International Inc. Method for producing fluorinated organic compounds
EP2190954A1 (de) 2007-09-18 2010-06-02 Uhde GmbH Vergasungsreaktor und verfahren zur flugstromvergasung
US8367867B2 (en) 2007-10-04 2013-02-05 Urea Casale S.A. Process and plant for urea production
US9079818B2 (en) * 2007-10-15 2015-07-14 Honeywell International Inc. Process for synthesis of fluorinated olefins
US20090117014A1 (en) * 2007-11-06 2009-05-07 Quantumsphere, Inc. System and method for ammonia synthesis
RU2010125261A (ru) 2007-11-20 2011-12-27 Е.И. Дюпон Де Немур Энд Компани (Us) Синтез гидрофторалканолов и гидрофторалкенов
US8115038B2 (en) 2007-12-19 2012-02-14 Occidental Chemical Corporation Methods of making chlorinated hydrocarbons
GB0800470D0 (en) 2008-01-11 2008-02-20 Redding John Improvements in or relating to jet nozzles
US8071826B2 (en) * 2008-04-04 2011-12-06 Honeywell International Inc. Process for the preparation of 2,3,3,3-tetrafluoropropene (HFO-1234yf)
CN102119145B (zh) 2008-08-07 2014-06-18 巴斯夫欧洲公司 制备芳香族异氰酸酯的方法
US9051231B2 (en) 2008-09-25 2015-06-09 Central Glass Company, Limited Process for producing 1,3,3,3-tetrafluoropropene
JP6022770B2 (ja) 2008-10-13 2016-11-09 ブルー キューブ アイピー エルエルシー 塩素化及び／又はフッ素化プロペンの製造方法
WO2010059493A1 (en) 2008-11-19 2010-05-27 Arkema Inc. Process for the manufacture of hydrofluoroolefins
KR20110114529A (ko) * 2008-12-25 2011-10-19 아사히 가라스 가부시키가이샤 1,1-디클로로-2,3,3,3-테트라플루오로프로펜 및 2,3,3,3-테트라플루오로프로펜의 제조 방법
CN101492341B (zh) 2009-03-05 2012-03-28 杨海珍 饱和多氯代烷烃的制备方法
KR101374000B1 (ko) 2009-04-23 2014-03-12 다이킨 고교 가부시키가이샤 2,3,3,3-테트라플루오로프로펜의 제조 방법
CN101544535B (zh) 2009-05-01 2012-07-18 浙江三美化工股份有限公司 一种合成1,1,1,3,3-五氯丙烷的制备方法
JP5459320B2 (ja) 2009-05-13 2014-04-02 ダイキン工業株式会社 塩素含有フルオロカーボン化合物の製造方法
JP5767231B2 (ja) 2009-10-09 2015-08-19 ダウ グローバル テクノロジーズ エルエルシー 塩素化及び／又はフッ素化されたプロペン及びより高級なアルケンを製造するプロセス
BR112012007916A2 (pt) 2009-10-09 2019-09-24 Dow Global Technologies Llc processo de etapa para a produção de propenos clorados ou fluorados e processo para preparar 1,1,3,3 - tetrafluorprop-1-eno
JP2013510869A (ja) 2009-11-16 2013-03-28 アーケマ・インコーポレイテッド クロロオレフィンを精製および安定化させるための方法
EP2504299B1 (en) 2009-11-27 2018-01-17 Daikin Industries, Ltd. Process for preparing 1,1,2,3-tetrachloropropene
WO2011077191A1 (en) 2009-12-23 2011-06-30 Arkema France Catalytic gas phase fluorination of 1230xa to 1234yf
JP2011144148A (ja) 2010-01-18 2011-07-28 Nippon Zeon Co Ltd 含水素ハロゲン化シクロペンタン、及びヘプタフルオロシクロペンテンの製造方法
CN101955414A (zh) 2010-04-20 2011-01-26 南通泰禾化工有限公司 1,1,2,3-四氯丙烯生产工艺
DE102010022414A1 (de) 2010-06-01 2011-12-01 Günther Kramb jun. Emulgiervorrichtung
PL2596859T3 (pl) 2010-07-21 2020-04-30 Otkrytoe Aktsionernoe Obschestvo Research & Design Institute Of Urea And Organic Synthesis Products (Oao Niik) Reaktor gazowo-cieczowy z komorą mieszania wirowego
CN101913980A (zh) 2010-09-07 2010-12-15 西安近代化学研究所 1，1，1，3，3-五氯丙烷的生产方法
CN101913979A (zh) 2010-09-07 2010-12-15 西安近代化学研究所 1，1，1，3，3-五氯丁烷的生产方法
CN101982227B (zh) 2010-09-15 2013-03-20 山东东岳高分子材料有限公司 一种用于高温裂解的气体快速混合反应装置及应用
CN102001911B (zh) 2010-09-20 2013-09-25 西安近代化学研究所 2,3,3,3-四氟丙烯的制备方法
KR101756752B1 (ko) 2010-12-16 2017-07-12 가부시끼가이샤 도꾸야마 탄소수 3의 염소화탄화수소의 제조 방법
CN102249846B (zh) 2011-05-31 2013-05-08 浙江师范大学 一种2-氯-3, 3, 3-三氟丙烯和2, 3-二氯-1, 1-二氟丙烯的联产制备方法
WO2012166394A1 (en) 2011-05-31 2012-12-06 Dow Global Technologies, Llc Process for the production of chlorinated propenes
JP6212035B2 (ja) 2011-05-31 2017-10-11 ブルー キューブ アイピー エルエルシー 塩素化プロペンの製造方法
CN102351637B (zh) 2011-08-31 2013-10-23 浙江师范大学 一种2, 3, 3, 3-四氟丙烯的制备方法

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