JPH11295833A - 減少された厚さ生長及び改良された均質性を有する塩化銀に富む平板状粒子を製造するための方法 - Google Patents

減少された厚さ生長及び改良された均質性を有する塩化銀に富む平板状粒子を製造するための方法

Info

Publication number: JPH11295833A
Authority: JP; Japan
Prior art keywords: silver; formula; grains; alkyl; tabular grains
Prior art date: 1998-01-27
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Pending

Application number

JP11013842A

Other languages

English (en)

Japanese (ja)

Inventor

Peter Verrept

ペテル・ヴェレプ

Ann Verbeeck

アン・ヴェルビーク

Nadia Vermant

ナディア・ヴェルマン

Frank Louwet

フランク・ルエ

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Agfa Gevaert NV

Original Assignee

Agfa Gevaert NV

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-01-27

Filing date

1999-01-22

Publication date

1999-10-29

1999-01-22 Application filed by Agfa Gevaert NV filed Critical Agfa Gevaert NV

1999-10-29 Publication of JPH11295833A publication Critical patent/JPH11295833A/ja

Status Pending legal-status Critical Current

Links

229910021607 Silver chloride Inorganic materials 0.000 title claims abstract description 28
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 title claims abstract description 28
238000004519 manufacturing process Methods 0.000 title claims description 13
230000001976 improved effect Effects 0.000 title description 4
-1 halide ions Chemical class 0.000 claims abstract description 69
229910052709 silver Inorganic materials 0.000 claims abstract description 64
239000004332 silver Substances 0.000 claims abstract description 64
239000013078 crystal Substances 0.000 claims abstract description 53
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims abstract description 38
125000000217 alkyl group Chemical group 0.000 claims abstract description 26
229920001400 block copolymer Polymers 0.000 claims abstract description 25
238000001556 precipitation Methods 0.000 claims abstract description 22
229910001961 silver nitrate Inorganic materials 0.000 claims abstract description 19
NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 13
125000002560 nitrile group Chemical group 0.000 claims abstract description 7
229910052760 oxygen Inorganic materials 0.000 claims abstract description 7
239000000839 emulsion Substances 0.000 claims description 82
108010010803 Gelatin Proteins 0.000 claims description 36
229920000159 gelatin Polymers 0.000 claims description 36
235000019322 gelatine Nutrition 0.000 claims description 36
235000011852 gelatine desserts Nutrition 0.000 claims description 36
239000008273 gelatin Substances 0.000 claims description 35
238000000034 method Methods 0.000 claims description 32
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 28
229910052739 hydrogen Inorganic materials 0.000 claims description 24
239000001257 hydrogen Substances 0.000 claims description 24
238000006243 chemical reaction Methods 0.000 claims description 23
239000000463 material Substances 0.000 claims description 20
125000000547 substituted alkyl group Chemical group 0.000 claims description 19
CCEOFEYFQLJLPV-UHFFFAOYSA-N C(=C)C(=N)N.C(C=C)(=O)N Chemical compound C(=C)C(=N)N.C(C=C)(=O)N CCEOFEYFQLJLPV-UHFFFAOYSA-N 0.000 claims description 18
150000001875 compounds Chemical class 0.000 claims description 18
150000003839 salts Chemical class 0.000 claims description 17
230000002378 acidificating effect Effects 0.000 claims description 15
HOLVRJRSWZOAJU-UHFFFAOYSA-N [Ag].ICl Chemical compound [Ag].ICl HOLVRJRSWZOAJU-UHFFFAOYSA-N 0.000 claims description 13
239000007864 aqueous solution Substances 0.000 claims description 11
239000003607 modifier Substances 0.000 claims description 11
239000002612 dispersion medium Substances 0.000 claims description 10
230000008569 process Effects 0.000 claims description 8
125000003118 aryl group Chemical group 0.000 claims description 7
SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 claims description 6
125000003107 substituted aryl group Chemical group 0.000 claims description 5
229910052799 carbon Inorganic materials 0.000 claims description 4
125000004432 carbon atom Chemical group C* 0.000 claims description 4
125000005647 linker group Chemical group 0.000 claims description 4
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 4
UVDYBBRVDUKNFV-UHFFFAOYSA-N 2-(prop-2-enoylamino)ethanesulfonic acid Chemical group OS(=O)(=O)CCNC(=O)C=C UVDYBBRVDUKNFV-UHFFFAOYSA-N 0.000 claims description 2
125000004435 hydrogen atom Chemical class [H]* 0.000 claims 11
