JPH0469109B2 - - Google Patents

Info

Publication number: JPH0469109B2
Authority: JP; Japan
Prior art keywords: ceramic powder; pzt; component; particle size; sintering
Prior art date: 1983-12-29
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

JP58245766A

Other languages

English (en)

Japanese (ja)

Other versions

JPS60141674A (ja

Inventor

Tetsuo Yoshimoto

Satoshi Tsukamura

Ishio Kato

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Nippon Soda Co Ltd

Original Assignee

Nippon Soda Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-12-29

Filing date

1983-12-29

Publication date

1992-11-05

1983-12-29 Application filed by Nippon Soda Co Ltd filed Critical Nippon Soda Co Ltd

1983-12-29 Priority to JP58245766A priority Critical patent/JPS60141674A/ja

1985-07-26 Publication of JPS60141674A publication Critical patent/JPS60141674A/ja

1992-11-05 Publication of JPH0469109B2 publication Critical patent/JPH0469109B2/ja

Status Granted legal-status Critical Current

Links

239000000843 powder Substances 0.000 claims description 59
239000000919 ceramic Substances 0.000 claims description 55
239000000203 mixture Substances 0.000 claims description 37
238000005245 sintering Methods 0.000 claims description 22
238000000034 method Methods 0.000 claims description 19
238000004519 manufacturing process Methods 0.000 claims description 18
239000002131 composite material Substances 0.000 claims description 9
239000012702 metal oxide precursor Substances 0.000 claims description 9
229910052573 porcelain Inorganic materials 0.000 claims description 7
230000007062 hydrolysis Effects 0.000 claims description 6
238000006460 hydrolysis reaction Methods 0.000 claims description 6
230000003301 hydrolyzing effect Effects 0.000 claims description 5
229910052758 niobium Inorganic materials 0.000 claims description 5
229910052725 zinc Inorganic materials 0.000 claims description 4
239000011230 binding agent Substances 0.000 claims description 3
229910052749 magnesium Inorganic materials 0.000 claims description 3
239000002243 precursor Substances 0.000 claims description 2
229910052719 titanium Inorganic materials 0.000 claims description 2
229910052726 zirconium Inorganic materials 0.000 claims description 2
125000001183 hydrocarbyl group Chemical group 0.000 claims 1
239000002245 particle Substances 0.000 description 36
238000009826 distribution Methods 0.000 description 19
230000000052 comparative effect Effects 0.000 description 12
238000002834 transmittance Methods 0.000 description 11
238000002441 X-ray diffraction Methods 0.000 description 10
238000010586 diagram Methods 0.000 description 10
239000002904 solvent Substances 0.000 description 10
CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 8
238000007088 Archimedes method Methods 0.000 description 7
239000010955 niobium Substances 0.000 description 6
229910052751 metal Inorganic materials 0.000 description 5
239000002184 metal Substances 0.000 description 5
238000000465 moulding Methods 0.000 description 5
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 5
230000003287 optical effect Effects 0.000 description 5
239000000243 solution Substances 0.000 description 5
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
239000013078 crystal Substances 0.000 description 4
230000001186 cumulative effect Effects 0.000 description 4
230000000694 effects Effects 0.000 description 4
239000000395 magnesium oxide Substances 0.000 description 4
229910052760 oxygen Inorganic materials 0.000 description 4
239000001301 oxygen Substances 0.000 description 4
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
239000000463 material Substances 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
-1 organic acid salt Chemical class 0.000 description 3
239000007858 starting material Substances 0.000 description 3
229910052715 tantalum Inorganic materials 0.000 description 3
239000010936 titanium Substances 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
239000011701 zinc Substances 0.000 description 3
DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
238000004220 aggregation Methods 0.000 description 2
230000002776 aggregation Effects 0.000 description 2
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
239000012298 atmosphere Substances 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
150000002430 hydrocarbons Chemical group 0.000 description 2
