PL417603A1 - Method for producing crystalline form of hydrate thiocyanate [di(2-amino-5-guanidine-pentane)(thiocyanate)copper(II)] complex - Google Patents
Method for producing crystalline form of hydrate thiocyanate [di(2-amino-5-guanidine-pentane)(thiocyanate)copper(II)] complexInfo
- Publication number
- PL417603A1 PL417603A1 PL417603A PL41760316A PL417603A1 PL 417603 A1 PL417603 A1 PL 417603A1 PL 417603 A PL417603 A PL 417603A PL 41760316 A PL41760316 A PL 41760316A PL 417603 A1 PL417603 A1 PL 417603A1
- Authority
- PL
- Poland
- Prior art keywords
- thiocyanate
- copper
- amino
- complex
- crystalline form
- Prior art date
Links
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 title abstract 2
- ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 title abstract 2
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N hydrogen thiocyanate Natural products SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- CIXFHVGWRUTUPZ-UHFFFAOYSA-N thiocyanic acid hydrate Chemical compound O.SC#N CIXFHVGWRUTUPZ-UHFFFAOYSA-N 0.000 title 1
- DYOKHDPMROZFEW-UHFFFAOYSA-N 2-(4-aminopentyl)guanidine Chemical compound CC(N)CCCN=C(N)N DYOKHDPMROZFEW-UHFFFAOYSA-N 0.000 abstract 2
- ODKSFYDXXFIFQN-UHFFFAOYSA-N Arginine Chemical compound OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 abstract 2
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical class Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 abstract 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 abstract 1
- BQVVSSAWECGTRN-UHFFFAOYSA-L copper;dithiocyanate Chemical compound [Cu+2].[S-]C#N.[S-]C#N BQVVSSAWECGTRN-UHFFFAOYSA-L 0.000 abstract 1
- ZNNZYHKDIALBAK-UHFFFAOYSA-M potassium thiocyanate Chemical compound [K+].[S-]C#N ZNNZYHKDIALBAK-UHFFFAOYSA-M 0.000 abstract 1
- 239000012266 salt solution Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 125000000858 thiocyanato group Chemical group *SC#N 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Przedmiotem zgłoszenia jest sposób wytwarzania krystalicznej formy kompleksu [di(2-amino-5-guanidynopentano)(tiocyjaniano)miedzi(II)] charakteryzujący się tym, że jedną część molową uwodnionej soli chlorku miedzi(II) lub soli siarczanu(VI) miedzi(II), rozpuszcza się w wodzie i poddaje się reakcji z dwiema częściami molowymi roztworu kwasu 2-amino-5-guanidynopentanowego oraz dwiema częściami molowymi roztworu soli tiocyjanianu potasu, po czym po minimum 2-18 dniach otrzymuje się jako drugi produkt krystaliczną formę kompleksu hydrat tiocyjanianu [di(2-amino-5-guanidynopentano)(tiocyjaniano)miedzi(II)].The subject of the application is a method for producing the crystalline form of the [di (2-amino-5-guanidinopentane) (thiocyanato) copper (II)] complex characterized in that one molar part of the hydrated copper (II) chloride salt or the copper (II) sulfate salt ( II), it is dissolved in water and reacted with two mole parts of the 2-amino-5-guanidinopentanoic acid solution and two mole parts of the potassium thiocyanate salt solution, after which after a minimum of 2-18 days a crystalline hydrate complex is obtained as a second product thiocyanate [di (2-amino-5-guanidinopentane) (copper (II) thiocyanate]].
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL417603A PL233840B1 (en) | 2016-06-16 | 2016-06-16 | Method for producing crystalline form of hydrate thiocyanate [di(2-amino-5-guanidine-pentane)(thiocyanate)copper(II)] complex |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL417603A PL233840B1 (en) | 2016-06-16 | 2016-06-16 | Method for producing crystalline form of hydrate thiocyanate [di(2-amino-5-guanidine-pentane)(thiocyanate)copper(II)] complex |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL417603A1 true PL417603A1 (en) | 2017-10-23 |
| PL233840B1 PL233840B1 (en) | 2019-11-29 |
Family
ID=60083641
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL417603A PL233840B1 (en) | 2016-06-16 | 2016-06-16 | Method for producing crystalline form of hydrate thiocyanate [di(2-amino-5-guanidine-pentane)(thiocyanate)copper(II)] complex |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL233840B1 (en) |
-
2016
- 2016-06-16 PL PL417603A patent/PL233840B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL233840B1 (en) | 2019-11-29 |
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