FI76643C - Förfarande för att beräkna fodertillsatser - Google Patents
Förfarande för att beräkna fodertillsatser Download PDFInfo
- Publication number
- FI76643C FI76643C FI831773A FI831773A FI76643C FI 76643 C FI76643 C FI 76643C FI 831773 A FI831773 A FI 831773A FI 831773 A FI831773 A FI 831773A FI 76643 C FI76643 C FI 76643C
- Authority
- FI
- Finland
- Prior art keywords
- color
- vanillin
- acid
- feed
- amount
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 16
- 239000003674 animal food additive Substances 0.000 title 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims description 20
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 claims description 20
- 235000012141 vanillin Nutrition 0.000 claims description 20
- 239000002555 ionophore Substances 0.000 claims description 18
- 230000000236 ionophoric effect Effects 0.000 claims description 18
- 239000002253 acid Substances 0.000 claims description 16
- 239000000243 solution Substances 0.000 claims description 15
- 239000002904 solvent Substances 0.000 claims description 15
- 150000001299 aldehydes Chemical class 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 8
- 229930191564 Monensin Natural products 0.000 claims description 7
- GAOZTHIDHYLHMS-UHFFFAOYSA-N Monensin A Natural products O1C(CC)(C2C(CC(O2)C2C(CC(C)C(O)(CO)O2)C)C)CCC1C(O1)(C)CCC21CC(O)C(C)C(C(C)C(OC)C(C)C(O)=O)O2 GAOZTHIDHYLHMS-UHFFFAOYSA-N 0.000 claims description 7
- 230000001476 alcoholic effect Effects 0.000 claims description 7
- 229960005358 monensin Drugs 0.000 claims description 7
- GAOZTHIDHYLHMS-KEOBGNEYSA-N monensin A Chemical compound C([C@@](O1)(C)[C@H]2CC[C@@](O2)(CC)[C@H]2[C@H](C[C@@H](O2)[C@@H]2[C@H](C[C@@H](C)[C@](O)(CO)O2)C)C)C[C@@]21C[C@H](O)[C@@H](C)[C@@H]([C@@H](C)[C@@H](OC)[C@H](C)C(O)=O)O2 GAOZTHIDHYLHMS-KEOBGNEYSA-N 0.000 claims description 7
- 239000011973 solid acid Substances 0.000 claims description 7
- YCPXWRQRBFJBPZ-UHFFFAOYSA-N 5-sulfosalicylic acid Chemical compound OC(=O)C1=CC(S(O)(=O)=O)=CC=C1O YCPXWRQRBFJBPZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000010414 supernatant solution Substances 0.000 claims description 5
- LWRSYTXEQUUTKW-UHFFFAOYSA-N 2,4-dimethoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C(OC)=C1 LWRSYTXEQUUTKW-UHFFFAOYSA-N 0.000 claims description 4
- KQXDHUJYNAXLNZ-XQSDOZFQSA-N Salinomycin Chemical compound O1[C@@H]([C@@H](CC)C(O)=O)CC[C@H](C)[C@@H]1[C@@H](C)[C@H](O)[C@H](C)C(=O)[C@H](CC)[C@@H]1[C@@H](C)C[C@@H](C)[C@@]2(C=C[C@@H](O)[C@@]3(O[C@@](C)(CC3)[C@@H]3O[C@@H](C)[C@@](O)(CC)CC3)O2)O1 KQXDHUJYNAXLNZ-XQSDOZFQSA-N 0.000 claims description 4
- 239000004189 Salinomycin Substances 0.000 claims description 4
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical group CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- 229960001548 salinomycin Drugs 0.000 claims description 4
- 235000019378 salinomycin Nutrition 0.000 claims description 4
- WJUFSDZVCOTFON-UHFFFAOYSA-N veratraldehyde Chemical compound COC1=CC=C(C=O)C=C1OC WJUFSDZVCOTFON-UHFFFAOYSA-N 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 3
