LT3732B - Process for preparing crystalline sucralose - Google Patents

Process for preparing crystalline sucralose Download PDF

Info

Publication number: LT3732B
Authority: LT; Lithuania
Prior art keywords: particle size; sucralose; microns; size; crystalline
Prior art date: 1986-07-15

Application number

LTIP1431A

Other languages

English (en)

Lithuanian (lt)

Inventor

Graham Jackson

Michael Ralph Jenner

Original Assignee

Tate & Lyle Plc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1986-07-15

Filing date

1993-10-28

Publication date

1996-02-26

1993-10-28 Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc

1995-05-25 Publication of LTIP1431A publication Critical patent/LTIP1431A/xx

1996-02-26 Publication of LT3732B publication Critical patent/LT3732B/lt

Links

239000004376 Sucralose Substances 0.000 title claims abstract description 27
BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 title claims abstract description 27
235000019408 sucralose Nutrition 0.000 title claims abstract description 27
238000004519 manufacturing process Methods 0.000 title description 2
238000000034 method Methods 0.000 claims abstract description 7
239000013078 crystal Substances 0.000 claims description 9
238000002425 crystallisation Methods 0.000 claims description 8
230000008025 crystallization Effects 0.000 claims description 8
239000002904 solvent Substances 0.000 claims description 4
238000002360 preparation method Methods 0.000 claims 1
239000002245 particle Substances 0.000 abstract description 31
238000009826 distribution Methods 0.000 abstract description 3
230000002708 enhancing effect Effects 0.000 abstract 1
238000010902 jet-milling Methods 0.000 abstract 1
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
239000000463 material Substances 0.000 description 8
239000010419 fine particle Substances 0.000 description 3
239000012530 fluid Substances 0.000 description 3
239000007864 aqueous solution Substances 0.000 description 2
238000002845 discoloration Methods 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000000126 substance Substances 0.000 description 2
235000000346 sugar Nutrition 0.000 description 2
229930006000 Sucrose Natural products 0.000 description 1
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
235000013361 beverage Nutrition 0.000 description 1
238000005422 blasting Methods 0.000 description 1
150000001720 carbohydrates Chemical class 0.000 description 1
235000014633 carbohydrates Nutrition 0.000 description 1
125000001309 chloro group Chemical group Cl* 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000001816 cooling Methods 0.000 description 1
239000002178 crystalline material Substances 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
238000011010 flushing procedure Methods 0.000 description 1
235000013305 food Nutrition 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
238000003801 milling Methods 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
238000000053 physical method Methods 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000007787 solid Substances 0.000 description 1
238000000859 sublimation Methods 0.000 description 1
230000008022 sublimation Effects 0.000 description 1
239000005720 sucrose Substances 0.000 description 1
150000008163 sugars Chemical class 0.000 description 1
239000006188 syrup Substances 0.000 description 1
235000020357 syrup Nutrition 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A23L27/33—Artificial sweetening agents containing sugars or derivatives
- A23L27/37—Halogenated sugars

Landscapes

Life Sciences & Earth Sciences (AREA)
Proteomics, Peptides & Aminoacids (AREA)
Health & Medical Sciences (AREA)
Nutrition Science (AREA)
Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Food Science & Technology (AREA)
Polymers & Plastics (AREA)
Seasonings (AREA)
Saccharide Compounds (AREA)
Enzymes And Modification Thereof (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

LTIP1431A 1986-07-15 1993-10-28 Process for preparing crystalline sucralose LT3732B (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GB868617222A GB8617222D0 (en)	1986-07-15	1986-07-15	Sweetener

Publications (2)

Publication Number	Publication Date
LTIP1431A LTIP1431A (en)	1995-05-25
LT3732B true LT3732B (en)	1996-02-26

Family

ID=10601082

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LTIP1431A LT3732B (en)	1986-07-15	1993-10-28	Process for preparing crystalline sucralose

Country Status (27)

