JPH0149340B2 - - Google Patents

Info

Publication number: JPH0149340B2
Authority: JP; Japan
Prior art keywords: fluoride; manufacturing; reaction; alkali metal; carried out
Prior art date: 1983-12-26
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP58251070A

Other languages

English (en)

Japanese (ja)

Other versions

JPS60136536A (ja

Inventor

Yonosuke Aisaka

Takashi Totsuka

Shoji Takagi

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Daikin Industries Ltd

Original Assignee

Daikin Kogyo Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-12-26

Filing date

1983-12-26

Publication date

1989-10-24

1983-12-26 Application filed by Daikin Kogyo Co Ltd filed Critical Daikin Kogyo Co Ltd

1983-12-26 Priority to JP58251070A priority Critical patent/JPS60136536A/ja

1984-12-19 Priority to KR1019840008099A priority patent/KR870002015B1/ko

1984-12-20 Priority to US06/684,344 priority patent/US4719052A/en

1984-12-21 Priority to DE8484116103T priority patent/DE3482258D1/de

1984-12-21 Priority to CA000470916A priority patent/CA1293739C/en

1984-12-21 Priority to EP87113971A priority patent/EP0258911B1/de

1984-12-21 Priority to EP84116103A priority patent/EP0148490B1/de

1984-12-21 Priority to DE8787113971T priority patent/DE3483535D1/de

1985-07-20 Publication of JPS60136536A publication Critical patent/JPS60136536A/ja

1989-10-24 Publication of JPH0149340B2 publication Critical patent/JPH0149340B2/ja

1991-02-27 Priority to CA000616011A priority patent/CA1318327C/en

Status Granted legal-status Critical Current

Links

OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 12
OFWDLJKVZZRPOX-UHFFFAOYSA-N 2,2,3,3-tetrafluorooxetane Chemical compound FC1(F)COC1(F)F OFWDLJKVZZRPOX-UHFFFAOYSA-N 0.000 claims description 11
238000006243 chemical reaction Methods 0.000 claims description 11
DZXSTVONXZVOKT-UHFFFAOYSA-N 2,2,3-trifluoropropanoyl fluoride Chemical compound FCC(F)(F)C(F)=O DZXSTVONXZVOKT-UHFFFAOYSA-N 0.000 claims description 10
238000004519 manufacturing process Methods 0.000 claims description 10
229910001515 alkali metal fluoride Inorganic materials 0.000 claims description 8
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 6
239000002841 Lewis acid Substances 0.000 claims description 5
150000007517 lewis acids Chemical class 0.000 claims description 5
229910018287 SbF 5 Inorganic materials 0.000 claims description 4
239000000010 aprotic solvent Substances 0.000 claims description 3
SBZXBUIDTXKZTM-UHFFFAOYSA-N diglyme Chemical group COCCOCCOC SBZXBUIDTXKZTM-UHFFFAOYSA-N 0.000 claims description 3
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
239000010425 asbestos Substances 0.000 claims description 2
238000000034 method Methods 0.000 claims description 2
239000002808 molecular sieve Substances 0.000 claims description 2
229910000480 nickel oxide Inorganic materials 0.000 claims description 2
GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 2
229910052895 riebeckite Inorganic materials 0.000 claims description 2
238000007142 ring opening reaction Methods 0.000 claims description 2
239000000741 silica gel Substances 0.000 claims description 2
229910002027 silica gel Inorganic materials 0.000 claims description 2
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 2
ZUHZGEOKBKGPSW-UHFFFAOYSA-N tetraglyme Chemical compound COCCOCCOCCOCCOC ZUHZGEOKBKGPSW-UHFFFAOYSA-N 0.000 claims description 2
YFNKIDBQEZZDLK-UHFFFAOYSA-N triglyme Chemical compound COCCOCCOCCOC YFNKIDBQEZZDLK-UHFFFAOYSA-N 0.000 claims 1
NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 12
239000003054 catalyst Substances 0.000 description 6
235000003270 potassium fluoride Nutrition 0.000 description 6
239000011698 potassium fluoride Substances 0.000 description 6
239000002994 raw material Substances 0.000 description 5
XJHCXCQVJFPJIK-UHFFFAOYSA-M caesium fluoride Chemical compound [F-].[Cs+] XJHCXCQVJFPJIK-UHFFFAOYSA-M 0.000 description 4
239000007789 gas Substances 0.000 description 4
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
239000012071 phase Substances 0.000 description 3
239000002904 solvent Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
235000011089 carbon dioxide Nutrition 0.000 description 2
239000007791 liquid phase Substances 0.000 description 2
239000000203 mixture Substances 0.000 description 2
PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 2
VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
VXZNUWALAXEDSJ-UHFFFAOYSA-N 3,3,3-trifluoropropanoyl fluoride Chemical compound FC(=O)CC(F)(F)F VXZNUWALAXEDSJ-UHFFFAOYSA-N 0.000 description 1
229910021583 Cobalt(III) fluoride Inorganic materials 0.000 description 1
KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
WAIPAZQMEIHHTJ-UHFFFAOYSA-N [Cr].[Co] Chemical compound [Cr].[Co] WAIPAZQMEIHHTJ-UHFFFAOYSA-N 0.000 description 1
239000003377 acid catalyst Substances 0.000 description 1
239000003905 agrochemical Substances 0.000 description 1
238000009835 boiling Methods 0.000 description 1
OEERIBPGRSLGEK-UHFFFAOYSA-N carbon dioxide;methanol Chemical compound OC.O=C=O OEERIBPGRSLGEK-UHFFFAOYSA-N 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
YCYBZKSMUPTWEE-UHFFFAOYSA-L cobalt(ii) fluoride Chemical compound F[Co]F YCYBZKSMUPTWEE-UHFFFAOYSA-L 0.000 description 1
238000001816 cooling Methods 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
229910001873 dinitrogen Inorganic materials 0.000 description 1
238000004821 distillation Methods 0.000 description 1
229940079593 drug Drugs 0.000 description 1
239000003814 drug Substances 0.000 description 1
-1 etc. Chemical compound 0.000 description 1
239000011737 fluorine Substances 0.000 description 1
229910052731 fluorine Inorganic materials 0.000 description 1
238000010574 gas phase reaction Methods 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
239000011968 lewis acid catalyst Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000000178 monomer Substances 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
RZWZRACFZGVKFM-UHFFFAOYSA-N propanoyl chloride Chemical compound CCC(Cl)=O RZWZRACFZGVKFM-UHFFFAOYSA-N 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000010992 reflux Methods 0.000 description 1
238000001577 simple distillation Methods 0.000 description 1
235000013024 sodium fluoride Nutrition 0.000 description 1
239000011775 sodium fluoride Substances 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1