239000011777 magnesium Substances 0.000 description 2
238000002156 mixing Methods 0.000 description 2
229910052759 nickel Inorganic materials 0.000 description 2
239000003960 organic solvent Substances 0.000 description 2
239000011164 primary particle Substances 0.000 description 2
239000006104 solid solution Substances 0.000 description 2
238000003756 stirring Methods 0.000 description 2
239000004215 Carbon black (E152) Substances 0.000 description 1
229910019653 Mg1/3Nb2/3 Inorganic materials 0.000 description 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 1
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
229910010413 TiO 2 Inorganic materials 0.000 description 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
230000032683 aging Effects 0.000 description 1
230000001476 alcoholic effect Effects 0.000 description 1
239000004411 aluminium Substances 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910052787 antimony Inorganic materials 0.000 description 1
239000003849 aromatic solvent Substances 0.000 description 1
238000009835 boiling Methods 0.000 description 1
238000001354 calcination Methods 0.000 description 1
230000003750 conditioning effect Effects 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000008878 coupling Effects 0.000 description 1
238000010168 coupling process Methods 0.000 description 1
238000005859 coupling reaction Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000005684 electric field Effects 0.000 description 1
238000000635 electron micrograph Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000011049 filling Methods 0.000 description 1
FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
238000007731 hot pressing Methods 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
229910052746 lanthanum Inorganic materials 0.000 description 1
FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical group [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 description 1
150000002611 lead compounds Chemical class 0.000 description 1
238000005259 measurement Methods 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
230000010287 polarization Effects 0.000 description 1
238000003825 pressing Methods 0.000 description 1
238000001272 pressureless sintering Methods 0.000 description 1
238000012545 processing Methods 0.000 description 1
238000010298 pulverizing process Methods 0.000 description 1
229910052761 rare earth metal Inorganic materials 0.000 description 1
239000002994 raw material Substances 0.000 description 1
238000010992 reflux Methods 0.000 description 1
238000004062 sedimentation Methods 0.000 description 1
229920002545 silicone oil Polymers 0.000 description 1
229910052709 silver Inorganic materials 0.000 description 1
239000004332 silver Substances 0.000 description 1
238000003746 solid phase reaction Methods 0.000 description 1
230000002195 synergetic effect Effects 0.000 description 1
238000012360 testing method Methods 0.000 description 1
238000005979 thermal decomposition reaction Methods 0.000 description 1
150000003609 titanium compounds Chemical class 0.000 description 1
230000005068 transpiration Effects 0.000 description 1
239000008096 xylene Substances 0.000 description 1
150000003755 zirconium compounds Chemical class 0.000 description 1

Landscapes

Compositions Of Oxide Ceramics (AREA)
Inorganic Insulating Materials (AREA)

JP58245766A 1983-12-29 1983-12-29 透光性強誘電体磁器の製造法 Granted JPS60141674A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP58245766A JPS60141674A (ja)	1983-12-29	1983-12-29	透光性強誘電体磁器の製造法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP58245766A JPS60141674A (ja)	1983-12-29	1983-12-29	透光性強誘電体磁器の製造法

Publications (2)

Publication Number	Publication Date
JPS60141674A JPS60141674A (ja)	1985-07-26
JPH0469109B2 true JPH0469109B2 (2)	1992-11-05

Family

ID=17138483

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP58245766A Granted JPS60141674A (ja)	1983-12-29	1983-12-29	透光性強誘電体磁器の製造法

Country Status (1)

Country	Link
JP (1)	JPS60141674A (2)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6311523A (ja) *	1986-07-02	1988-01-19	Natl Inst For Res In Inorg Mater	易焼結性圧電セラミツクス粉末の製造法

1983
- 1983-12-29 JP JP58245766A patent/JPS60141674A/ja active Granted

Also Published As

Publication number	Publication date
JPS60141674A (ja)	1985-07-26

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