NO318176B1 - Faststoff-oksidbrenselcelle - Google Patents

Faststoff-oksidbrenselcelle Download PDF

Info

Publication number: NO318176B1
Authority: NO; Norway
Prior art keywords: ysz; lsm; resistance; electrolyte; cell
Prior art date: 1993-03-01

Application number

NO19953416A

Other languages

English (en)

Norwegian (no)

Other versions

NO953416D0 (no

NO953416L (no

Inventor

Carsten Bagger

Bruno Kindl

Mogens Mogensen

Original Assignee

Forskningsct Riso

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1993-03-01

Filing date

1995-08-31

Publication date

2005-02-14

1995-08-31 Application filed by Forskningsct Riso filed Critical Forskningsct Riso

1995-08-31 Publication of NO953416D0 publication Critical patent/NO953416D0/no

1995-10-31 Publication of NO953416L publication Critical patent/NO953416L/no

2005-02-14 Publication of NO318176B1 publication Critical patent/NO318176B1/no

Links

239000000446 fuel Substances 0.000 title claims abstract description 15
239000007787 solid Substances 0.000 title claims abstract description 15
239000003792 electrolyte Substances 0.000 claims abstract description 34
239000000203 mixture Substances 0.000 claims abstract description 19
239000010406 cathode material Substances 0.000 claims description 5
210000004027 cell Anatomy 0.000 description 45
230000010287 polarization Effects 0.000 description 33
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 20
238000005245 sintering Methods 0.000 description 20
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical group [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 18
238000012360 testing method Methods 0.000 description 18
239000011572 manganese Substances 0.000 description 15
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 12
229910052760 oxygen Inorganic materials 0.000 description 12
239000001301 oxygen Substances 0.000 description 12
239000000843 powder Substances 0.000 description 11
238000006243 chemical reaction Methods 0.000 description 10
239000007789 gas Substances 0.000 description 10
229910052697 platinum Inorganic materials 0.000 description 10
239000011195 cermet Substances 0.000 description 9
230000000694 effects Effects 0.000 description 9
239000002002 slurry Substances 0.000 description 9
NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Inorganic materials O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 8
238000004519 manufacturing process Methods 0.000 description 8
238000005259 measurement Methods 0.000 description 8
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 7
229910052737 gold Inorganic materials 0.000 description 7
239000010931 gold Substances 0.000 description 7
238000000034 method Methods 0.000 description 7
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 7
229910052726 zirconium Inorganic materials 0.000 description 7
238000000498 ball milling Methods 0.000 description 5
230000015572 biosynthetic process Effects 0.000 description 5
230000007423 decrease Effects 0.000 description 5
238000003801 milling Methods 0.000 description 5
238000012856 packing Methods 0.000 description 5
238000011946 reduction process Methods 0.000 description 5
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
239000004698 Polyethylene Substances 0.000 description 4
238000005266 casting Methods 0.000 description 4
238000009826 distribution Methods 0.000 description 4
238000010438 heat treatment Methods 0.000 description 4
229910052748 manganese Inorganic materials 0.000 description 4
210000003739 neck Anatomy 0.000 description 4
-1 polyethylene Polymers 0.000 description 4
229920000573 polyethylene Polymers 0.000 description 4
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 3
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
229910052782 aluminium Inorganic materials 0.000 description 3
239000000919 ceramic Substances 0.000 description 3
238000003487 electrochemical reaction Methods 0.000 description 3
239000007772 electrode material Substances 0.000 description 3
238000002847 impedance measurement Methods 0.000 description 3
239000000463 material Substances 0.000 description 3
230000003647 oxidation Effects 0.000 description 3
238000007254 oxidation reaction Methods 0.000 description 3
239000002245 particle Substances 0.000 description 3
229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 3
229920000036 polyvinylpyrrolidone Polymers 0.000 description 3
235000013855 polyvinylpyrrolidone Nutrition 0.000 description 3
230000009467 reduction Effects 0.000 description 3
239000000243 solution Substances 0.000 description 3
238000003786 synthesis reaction Methods 0.000 description 3
238000009210 therapy by ultrasound Methods 0.000 description 3
238000004458 analytical method Methods 0.000 description 2
238000004364 calculation method Methods 0.000 description 2
230000006835 compression Effects 0.000 description 2
238000007906 compression Methods 0.000 description 2
239000004020 conductor Substances 0.000 description 2
DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
239000002270 dispersing agent Substances 0.000 description 2
238000001035 drying Methods 0.000 description 2
239000002001 electrolyte material Substances 0.000 description 2
239000002737 fuel gas Substances 0.000 description 2
AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
238000002347 injection Methods 0.000 description 2
239000007924 injection Substances 0.000 description 2
238000001746 injection moulding Methods 0.000 description 2
238000002156 mixing Methods 0.000 description 2
239000003960 organic solvent Substances 0.000 description 2
239000004449 solid propellant Substances 0.000 description 2
239000000758 substrate Substances 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
229910002328 LaMnO3 Inorganic materials 0.000 description 1
229920002565 Polyethylene Glycol 400 Polymers 0.000 description 1
238000000627 alternating current impedance spectroscopy Methods 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
YWAAKSBJISUYNU-UHFFFAOYSA-N buta-1,2-dien-1-one Chemical compound CC=C=C=O YWAAKSBJISUYNU-UHFFFAOYSA-N 0.000 description 1
239000003990 capacitor Substances 0.000 description 1
238000005094 computer simulation Methods 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
238000005336 cracking Methods 0.000 description 1
125000004122 cyclic group Chemical group 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000007571 dilatometry Methods 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000005553 drilling Methods 0.000 description 1
238000002593 electrical impedance tomography Methods 0.000 description 1
238000002848 electrochemical method Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
238000011156 evaluation Methods 0.000 description 1
238000004880 explosion Methods 0.000 description 1
239000011440 grout Substances 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
230000004941 influx Effects 0.000 description 1
230000003993 interaction Effects 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
239000008188 pellet Substances 0.000 description 1
238000005325 percolation Methods 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
229940068918 polyethylene glycol 400 Drugs 0.000 description 1
239000001267 polyvinylpyrrolidone Substances 0.000 description 1
230000008092 positive effect Effects 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000007650 screen-printing Methods 0.000 description 1
239000003566 sealing material Substances 0.000 description 1
238000005507 spraying Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
229910001928 zirconium oxide Inorganic materials 0.000 description 1