Classifications

- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

Catalysts (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

JP58251070A 1983-12-26 1983-12-26 ２，２，３−トリフルオロプロピオニルフルオライドの製法 Granted JPS60136536A (ja)

Priority Applications (9)

Application Number	Priority Date	Filing Date	Title
JP58251070A JPS60136536A (ja)	1983-12-26	1983-12-26	２，２，３−トリフルオロプロピオニルフルオライドの製法
KR1019840008099A KR870002015B1 (ko)	1983-12-26	1984-12-19	2,2-디플루오로프로피온산 유도체의 제조방법
US06/684,344 US4719052A (en)	1983-12-26	1984-12-20	2,2-difluoropropionic acid derivatives
EP87113971A EP0258911B1 (de)	1983-12-26	1984-12-21	Verfahren zur Herstellung von 2,2,3-Trifluorpropionsäurefluorid
CA000470916A CA1293739C (en)	1983-12-26	1984-12-21	Process for preparing 2,2,3-trifluoropropionyl fluoride
DE8484116103T DE3482258D1 (de)	1983-12-26	1984-12-21	2,2-difluorpropionsaeurederivate und verfahren zu ihrer herstellung.
EP84116103A EP0148490B1 (de)	1983-12-26	1984-12-21	2,2-Difluorpropionsäurederivate und Verfahren zu ihrer Herstellung
DE8787113971T DE3483535D1 (de)	1983-12-26	1984-12-21	Verfahren zur herstellung von 2,2,3-trifluorpropionsaeurefluorid.
CA000616011A CA1318327C (en)	1983-12-26	1991-02-27	2,2-difluoropropionic acid derivatives

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP58251070A JPS60136536A (ja)	1983-12-26	1983-12-26	２，２，３−トリフルオロプロピオニルフルオライドの製法

Publications (2)

Publication Number	Publication Date
JPS60136536A JPS60136536A (ja)	1985-07-20
JPH0149340B2 true JPH0149340B2 (de)	1989-10-24