IGPLBQCRFFZZOG-UHFFFAOYSA-N 2-(1-aminoprop-2-enylideneamino)ethanesulfonic acid Chemical group C=CC(N)=NCCS(O)(=O)=O IGPLBQCRFFZZOG-UHFFFAOYSA-N 0.000 claims 1
101100386054 Saccharomyces cerevisiae (strain ATCC 204508 / S288c) CYS3 gene Proteins 0.000 claims 1
101150035983 str1 gene Proteins 0.000 claims 1
HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 abstract description 6
241000276425 Xiphophorus maculatus Species 0.000 abstract 2
239000000243 solution Substances 0.000 description 55
239000010410 layer Substances 0.000 description 40
239000000975 dye Substances 0.000 description 26
229920000642 polymer Polymers 0.000 description 20
NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 20
XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 19
230000006911 nucleation Effects 0.000 description 19
238000010899 nucleation Methods 0.000 description 19
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 15
238000009826 distribution Methods 0.000 description 13
239000003795 chemical substances by application Substances 0.000 description 11
230000005070 ripening Effects 0.000 description 11
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239000000203 mixture Substances 0.000 description 9
238000011160 research Methods 0.000 description 9
229930024421 Adenine Natural products 0.000 description 8
GFFGJBXGBJISGV-UHFFFAOYSA-N Adenine Chemical compound NC1=NC=NC2=C1N=CN2 GFFGJBXGBJISGV-UHFFFAOYSA-N 0.000 description 8
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
229960000643 adenine Drugs 0.000 description 8
239000002585 base Substances 0.000 description 8
239000000084 colloidal system Substances 0.000 description 8
150000002431 hydrogen Chemical class 0.000 description 8
238000003384 imaging method Methods 0.000 description 7
238000012545 processing Methods 0.000 description 7
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 7
239000000126 substance Substances 0.000 description 7
150000001252 acrylic acid derivatives Chemical class 0.000 description 6
239000011248 coating agent Substances 0.000 description 6
238000000576 coating method Methods 0.000 description 6
XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 description 6
239000002245 particle Substances 0.000 description 6
230000035945 sensitivity Effects 0.000 description 6
FVAUCKIRQBBSSJ-UHFFFAOYSA-M sodium iodide Chemical compound [Na+].[I-] FVAUCKIRQBBSSJ-UHFFFAOYSA-M 0.000 description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
QGKMIGUHVLGJBR-UHFFFAOYSA-M (4z)-1-(3-methylbutyl)-4-[[1-(3-methylbutyl)quinolin-1-ium-4-yl]methylidene]quinoline;iodide Chemical compound [I-].C12=CC=CC=C2N(CCC(C)C)C=CC1=CC1=CC=[N+](CCC(C)C)C2=CC=CC=C12 QGKMIGUHVLGJBR-UHFFFAOYSA-M 0.000 description 5
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 5
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
229910021612 Silver iodide Inorganic materials 0.000 description 5
239000006224 matting agent Substances 0.000 description 5
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
238000002360 preparation method Methods 0.000 description 5
230000001681 protective effect Effects 0.000 description 5
230000001235 sensitizing effect Effects 0.000 description 5
229940045105 silver iodide Drugs 0.000 description 5
239000003381 stabilizer Substances 0.000 description 5
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 4
239000005977 Ethylene Substances 0.000 description 4
206010070834 Sensitisation Diseases 0.000 description 4
239000011230 binding agent Substances 0.000 description 4
150000003841 chloride salts Chemical class 0.000 description 4
239000006185 dispersion Substances 0.000 description 4
229940006461 iodide ion Drugs 0.000 description 4
DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 4
229920001983 poloxamer Polymers 0.000 description 4
239000004848 polyfunctional curative Substances 0.000 description 4
230000008313 sensitization Effects 0.000 description 4
239000010944 silver (metal) Substances 0.000 description 4
239000011780 sodium chloride Substances 0.000 description 4
125000001424 substituent group Chemical group 0.000 description 4
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 3
DRSHXJFUUPIBHX-UHFFFAOYSA-N COc1ccc(cc1)N1N=CC2C=NC(Nc3cc(OC)c(OC)c(OCCCN4CCN(C)CC4)c3)=NC12 Chemical compound COc1ccc(cc1)N1N=CC2C=NC(Nc3cc(OC)c(OC)c(OCCCN4CCN(C)CC4)c3)=NC12 DRSHXJFUUPIBHX-UHFFFAOYSA-N 0.000 description 3
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 3
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
239000002253 acid Substances 0.000 description 3