Classifications

- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
- H01M4/90—Selection of catalytic material
- H01M4/9016—Oxides, hydroxides or oxygenated metallic salts
- H01M4/9025—Oxides specially used in fuel cell operating at high temperature, e.g. SOFC
- H01M4/9033—Complex oxides, optionally doped, of the type M1MeO3, M1 being an alkaline earth metal or a rare earth, Me being a metal, e.g. perovskites
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- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
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- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6565—Cooling rate
- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/95—Products characterised by their size, e.g. microceramics
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9607—Thermal properties, e.g. thermal expansion coefficient
- C04B2235/9615—Linear firing shrinkage
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9607—Thermal properties, e.g. thermal expansion coefficient
- C04B2235/9623—Ceramic setters properties
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells

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Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Ceramic Engineering (AREA)
Manufacturing & Machinery (AREA)
Materials Engineering (AREA)
Structural Engineering (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Composite Materials (AREA)
Chemical Kinetics & Catalysis (AREA)
Electrochemistry (AREA)
General Chemical & Material Sciences (AREA)
Fuel Cell (AREA)
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NO19953416A 1993-03-01 1995-08-31 Faststoff-oksidbrenselcelle NO318176B1 (no)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DK022593A DK171621B1 (da)	1993-03-01	1993-03-01	Fastoxidbrændselscelle med katode af LSM og YSZ
PCT/DK1994/000084 WO1994020998A1 (en)	1993-03-01	1994-03-01	Solid oxide fuel cell

Publications (3)

Publication Number	Publication Date
NO953416D0 NO953416D0 (no)	1995-08-31
NO953416L NO953416L (no)	1995-10-31
NO318176B1 true NO318176B1 (no)	2005-02-14

Family

ID=8091142

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO19953416A NO318176B1 (no)	1993-03-01	1995-08-31	Faststoff-oksidbrenselcelle

Country Status (9)

Country	Link
US (2)	USD360020S (da)
EP (1)	EP0687387B1 (da)
JP (1)	JP3351791B2 (da)
AT (1)	ATE153181T1 (da)
AU (1)	AU6202194A (da)
DE (1)	DE69403198T2 (da)
DK (1)	DK171621B1 (da)
NO (1)	NO318176B1 (da)
WO (1)	WO1994020998A1 (da)

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1993
- 1993-03-01 DK DK022593A patent/DK171621B1/da not_active IP Right Cessation
- 1993-04-09 US US29/006,945 patent/USD360020S/en not_active Expired - Lifetime
1994
- 1994-03-01 AT AT94908982T patent/ATE153181T1/de not_active IP Right Cessation
- 1994-03-01 US US08/513,823 patent/US5591537A/en not_active Expired - Lifetime
- 1994-03-01 AU AU62021/94A patent/AU6202194A/en not_active Abandoned
- 1994-03-01 EP EP94908982A patent/EP0687387B1/en not_active Expired - Lifetime
- 1994-03-01 WO PCT/DK1994/000084 patent/WO1994020998A1/en not_active Ceased
- 1994-03-01 JP JP51947394A patent/JP3351791B2/ja not_active Expired - Lifetime
- 1994-03-01 DE DE69403198T patent/DE69403198T2/de not_active Expired - Lifetime
1995
- 1995-08-31 NO NO19953416A patent/NO318176B1/no not_active IP Right Cessation