Family

ID=17217173

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP58251070A Granted JPS60136536A (ja)	1983-12-26	1983-12-26	２，２，３−トリフルオロプロピオニルフルオライドの製法

Country Status (1)

Country	Link
JP (1)	JPS60136536A (de)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7622547B2 (en)	2005-02-10	2009-11-24	Daicel Chemical Industries, Ltd.	Process and activated carbon catalyst for ring-opening polymerization of lactone compounds
US7851583B2 (en)	2005-02-10	2010-12-14	Daicel Chemical Industries, Ltd.	Process and activated carbon catalyst for ring-opening polymerization

1983
- 1983-12-26 JP JP58251070A patent/JPS60136536A/ja active Granted

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7622547B2 (en)	2005-02-10	2009-11-24	Daicel Chemical Industries, Ltd.	Process and activated carbon catalyst for ring-opening polymerization of lactone compounds
US7851583B2 (en)	2005-02-10	2010-12-14	Daicel Chemical Industries, Ltd.	Process and activated carbon catalyst for ring-opening polymerization

Also Published As

Publication number	Publication date
JPS60136536A (ja)	1985-07-20

Publication	Publication Date	Title
CA2166971C (en)	2005-09-27	Process for the preparation of 1,1,1,3,3-pentafluoropropane
EP0396974B1 (de)	1993-08-11	Verfahren zur Herstellung von Fluoralkylvinylverbindungen
EP0258911B1 (de)	1990-10-31	Verfahren zur Herstellung von 2,2,3-Trifluorpropionsäurefluorid
JP3248184B2 (ja)	2002-01-21	１，１，１，３，３‐ペンタフルオロプロパンの製造方法，及び１，１，１，３，３‐ペンタフルオロ‐２，３‐ジクロロプロパンの製造方法
JPS6346748B2 (de)	1988-09-19
JPH07106996B2 (ja)	1995-11-15	飽和した、ふつ素を含有するが塩素を含有しない炭化水素の製造方法
JPH04211027A (ja)	1992-08-03	１，１，１，３，３，３−ヘキサフルオロプロパン及び２−クロロ−１，１，１，３，３，３−ヘキサフルオロプロパンの製造方法
EP0004636B1 (de)	1982-07-07	Verfahren zur Darstellung von Benzotrifluorid und seinen Derivaten
EP0074069B1 (de)	1986-01-08	Verfahren zur Herstellung von Chlortrifluormethylbenzol
US5728902A (en)	1998-03-17	Method for manufacturing 1,1,1,3,3-pentafluoropropene
CA2094892A1 (en)	1993-10-30	Process for the preparation of hexafluorobutane, and intermediates thereby obtainable
US3433838A (en)	1969-03-18	Purification of perhaloacetones
JPH0149340B2 (de)	1989-10-24
EP0815066A1 (de)	1998-01-07	Zwischenprodukte für die synthese von trifluormethylierten organische verbindungen
EP0408004A1 (de)	1991-01-16	Verfahren zur Herstellung von 1,2-Dichlor-1,1,2-Trifluorethan
US3265740A (en)	1966-08-09	Process for chlorinating acetone and acetylacetone
US5449842A (en)	1995-09-12	Gas phase process for the production of 1,1-dichloro-1-fluoroethane and/or 1-chloro-1,1-difluoroethane from vinylidene chloride
US5629458A (en)	1997-05-13	Process for the preparation of 2 2 2 trifluoroethanol
JPWO1993016973A1 (ja)	1994-03-03	１，１，１，２，２，４，４，５，５，５‐デカフルオロペンタンの製造方法及びその製造用中間体
JPH09169687A (ja)	1997-06-30	イソホロンの製造方法
EP0421322B1 (de)	1994-01-05	Verfahren zur Herstellung von Pentafluordichlorpropanen
JPH021819B2 (de)	1990-01-12
RU2134257C1 (ru)	1999-08-10	Способ гидрофторирования фторолефинов
JPH0688919B2 (ja)	1994-11-09	含水素フルオロクロロアルカンの製造方法
JPH10287609A (ja)	1998-10-27	３，３−ジクロロ−１，１，１−トリフルオロアセトンの製造方法

JPH0149340B2 - - Google Patents

Info

Links

Classifications

Landscapes

Priority Applications (9)

Applications Claiming Priority (1)

Publications (2)

Family

ID=17217173

Family Applications (1)

Country Status (1)

Cited By (2)

Cited By (2)

Also Published As

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