- IAJBQAYHSQIQRE-UHFFFAOYSA-N 2,4,5-trimethoxybenzaldehyde Chemical compound COC1=CC(OC)=C(C=O)C=C1OC IAJBQAYHSQIQRE-UHFFFAOYSA-N 0.000 claims description 2
- BGNGWHSBYQYVRX-UHFFFAOYSA-N 4-(dimethylamino)benzaldehyde Chemical compound CN(C)C1=CC=C(C=O)C=C1 BGNGWHSBYQYVRX-UHFFFAOYSA-N 0.000 claims description 2
- 241000723347 Cinnamomum Species 0.000 claims description 2
- DNAVOCNYHNNEQI-UHFFFAOYSA-N asaronaldehyde Natural products COC1=CC(OC)=C(C=CC=O)C=C1OC DNAVOCNYHNNEQI-UHFFFAOYSA-N 0.000 claims description 2
- 235000017803 cinnamon Nutrition 0.000 claims description 2
- 229940073505 ethyl vanillin Drugs 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims 1
- 239000006228 supernatant Substances 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229910002012 Aerosil® Inorganic materials 0.000 description 2
- 241000283690 Bos taurus Species 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- VHKXXVVRRDYCIK-CWCPJSEDSA-N Narasin Chemical compound C[C@H]1C[C@H](C)[C@H]([C@@H](CC)C(O)=O)O[C@H]1[C@@H](C)[C@H](O)[C@H](C)C(=O)[C@H](CC)[C@@H]1[C@@H](C)C[C@@H](C)[C@@]2(C=C[C@@H](O)[C@@]3(O[C@@](C)(CC3)[C@@H]3O[C@@H](C)[C@@](O)(CC)CC3)O2)O1 VHKXXVVRRDYCIK-CWCPJSEDSA-N 0.000 description 2
- VHKXXVVRRDYCIK-UHFFFAOYSA-N Narasin Natural products CC1CC(C)C(C(CC)C(O)=O)OC1C(C)C(O)C(C)C(=O)C(CC)C1C(C)CC(C)C2(C=CC(O)C3(OC(C)(CC3)C3OC(C)C(O)(CC)CC3)O2)O1 VHKXXVVRRDYCIK-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- -1 aryl aldehydes Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000019359 magnesium stearate Nutrition 0.000 description 2
- 229960001851 narasin Drugs 0.000 description 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 2
- 239000003377 acid catalyst Substances 0.000 description 1
- DQPBABKTKYNPMH-UHFFFAOYSA-N amino hydrogen sulfate Chemical compound NOS(O)(=O)=O DQPBABKTKYNPMH-UHFFFAOYSA-N 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- JJVNINGBHGBWJH-UHFFFAOYSA-N ortho-vanillin Chemical compound COC1=CC=CC(C=O)=C1O JJVNINGBHGBWJH-UHFFFAOYSA-N 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000007916 tablet composition Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
Landscapes
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Medicinal Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Fodder In General (AREA)
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Claims (8)
1. Förfarande för beräkning av mängden av en va-nillin-positiv jonofor, sora monensin eller salinomycin, 5. ett foder, varvid man blandar fodret med ett alkoholhal-tigt lösningsmedel, tillsätter en syra med ett pKa-värde mindre än 4 och en färgproducerande arylaldehyd, som vanillin, etylvanillin, 2,4-dimetoxibensaldehyd, 3,4-dimetox.i-bensaldehyd, 2,4,5-trimetoxibensaldehyd, 4-dimetylamino-10 bensaldehyd eller kanelaldehyd, den resulterande lösningen vid en temperatur, vilken är tillräcklig att alstra en färgreaktion, och jämför den sälunda procuderade färgen med en standard, kännetecknat därav, att man använder bäde syran och den färgproducerande arylaldehyden 15 i fast form.
2. Förfarande enligt patentkravet 1, k ä n n e; -t e c k n a t därav, att den färgproducerande arylaldehyden är vanillin.