Also Published As

Publication number	Publication date
ATE153181T1 (de)	1997-05-15
EP0687387B1 (en)	1997-05-14
NO953416D0 (no)	1995-08-31
WO1994020998A1 (en)	1994-09-15
US5591537A (en)	1997-01-07
JP3351791B2 (ja)	2002-12-03
DE69403198D1 (de)	1997-06-19
DK171621B1 (da)	1997-02-24
DK22593A (da)	1994-09-02
NO953416L (no)	1995-10-31
AU6202194A (en)	1994-09-26
JPH08507639A (ja)	1996-08-13
EP0687387A1 (en)	1995-12-20
USD360020S (en)	1995-07-04
DE69403198T2 (de)	1997-08-21
DK22593D0 (da)	1993-03-01

Legal Events

Date	Code	Title	Description
2014-03-10	MK1K	Patent expired

Publication	Publication Date	Title
NO318176B1 (no)	2005-02-14	Faststoff-oksidbrenselcelle
Holtappels et al.	2002	Fabrication and performance of advanced multi-layer SOFC cathodes
Shimada et al.	2020	Performance comparison of perovskite composite cathodes with BaZr0. 1Ce0. 7Y0. 1Yb0. 1O3–δ in anode-supported protonic ceramic fuel cells
Zhou et al.	2008	SmBaCo2O5+ x double-perovskite structure cathode material for intermediate-temperature solid-oxide fuel cells
Rotureau et al.	2005	Development of a planar SOFC device using screen-printing technology
Taillades et al.	2010	Intermediate temperature anode‐supported fuel cell based on BaCe0. 9Y0. 1O3 electrolyte with novel Pr2NiO4 cathode
Mahmood et al.	2015	High-performance solid oxide electrolysis cell based on ScSZ/GDC (scandia-stabilized zirconia/gadolinium-doped ceria) bi-layered electrolyte and LSCF (lanthanum strontium cobalt ferrite) oxygen electrode
Park et al.	2014	Ex-solution of Ni nanoparticles in a La0. 2Sr0. 8Ti1− xNixO3− δ alternative anode for solid oxide fuel cell
Guo et al.	2008	Electrical and stability performance of anode-supported solid oxide fuel cells with strontium-and magnesium-doped lanthanum gallate thin electrolyte
Yoo et al.	2015	La2NiO4+ δ as oxygen electrode in reversible solid oxide cells
Magrasó et al.	2014	Cathode compatibility, operation, and stability of LaNbO4-based proton conducting fuel cells
Zheng et al.	2023	A double perovskite oxygen electrode in Zr-rich proton conducting ceramic cells for efficient electricity generation and hydrogen production
Lei et al.	2014	Ni-based anode-supported Al2O3-doped-Y2O3-stabilized ZrO2 thin electrolyte solid oxide fuel cells with Y2O3-stabilized ZrO2 buffer layer
Marinha et al.	2012	Electrochemical investigation of oxygen reduction reaction on La0. 6Sr0. 4Co0. 2Fe0. 8O3− δ cathodes deposited by Electrostatic Spray Deposition
Park et al.	2015	Design of a dual-layer ceramic interconnect based on perovskite oxides for segmented-in-series solid oxide fuel cells
Sumi et al.	2015	Prevention of reaction between (Ba, Sr)(Co, Fe) O3 cathodes and yttria-stabilized zirconica electrolytes for intermediate-temperature solid oxide fuel cells
Qian et al.	2015	Chemically stable BaZr0. 7Pr0. 1Y0. 2O3-δ-BaCe0. 8Y0. 2O3-δ bilayer electrolyte for intermediate temperature solid oxide fuel cells
Park et al.	2015	Effect of anode firing on the performance of lanthanum and nickel co-doped SrTiO3 (La0. 2Sr0. 8Ti0. 9Ni0. 1O3− δ) anode of solid oxide fuel cell
Zhao et al.	2021	Stable perovskite-fluorite dual-phase composites synthesized by one-pot solid-state reactive sintering for protonic ceramic fuel cells
Sauvet et al.	2001	Electrochemical properties of a new type of anode material La1− xSrxCr1− yRuyO3− δ for SOFC under hydrogen and methane at intermediate temperatures
Chen et al.	2012	Characterization of La0. 6Sr0. 4Co0. 2Fe0. 8O3–δ+ La2NiO4+ δ composite cathode materials for solid oxide fuel cells
Wang et al.	2014	Electrochemical comparison of cobalt-free La0. 5Sr0. 5Fe0. 9Mo0. 1O3− δ based cathode materials for intermediate-temperature solid oxide fuel cells
CN111048814A (zh)	2020-04-21	一种薄膜氢电极固体氧化物电池及其制备方法
Morales et al.	2015	The effect of anode support on the electrochemical performance of microtubular solid oxide fuel cells fabricated by gel-casting
Park et al.	2015	Electrochemical performance and stability of La0. 2Sr0. 8Ti0. 9Ni0. 1O3-δ and La0. 2Sr0. 8Ti0. 9Ni0. 1O3-δ-Gd0. 2Ce0. 8O2-δ anode with anode interlayer in H2 and CH4