239000003513 alkali Substances 0.000 description 3
150000001409 amidines Chemical class 0.000 description 3
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238000001493 electron microscopy Methods 0.000 description 3
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PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 3
229910052737 gold Inorganic materials 0.000 description 3
239000010931 gold Substances 0.000 description 3
150000004820 halides Chemical class 0.000 description 3
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150000004694 iodide salts Chemical class 0.000 description 3
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AXPUQAAUHKSVKR-UHFFFAOYSA-N prop-2-enimidamide Chemical compound NC(=N)C=C AXPUQAAUHKSVKR-UHFFFAOYSA-N 0.000 description 3
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241001479434 Agfa Species 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
ZRALSGWEFCBTJO-UHFFFAOYSA-N Guanidine Chemical compound NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 description 2
FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 description 2
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
229910002651 NO3 Inorganic materials 0.000 description 2
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 2
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150000001299 aldehydes Chemical class 0.000 description 2
LEQAOMBKQFMDFZ-UHFFFAOYSA-N alpha-ketodiacetal Natural products O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
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BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
235000021240 caseins Nutrition 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
125000002091 cationic group Chemical group 0.000 description 1
239000001913 cellulose Substances 0.000 description 1
229920002678 cellulose Polymers 0.000 description 1
230000008859 change Effects 0.000 description 1
239000008119 colloidal silica Substances 0.000 description 1
238000004132 cross linking Methods 0.000 description 1
238000000502 dialysis Methods 0.000 description 1
150000001991 dicarboxylic acids Chemical class 0.000 description 1
238000009792 diffusion process Methods 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
SWSQBOPZIKWTGO-UHFFFAOYSA-N dimethylaminoamidine Natural products CN(C)C(N)=N SWSQBOPZIKWTGO-UHFFFAOYSA-N 0.000 description 1
AILJBODFYLXZLU-UHFFFAOYSA-H dioxido-oxo-selanylidene-lambda6-sulfane gold(3+) Chemical compound [Au+3].[Au+3].[O-]S([O-])(=O)=[Se].[O-]S([O-])(=O)=[Se].[O-]S([O-])(=O)=[Se] AILJBODFYLXZLU-UHFFFAOYSA-H 0.000 description 1
ADPOBOOHCUVXGO-UHFFFAOYSA-H dioxido-oxo-sulfanylidene-$l^{6}-sulfane;gold(3+) Chemical compound [Au+3].[Au+3].[O-]S([O-])(=O)=S.[O-]S([O-])(=O)=S.[O-]S([O-])(=O)=S ADPOBOOHCUVXGO-UHFFFAOYSA-H 0.000 description 1
AFOSIXZFDONLBT-UHFFFAOYSA-N divinyl sulfone Chemical compound C=CS(=O)(=O)C=C AFOSIXZFDONLBT-UHFFFAOYSA-N 0.000 description 1
238000005868 electrolysis reaction Methods 0.000 description 1
150000002118 epoxides Chemical class 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000000835 fiber Substances 0.000 description 1
239000010946 fine silver Substances 0.000 description 1
238000005189 flocculation Methods 0.000 description 1
230000016615 flocculation Effects 0.000 description 1
125000000524 functional group Chemical group 0.000 description 1
229940083124 ganglion-blocking antiadrenergic secondary and tertiary amines Drugs 0.000 description 1
125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 1
229940015043 glyoxal Drugs 0.000 description 1
239000001046 green dye Substances 0.000 description 1
150000002366 halogen compounds Chemical class 0.000 description 1
125000005843 halogen group Chemical group 0.000 description 1
125000000623 heterocyclic group Chemical group 0.000 description 1
150000002429 hydrazines Chemical class 0.000 description 1
ZMZDMBWJUHKJPS-UHFFFAOYSA-N hydrogen thiocyanate Natural products SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 description 1
230000002209 hydrophobic effect Effects 0.000 description 1
125000004356 hydroxy functional group Chemical group O* 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
125000002768 hydroxyalkyl group Chemical group 0.000 description 1
150000002466 imines Chemical class 0.000 description 1
239000003112 inhibitor Substances 0.000 description 1
229910001503 inorganic bromide Inorganic materials 0.000 description 1
229910001505 inorganic iodide Inorganic materials 0.000 description 1