3. Förfarande enligt patentkravet 1 eller 2, 20 kännetecknat därav, att syran är 5-sulfosali-cylsyra.
4. Förfarande enligt patentkravet 1, kännetecknat därav, att det omfattar steg, vid vilka man 25 a) blandar ett foder som innehäller en vanillin- positiv jonofor med ett alkoholhaltigt lösningsmedel, b) dekanteras en del av den ovanför fällningen liggande vätskan, c) tillsätter en eller flera tabletter, som inne-30 häller en fast syra, vilken har ett pKa-värde under 4, och en eller flera tabletter, som innehäller vanillin, till den nämnda delen av den ovanför fällningen liggande vätska vid en temperatur som är tillräcklig att alstra en färgreaktion, och 35 d) jämför den därvid bildade färgen med en stan dard, vilken hänför sig tili de specifikä mängderna och volymerna av de använda testmaterialen. Il
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB8215419 | 1982-05-26 | ||
| GB8215419 | 1982-05-26 |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| FI831773A0 FI831773A0 (fi) | 1983-05-19 |
| FI831773L FI831773L (fi) | 1983-11-27 |
| FI76643B FI76643B (fi) | 1988-07-29 |
| FI76643C true FI76643C (sv) | 1988-11-10 |
Family
ID=10530654
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI831773A FI76643C (sv) | 1982-05-26 | 1983-05-19 | Förfarande för att beräkna fodertillsatser |
Country Status (22)
| Country | Link |
|---|---|
| JP (1) | JPS58223753A (sv) |
| AT (1) | AT391760B (sv) |
| BE (1) | BE896809A (sv) |
| CH (1) | CH656959A5 (sv) |
| CS (1) | CS258112B2 (sv) |
| DD (1) | DD209914A5 (sv) |
| DE (1) | DE3318597A1 (sv) |
| DK (1) | DK157713C (sv) |
| ES (1) | ES522640A0 (sv) |
| FI (1) | FI76643C (sv) |
| FR (1) | FR2527777B1 (sv) |
| GR (1) | GR79289B (sv) |
| HU (1) | HU185599B (sv) |
| IE (1) | IE54906B1 (sv) |
| IL (1) | IL68741A0 (sv) |
| IT (1) | IT1203653B (sv) |
| LU (1) | LU84814A1 (sv) |
| NL (1) | NL8301798A (sv) |
| NO (1) | NO163507C (sv) |
| PL (1) | PL136878B1 (sv) |
| RO (1) | RO86696B (sv) |
| SE (1) | SE8302832L (sv) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090232949A1 (en) * | 2008-03-12 | 2009-09-17 | Zinpro Corporation | Fluorescent dye tracer method for animal feed supplement products |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA998873A (en) * | 1972-11-17 | 1976-10-26 | Naremco | Prevention of fungi and molds in poultry and animal feedstuffs |
| US3915637A (en) * | 1973-03-16 | 1975-10-28 | A H P Inc | Analysis for water and feed additives |
-
1983
- 1983-03-19 RO RO110998A patent/RO86696B/ro unknown
- 1983-05-19 CH CH2740/83A patent/CH656959A5/fr not_active IP Right Cessation
- 1983-05-19 SE SE8302832A patent/SE8302832L/sv unknown
- 1983-05-19 FI FI831773A patent/FI76643C/sv not_active IP Right Cessation
- 1983-05-20 BE BE6/47829A patent/BE896809A/fr not_active IP Right Cessation
- 1983-05-20 IL IL68741A patent/IL68741A0/xx not_active IP Right Cessation
- 1983-05-20 PL PL1983242095A patent/PL136878B1/pl unknown
- 1983-05-20 LU LU84814A patent/LU84814A1/fr unknown
- 1983-05-20 CS CS833610A patent/CS258112B2/cs unknown
- 1983-05-20 NL NL8301798A patent/NL8301798A/nl not_active Application Discontinuation
- 1983-05-21 DE DE19833318597 patent/DE3318597A1/de not_active Withdrawn
- 1983-05-23 IE IE1212/83A patent/IE54906B1/en not_active IP Right Cessation
- 1983-05-24 IT IT48357/83A patent/IT1203653B/it active
- 1983-05-24 NO NO831836A patent/NO163507C/no unknown
- 1983-05-24 ES ES522640A patent/ES522640A0/es active Granted
- 1983-05-24 DK DK231483A patent/DK157713C/da not_active IP Right Cessation
- 1983-05-24 AT AT0187683A patent/AT391760B/de not_active IP Right Cessation
- 1983-05-24 GR GR71443A patent/GR79289B/el unknown
- 1983-05-25 DD DD83251247A patent/DD209914A5/de not_active IP Right Cessation
- 1983-05-25 JP JP58092209A patent/JPS58223753A/ja active Granted
- 1983-05-25 FR FR8308588A patent/FR2527777B1/fr not_active Expired
- 1983-05-25 HU HU831848A patent/HU185599B/hu not_active IP Right Cessation
Also Published As
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM | Patent lapsed | ||
| MM | Patent lapsed |
Owner name: LILLY INDUSTRIES LIMITED |