Country	Link
US (1)	US4918182A (de)
EP (1)	EP0255260B1 (de)
JP (1)	JP2562147B2 (de)
KR (1)	KR950008268B1 (de)
AR (1)	AR241570A1 (de)
AT (1)	ATE52005T1 (de)
AU (1)	AU591998B2 (de)
CA (1)	CA1290329C (de)
DE (1)	DE3762303D1 (de)
DK (1)	DK173232B1 (de)
ES (1)	ES2016362B3 (de)
FI (1)	FI85145C (de)
GB (2)	GB8617222D0 (de)
GE (1)	GEP19960447B (de)
GR (1)	GR3000441T3 (de)
IE (1)	IE60432B1 (de)
IL (1)	IL83188A (de)
LT (1)	LT3732B (de)
LV (1)	LV5197A3 (de)
MD (1)	MD108C2 (de)
MX (1)	MX7362A (de)
NO (1)	NO172164C (de)
NZ (1)	NZ221063A (de)
PH (1)	PH24116A (de)
RU (1)	RU1825318C (de)
UA (1)	UA18713A1 (de)
ZA (1)	ZA875121B (de)

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GB8627139D0 (en) *	1986-11-13	1986-12-10	Tate & Lyle Plc	Sweetening composition
US4971797A (en) *	1988-12-22	1990-11-20	Warner-Lambert Company	Stabilized sucralose complex
US5225536A (en) *	1989-08-16	1993-07-06	Sadao Nishibori	Particles of gelatin and amino acid to be blended in resins
FI96041C (fi) *	1993-03-19	1996-04-25	Sucros Oy	Makeutusaine, menetelmä sen valmistamiseksi ja sen käyttö
FI95147C (fi) *	1993-03-19	1995-12-27	Sucros Oy	Menetelmä sokerituotteen valmistamiseksi ja menetelmällä valmistetun tuotteen käyttö
US5498709A (en) *	1994-10-17	1996-03-12	Mcneil-Ppc, Inc.	Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
GB9517281D0 (en) *	1995-08-23	1995-10-25	Tate & Lyle Plc	Solid sucralose
US7588793B1 (en)	1998-06-05	2009-09-15	Cadbury Adams Usa, Llc	Enhanced flavoring compositions containing N-ethyl-p-menthane-3-carboxamide and method of making and using same
EP2277393B1 (de)	1999-04-16	2012-12-12	San-Ei Gen F.F.I., Inc.	Zusammensetzung enthaltend Sucralose
US20020004749A1 (en) *	2000-02-09	2002-01-10	Froseth Barrie R.	Customized food selection, ordering and distribution system and method
US7041277B2 (en) *	2000-03-10	2006-05-09	Cadbury Adams Usa Llc	Chewing gum and confectionery compositions with encapsulated stain removing agent compositions, and methods of making and using the same
AU3955002A (en)	2000-11-17	2002-06-03	Mcneil Ppc Inc	Meltable form of sucralose
EP1339728B1 (de)	2000-11-17	2013-02-27	Tate & Lyle Technology Limited	Verbesserte sucralose enthaltende zusammensetzung und verfahren zur kristallisation von sucralose
US20030012853A1 (en) *	2001-02-28	2003-01-16	Jensen Michael Laurence	Sweet and salty microwave popcorn compositions; arrangements and method
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US6890581B2 (en) *	2002-04-05	2005-05-10	Tate & Lyle Public Limited Company	Methods for buffer stabilized aqueous deacylation
US7445769B2 (en)	2002-10-31	2008-11-04	Cadbury Adams Usa Llc	Compositions for removing stains from dental surfaces and methods of making and using the same
US6943248B2 (en)	2003-04-30	2005-09-13	Tate & Lyle Public Limited Company	Crystalline form of sucralose, and method for producing it
US7390518B2 (en)	2003-07-11	2008-06-24	Cadbury Adams Usa, Llc	Stain removing chewing gum composition
US20080317681A1 (en) *	2003-07-11	2008-12-25	Petros Gebreselassie	Compositions containing a stain removing complex, and methods of making and using the same
US8591973B2 (en)	2005-05-23	2013-11-26	Kraft Foods Global Brands Llc	Delivery system for active components and a material having preselected hydrophobicity as part of an edible composition
US20050112236A1 (en) *	2003-11-21	2005-05-26	Navroz Boghani	Delivery system for active components as part of an edible composition having preselected tensile strength
US8591972B2 (en) *	2005-05-23	2013-11-26	Kraft Foods Global Brands Llc	Delivery system for coated active components as part of an edible composition
US9271904B2 (en) *	2003-11-21	2016-03-01	Intercontinental Great Brands Llc	Controlled release oral delivery systems
US20060263473A1 (en) *	2005-05-23	2006-11-23	Cadbury Adams Usa Llc	Compressed delivery system for active components as part of an edible composition
US8591968B2 (en) *	2005-05-23	2013-11-26	Kraft Foods Global Brands Llc	Edible composition including a delivery system for active components
US8389032B2 (en)	2005-05-23	2013-03-05	Kraft Foods Global Brands Llc	Delivery system for active components as part of an edible composition having selected particle size
US8591974B2 (en)	2003-11-21	2013-11-26	Kraft Foods Global Brands Llc	Delivery system for two or more active components as part of an edible composition