229910017053 inorganic salt Inorganic materials 0.000 description 1
239000011229 interlayer Substances 0.000 description 1
JDNTWHVOXJZDSN-UHFFFAOYSA-N iodoacetic acid Chemical compound OC(=O)CI JDNTWHVOXJZDSN-UHFFFAOYSA-N 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
150000003951 lactams Chemical class 0.000 description 1
150000002596 lactones Chemical class 0.000 description 1
230000031700 light absorption Effects 0.000 description 1
239000000314 lubricant Substances 0.000 description 1
229910021645 metal ion Inorganic materials 0.000 description 1
WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
150000005054 naphthyridines Chemical class 0.000 description 1
230000003472 neutralizing effect Effects 0.000 description 1
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
125000000018 nitroso group Chemical group N(=O)* 0.000 description 1
229910000510 noble metal Inorganic materials 0.000 description 1
JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
239000003605 opacifier Substances 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
AICOOMRHRUFYCM-ZRRPKQBOSA-N oxazine, 1 Chemical compound C([C@@H]1[C@H](C(C[C@]2(C)[C@@H]([C@H](C)N(C)C)[C@H](O)C[C@]21C)=O)CC1=CC2)C[C@H]1[C@@]1(C)[C@H]2N=C(C(C)C)OC1 AICOOMRHRUFYCM-ZRRPKQBOSA-N 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
QUBQYFYWUJJAAK-UHFFFAOYSA-N oxymethurea Chemical compound OCNC(=O)NCO QUBQYFYWUJJAAK-UHFFFAOYSA-N 0.000 description 1
229950005308 oxymethurea Drugs 0.000 description 1
229910052763 palladium Inorganic materials 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
CMCWWLVWPDLCRM-UHFFFAOYSA-N phenidone Chemical compound N1C(=O)CCN1C1=CC=CC=C1 CMCWWLVWPDLCRM-UHFFFAOYSA-N 0.000 description 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
239000010452 phosphate Substances 0.000 description 1
125000000612 phthaloyl group Chemical group C(C=1C(C(=O)*)=CC=CC1)(=O)* 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
229910052697 platinum Inorganic materials 0.000 description 1
229920003214 poly(methacrylonitrile) Polymers 0.000 description 1
229920002451 polyvinyl alcohol Polymers 0.000 description 1
229940068984 polyvinyl alcohol Drugs 0.000 description 1
229920001592 potato starch Polymers 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
239000000047 product Substances 0.000 description 1
235000018102 proteins Nutrition 0.000 description 1
108090000623 proteins and genes Proteins 0.000 description 1
102000004169 proteins and genes Human genes 0.000 description 1
UGZVCHWAXABBHR-UHFFFAOYSA-O pyridin-1-ium-1-carboxamide Chemical class NC(=O)[N+]1=CC=CC=C1 UGZVCHWAXABBHR-UHFFFAOYSA-O 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
239000001044 red dye Substances 0.000 description 1
238000012552 review Methods 0.000 description 1
PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 description 1
239000012487 rinsing solution Substances 0.000 description 1
CRDYSYOERSZTHZ-UHFFFAOYSA-M selenocyanate Chemical compound [Se-]C#N CRDYSYOERSZTHZ-UHFFFAOYSA-M 0.000 description 1
IYKVLICPFCEZOF-UHFFFAOYSA-N selenourea Chemical compound NC(N)=[Se] IYKVLICPFCEZOF-UHFFFAOYSA-N 0.000 description 1
239000004065 semiconductor Substances 0.000 description 1
150000004756 silanes Chemical class 0.000 description 1
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
239000002904 solvent Substances 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
125000005504 styryl group Chemical group 0.000 description 1
125000004964 sulfoalkyl group Chemical group 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
DHCDFWKWKRSZHF-UHFFFAOYSA-N sulfurothioic S-acid Chemical compound OS(O)(=O)=S DHCDFWKWKRSZHF-UHFFFAOYSA-N 0.000 description 1
JJJPTTANZGDADF-UHFFFAOYSA-N thiadiazole-4-thiol Chemical compound SC1=CSN=N1 JJJPTTANZGDADF-UHFFFAOYSA-N 0.000 description 1
150000003606 tin compounds Chemical class 0.000 description 1
239000004408 titanium dioxide Substances 0.000 description 1
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
230000009466 transformation Effects 0.000 description 1
230000001131 transforming effect Effects 0.000 description 1
WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
229910052721 tungsten Inorganic materials 0.000 description 1
239000010937 tungsten Substances 0.000 description 1
229920001567 vinyl ester resin Polymers 0.000 description 1
229920003170 water-soluble synthetic polymer Polymers 0.000 description 1
239000005019 zein Substances 0.000 description 1
229940093612 zein Drugs 0.000 description 1

