PL424690A1 - Method for oxygenation of alpha-pinene - Google Patents

Method for oxygenation of alpha-pinene

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Publication number
PL424690A1
PL424690A1 PL424690A PL42469018A PL424690A1 PL 424690 A1 PL424690 A1 PL 424690A1 PL 424690 A PL424690 A PL 424690A PL 42469018 A PL42469018 A PL 42469018A PL 424690 A1 PL424690 A1 PL 424690A1
Authority
PL
Poland
Prior art keywords
pinene
weight
catalyst
oxygenation
alpha
Prior art date
Application number
PL424690A
Other languages
Polish (pl)
Other versions
PL237108B1 (en
Inventor
Agnieszka Wróblewska
Karol Miądlicki
Dominika Kłosin
Original Assignee
Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zachodniopomorski Uniwersytet Technologiczny W Szczecinie filed Critical Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
Priority to PL424690A priority Critical patent/PL237108B1/en
Publication of PL424690A1 publication Critical patent/PL424690A1/en
Publication of PL237108B1 publication Critical patent/PL237108B1/en

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  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób utleniania α-pinenu, w obecności katalizatora, w atmosferze powietrza, pod ciśnieniem atmosferycznym, z intensywnością mieszania 500 obr/minutę, który charakteryzuje się tym, że stosuje się katalizator TS-1 o zawartości tytanu od 3,08% wag. do 9,92% wagowych, w ilości od 0,25% wag. do 10% wagowych w mieszaninie reakcyjnej, przy czym proces prowadzi się w temperaturze 60 - 140°C, w czasie od 0,25h do 72h godzin. Do reaktora szklanego wprowadza się w pierwszej kolejności α-pinen, a później katalizator.The subject of the application is a method for the oxidation of α-pinene in the presence of a catalyst, in an air atmosphere, at atmospheric pressure, with a mixing intensity of 500 rpm, characterized in that the TS-1 catalyst with a titanium content of 3.08% by weight is used . to 9.92% by weight, in an amount of from 0.25% by weight. up to 10% by weight in the reaction mixture, the process being carried out at a temperature of 60 - 140°C, for 0.25 to 72 hours. The α-pinene is introduced into the glass reactor first, followed by the catalyst.

PL424690A 2018-02-27 2018-02-27 Method for oxygenation of alpha-pinene PL237108B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL424690A PL237108B1 (en) 2018-02-27 2018-02-27 Method for oxygenation of alpha-pinene

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL424690A PL237108B1 (en) 2018-02-27 2018-02-27 Method for oxygenation of alpha-pinene

Publications (2)

Publication Number Publication Date
PL424690A1 true PL424690A1 (en) 2019-09-09
PL237108B1 PL237108B1 (en) 2021-03-22

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Family Applications (1)

Application Number Title Priority Date Filing Date
PL424690A PL237108B1 (en) 2018-02-27 2018-02-27 Method for oxygenation of alpha-pinene

Country Status (1)

Country Link
PL (1) PL237108B1 (en)

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000054880A1 (en) * 1999-03-16 2000-09-21 Consejo Superior De Investigaciones Cientificas MCM-41 TYPE MICROPOROUS MATERIALS CONTAINING TITANIUM AND THEIR UTILIZATION AS CATALYSTS IN α-PINENE OXIDATION

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000054880A1 (en) * 1999-03-16 2000-09-21 Consejo Superior De Investigaciones Cientificas MCM-41 TYPE MICROPOROUS MATERIALS CONTAINING TITANIUM AND THEIR UTILIZATION AS CATALYSTS IN α-PINENE OXIDATION

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
J. MOL. CATAL, A: CHEMICAL, 4 January 2011 (2011-01-04) *

Also Published As

Publication number Publication date
PL237108B1 (en) 2021-03-22

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