US20060263474A1 (en) *	2005-05-23	2006-11-23	Cadbury Adams Usa Llc.	Enhanced flavor-release comestible compositions and methods for same
US8597703B2 (en)	2005-05-23	2013-12-03	Kraft Foods Global Brands Llc	Delivery system for active components as part of an edible composition including a ratio of encapsulating material and active component
US8389031B2 (en) *	2005-05-23	2013-03-05	Kraft Foods Global Brands Llc	Coated delivery system for active components as part of an edible composition
EA200601742A1 (ru) *	2004-03-19	2007-02-27	Фармед Медикэр Прайвит Лимитед	Усовершенствованный способ производства хлорированной сахарозы
US20060024245A1 (en) *	2004-07-29	2006-02-02	Cadbury Adams, Llc.	Tooth whitening compositions and delivery systems therefor
US7641892B2 (en)	2004-07-29	2010-01-05	Cadburry Adams USA, LLC	Tooth whitening compositions and delivery systems therefor
CA2576375C (en)	2004-08-11	2010-12-21	Cadbury Adams Usa Llc	Sensate compositions and delivery systems therefor
US20060068058A1 (en) *	2004-09-30	2006-03-30	Cadbury Adams Usa Llc	Thermally stable, high tensile strength encapsulation compositions for actives
US7955630B2 (en) *	2004-09-30	2011-06-07	Kraft Foods Global Brands Llc	Thermally stable, high tensile strength encapsulated actives
US20060068059A1 (en) *	2004-09-30	2006-03-30	Cadbury Adams Usa Llc	Encapsulated compositions and methods of preparation
US20060280837A1 (en) *	2004-08-25	2006-12-14	Cadbury Adams Usa Llc.	Multi-modality sensations in chewing gum compositions
US20080063747A1 (en) *	2004-08-25	2008-03-13	Cadbury Adams Usa Llc	Dusting compositions for chewing gum products
US7727565B2 (en)	2004-08-25	2010-06-01	Cadbury Adams Usa Llc	Liquid-filled chewing gum composition
US20070020330A1 (en) *	2004-11-24	2007-01-25	Medpointe Healthcare Inc.	Compositions comprising azelastine and methods of use thereof
US8758816B2 (en) *	2004-11-24	2014-06-24	Meda Pharmaceuticals Inc.	Compositions comprising azelastine and methods of use thereof
EP2522365B1 (de)	2004-11-24	2016-10-26	Meda Pharmaceuticals Inc.	Zusammensetzungen aus Azelastin und Verwendungsverfahren dafür
US9198448B2 (en) *	2005-02-07	2015-12-01	Intercontinental Great Brands Llc	Stable tooth whitening gum with reactive ingredients
US7851005B2 (en) *	2005-05-23	2010-12-14	Cadbury Adams Usa Llc	Taste potentiator compositions and beverages containing same
US7851006B2 (en) *	2005-05-23	2010-12-14	Cadbury Adams Usa Llc	Taste potentiator compositions and beverages containing same
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US20060276639A1 (en) *	2005-06-01	2006-12-07	Healthy Brands, Llc	Conversion of sucralose-6-ester to sucralose
US20070053972A1 (en) *	2005-09-08	2007-03-08	Cadbury Adams Usa Llc.	Gelatin capsules containing actives
US20070221236A1 (en) *	2005-10-05	2007-09-27	Cadbury Adams Usa Llc.	Cooling compositions including menthyl esters
CN101346073B (zh) *	2005-12-23	2013-02-13	卡夫食品环球品牌有限责任公司	提供基本上类似于由薄荷醇提供的感觉的组合物
EP1973422B1 (de)	2005-12-23	2014-06-11	Intercontinental Great Brands LLC	Zusammensetzungen für die orale oder dermale abgabe, die ein wärmegefühl vermitteln
US20070178187A1 (en) *	2006-01-27	2007-08-02	Cadbury Adams Usa Llc	Chewing gum compositions including free neotame sweetener compositions
US20070178188A1 (en) *	2006-01-27	2007-08-02	Cadbury Adams Usa Llc	Chewing gum compositions including free neotame sweetener compositions
CA2647148A1 (en) *	2006-03-22	2008-01-31	V.B. Medicare Pvt. Ltd.	Novel crystallization methods and novel crystalline and amorphous forms of halogenated sugars
US20070264403A1 (en) *	2006-05-11	2007-11-15	Nehmer Warren L	Sparkling agglomerated sweetener, and method of making it
US20080063748A1 (en) *	2006-09-08	2008-03-13	Cadbury Adams Usa Llc.	Center-fill confectionery and chewing gum compositions containing suspended saccharide particles
US20090004360A1 (en) *	2007-05-14	2009-01-01	Cadbury Adams Usa Llc	Taste Potentiator Compositions in Oral Delivery Systems
CA2706368A1 (en) *	2007-11-20	2009-05-28	Cadbury Adams Usa Llc	Dual coated confectionery product
JP5894580B2 (ja) *	2010-05-12	2016-03-30	カーギル・インコーポレイテッド	苦い異味が低減された甘味料組成物および調製方法
CN103635096B (zh)	2011-04-29	2016-08-17	洲际大品牌有限责任公司	被包封的酸、其制备方法及包括所述被包封的酸的咀嚼型胶基糖
CN112806551B (zh) *	2020-12-30	2023-09-15	翁源广业清怡食品科技有限公司	一种提高三氯蔗糖热稳定性的粒化生产方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB2075646A (en)	1980-05-07	1981-11-18	Exxon Research Engineering Co	Process and apparatus for furnace operation with gas seal