Classifications

- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/0051—Tabular grain emulsions
- G03C1/0053—Tabular grain emulsions with high content of silver chloride
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/06—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
- G03C1/07—Substances influencing grain growth during silver salt formation
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/0357—Monodisperse emulsion
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/03594—Size of the grains
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/03—111 crystal face
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/47—Polymer
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C5/00—Photographic processes or agents therefor; Regeneration of such processing agents
- G03C5/16—X-ray, infrared, or ultraviolet ray processes

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Physics & Mathematics (AREA)
General Physics & Mathematics (AREA)
Silver Salt Photography Or Processing Solution Therefor (AREA)

JP11013842A 1998-01-27 1999-01-22 減少された厚さ生長及び改良された均質性を有する塩化銀に富む平板状粒子を製造するための方法 Pending JPH11295833A (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
EP98200236.2		1998-01-27
EP98200236A EP0932076B1 (fr)	1998-01-27	1998-01-27	Procédé pour la préparation des grains tabulaires riches en chlorure d'argent avec croissance en épaisseur réduite et homogénéité améliorée

Publications (1)

Publication Number	Publication Date
JPH11295833A true JPH11295833A (ja)	1999-10-29

Family

ID=8233328

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP11013842A Pending JPH11295833A (ja)	1998-01-27	1999-01-22	減少された厚さ生長及び改良された均質性を有する塩化銀に富む平板状粒子を製造するための方法

Country Status (3)

Country	Link
EP (1)	EP0932076B1 (fr)
JP (1)	JPH11295833A (fr)
DE (1)	DE69817316D1 (fr)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5252442A (en) *	1991-05-14	1993-10-12	Eastman Kodak Company	Radiographic elements with improved detective quantum efficiencies
US5252453A (en) *	1992-11-04	1993-10-12	Eastman Kodak Company	Process for accelerating the precipitation of a low coefficient of variation emulsion
US5733716A (en) *	1995-08-16	1998-03-31	Konica Corporation	Silver halide photographic light sensitive material

1998
- 1998-01-27 EP EP98200236A patent/EP0932076B1/fr not_active Expired - Lifetime
- 1998-01-27 DE DE69817316T patent/DE69817316D1/de not_active Expired - Lifetime
1999
- 1999-01-22 JP JP11013842A patent/JPH11295833A/ja active Pending

Also Published As

Publication number	Publication date
DE69817316D1 (de)	2003-09-25
EP0932076A1 (fr)	1999-07-28
EP0932076B1 (fr)	2003-08-20

Publication	Publication Date	Title
JPH05181219A (ja)	1993-07-23	高塩化物平板状粒子乳剤の改良製造方法
JPH0573209B2 (fr)	1993-10-13
JP2835636B2 (ja)	1998-12-14	感光性ハロゲン化銀乳剤の製造方法
JPH04318544A (ja)	1992-11-10	溶解物理現像包含処理用ハロゲン化銀乳剤
JP3597536B2 (ja)	2004-12-08	感度の高い写真乳剤
JPH0789200B2 (ja)	1995-09-27	ハロゲン化銀乳剤の製造方法
JP3170525B2 (ja)	2001-05-28	塩化物含量の高い平板状乳剤粒子の製造法
JP2000321696A (ja)	2000-11-24	乳剤調製方法
US6162599A (en)	2000-12-19	Photosensitive image-forming element containing silver halide crystals which are internally modified with a metal ligand complex forming deep electron traps
JP2791492B2 (ja)	1998-08-27	画像形成方法
JPH11295833A (ja)	1999-10-29	減少された厚さ生長及び改良された均質性を有する塩化銀に富む平板状粒子を製造するための方法
US6010840A (en)	2000-01-04	Method for preparing tabular grains rich in silver chloride with reduced thickness growth and improved homogeneity
JPS6342769B2 (fr)	1988-08-25
JPH11223894A (ja)	1999-08-17	臭化銀に富む形態学的に均一な｛１１１｝平板状結晶の製造法
JPH0561205B2 (fr)	1993-09-03
JPH0876303A (ja)	1996-03-22	ハロゲン化銀写真感光材料及びその処理方法
JPH0254534B2 (fr)	1990-11-21
JPH07507646A (ja)	1995-08-24	平板状粒子の製造方法
US6316176B1 (en)	2001-11-13	Photosensitive silver halide element comprising chemically sensitized emulsion grains and method to prepare them
JPH07113738B2 (ja)	1995-12-06	経時カブリ等の少ない改良されたハロゲン化銀写真感光材料
JP2001056519A (ja)	2001-02-27	化学増感乳剤粒子を含む感光性ハロゲン化銀材料及びその製造方法
JP2709799B2 (ja)	1998-02-04	ハロゲン化銀乳剤の製造方法
JPH06301131A (ja)	1994-10-28	オリゴマー改質された平板状粒子乳剤
JP2907964B2 (ja)	1999-06-21	高感度で現像性が良好なハロゲン化銀乳剤
JPH0431378B2 (fr)	1992-05-26