Family Cites Families (5)

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GB2065646B (en) *	1979-12-18	1983-10-05	Tate & Lyle Ltd	Crystalline 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose
EP0030804B1 (de) *	1979-12-18	1983-10-19	TATE & LYLE PUBLIC LIMITED COMPANY	Kristallin-4,1',6'-trichlor-4,1',6'-trideoxy-galactosucrose
US4612373A (en) *	1982-09-13	1986-09-16	Tate & Lyle Public Limited Co.	Trichloro, 6-substituted sucrose compounds, compositions and uses therefor
US4538764A (en) *	1983-06-30	1985-09-03	Dunbar Richard M	Method and apparatus for providing finely divided powder
JPS63129955A (ja) *	1986-11-21	1988-06-02	Ajinomoto General Foods Kk	コ−ヒ−抽出液の安定化方法

1986
- 1986-07-15 GB GB868617222A patent/GB8617222D0/en active Pending
1987
- 1987-07-14 AU AU75655/87A patent/AU591998B2/en not_active Expired
- 1987-07-14 UA UA4203155A patent/UA18713A1/uk unknown
- 1987-07-14 IE IE189587A patent/IE60432B1/en not_active IP Right Cessation
- 1987-07-14 FI FI873105A patent/FI85145C/fi not_active IP Right Cessation
- 1987-07-14 DK DK198703669A patent/DK173232B1/da not_active IP Right Cessation
- 1987-07-14 NZ NZ221063A patent/NZ221063A/en unknown
- 1987-07-14 IL IL83188A patent/IL83188A/xx not_active IP Right Cessation
- 1987-07-14 ZA ZA875121A patent/ZA875121B/xx unknown
- 1987-07-14 PH PH35531A patent/PH24116A/en unknown
- 1987-07-14 RU SU4203155A patent/RU1825318C/ru active
- 1987-07-15 KR KR1019870007638A patent/KR950008268B1/ko not_active Expired - Lifetime
- 1987-07-15 JP JP62176931A patent/JP2562147B2/ja not_active Expired - Lifetime
- 1987-07-15 EP EP87306284A patent/EP0255260B1/de not_active Expired - Lifetime
- 1987-07-15 NO NO872942A patent/NO172164C/no unknown
- 1987-07-15 CA CA000542231A patent/CA1290329C/en not_active Expired - Lifetime
- 1987-07-15 AT AT87306284T patent/ATE52005T1/de not_active IP Right Cessation
- 1987-07-15 AR AR87308152A patent/AR241570A1/es active
- 1987-07-15 DE DE8787306284T patent/DE3762303D1/de not_active Expired - Lifetime
- 1987-07-15 GB GB08716628A patent/GB2193496A/en not_active Withdrawn
- 1987-07-15 ES ES87306284T patent/ES2016362B3/es not_active Expired - Lifetime
- 1987-07-15 US US07/073,454 patent/US4918182A/en not_active Expired - Lifetime
- 1987-07-15 MX MX736287A patent/MX7362A/es unknown
1990
- 1990-04-19 GR GR90400200T patent/GR3000441T3/el unknown
1992
- 1992-12-29 LV LV920528A patent/LV5197A3/xx unknown
1993
- 1993-07-30 GE GEAP19931296A patent/GEP19960447B/en unknown
- 1993-10-28 LT LTIP1431A patent/LT3732B/lt not_active IP Right Cessation
1994
- 1994-03-23 MD MD94-0110A patent/MD108C2/ro not_active IP Right Cessation

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB2075646A (en)	1980-05-07	1981-11-18	Exxon Research Engineering Co	Process and apparatus for furnace operation with gas seal

Also Published As

Publication number	Publication date
PH24116A (en)	1990-03-05
ZA875121B (en)	1988-03-30
NO172164B (no)	1993-03-08
IE871895L (en)	1988-01-15
CA1290329C (en)	1991-10-08
AU591998B2 (en)	1989-12-21
LTIP1431A (en)	1995-05-25
KR880001232A (ko)	1988-04-22
ATE52005T1 (de)	1990-05-15
US4918182A (en)	1990-04-17
MD108C2 (ro)	1995-05-31
GEP19960447B (en)	1996-08-29
FI873105L (fi)	1988-01-16
DK173232B1 (da)	2000-04-25
AR241570A1 (es)	1992-09-30
LV5197A3 (lv)	1993-10-10
EP0255260A1 (de)	1988-02-03
FI873105A0 (fi)	1987-07-14
ES2016362B3 (es)	1990-11-01
JP2562147B2 (ja)	1996-12-11
DE3762303D1 (en)	1990-05-23
EP0255260B1 (de)	1990-04-18
MD108B1 (ro)	1994-12-31
IL83188A (en)	1991-08-16
NZ221063A (en)	1990-01-29
DK366987A (da)	1988-01-16
GB2193496A (en)	1988-02-10
IL83188A0 (en)	1987-12-31
FI85145B (fi)	1991-11-29
NO172164C (no)	1993-06-16
AU7565587A (en)	1988-01-21
UA18713A1 (uk)	1997-12-25
FI85145C (fi)	1992-03-10
JPS6374466A (ja)	1988-04-04
GR3000441T3 (en)	1991-06-28
NO872942L (no)	1988-01-18
IE60432B1 (en)	1994-07-13
GB8617222D0 (en)	1986-08-20
KR950008268B1 (ko)	1995-07-27
DK366987D0 (da)	1987-07-14
RU1825318C (ru)	1993-06-30
GB8716628D0 (en)	1987-08-19
MX7362A (es)	1993-12-01
NO872942D0 (no)	1987-07-15

Legal Events

Date	Code	Title	Description
1996-04-25	TK9A	Rectifications: patents	Free format text: TATE & LYLE PUBLIC LIMITED COMPANY, SUGAR QUAY, LOWER THAMES STREET, LONDON EC3R 6DQ, GB, 19960228
2003-06-25	MM9A	Lapsed patents	Effective date: 20021028

Publication	Publication Date	Title
LT3732B (en)	1996-02-26	Process for preparing crystalline sucralose
EP0497439B1 (de)	1995-09-13	Erythritol-Zusammensetzungen
US12227473B2 (en)	2025-02-18	Production of glycolaldehyde by thermolytic fragmentation
US4199373A (en)	1980-04-22	Process for the manufacture of crystalline fructose
KR20090045070A (ko)	2009-05-07	말티톨의 증발결정화 방법
KR20060008941A (ko)	2006-01-27	개선된 결정성 형태의 수크랄로즈, 및 그 제조 방법
EP0973692B1 (de)	2001-11-14	Verfahren zur anreicherung von rohsalz
JPH10310595A (ja)	1998-11-24	１，６−ｇｐｓまたは１，１−ｇｐｍに富む混合物の製造方法
KR20230062627A (ko)	2023-05-09	고형 알룰로오스 조성물의 제조를 위한 압출 공정
AU777732B2 (en)	2004-10-28	Molasses-containing crystal composition and method for producing the same
CN115052488A (zh)	2022-09-13	固体形式的葡萄糖及用于制造固体形式的葡萄糖的方法
PT85894B (pt)	1993-01-29	Processo para a preparacao de um adocante
US6755914B2 (en)	2004-06-29	Crystalline mixture solid composition and preparation thereof
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