JPS60141674A - 透光性強誘電体磁器の製造法 - Google Patents
透光性強誘電体磁器の製造法Info
- Publication number
- JPS60141674A JPS60141674A JP58245766A JP24576683A JPS60141674A JP S60141674 A JPS60141674 A JP S60141674A JP 58245766 A JP58245766 A JP 58245766A JP 24576683 A JP24576683 A JP 24576683A JP S60141674 A JPS60141674 A JP S60141674A
- Authority
- JP
- Japan
- Prior art keywords
- ceramic powder
- pzt
- sintering
- particle size
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000919 ceramic Substances 0.000 title claims description 53
- 238000004519 manufacturing process Methods 0.000 title claims description 20
- 239000000843 powder Substances 0.000 claims description 56
- 239000000203 mixture Substances 0.000 claims description 35
- 238000005245 sintering Methods 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 18
- 239000012702 metal oxide precursor Substances 0.000 claims description 10
- 239000002131 composite material Substances 0.000 claims description 9
- 229910052573 porcelain Inorganic materials 0.000 claims description 7
- 230000007062 hydrolysis Effects 0.000 claims description 6
- 238000006460 hydrolysis reaction Methods 0.000 claims description 6
- 238000000465 moulding Methods 0.000 claims description 6
- 230000003301 hydrolyzing effect Effects 0.000 claims description 4
- 239000011230 binding agent Substances 0.000 claims description 3
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 239000002245 particle Substances 0.000 description 31
- 238000009826 distribution Methods 0.000 description 17
- 230000000052 comparative effect Effects 0.000 description 15
- 238000002441 X-ray diffraction Methods 0.000 description 12
- 239000002904 solvent Substances 0.000 description 11
- 238000002834 transmittance Methods 0.000 description 11
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 8
- 238000007088 Archimedes method Methods 0.000 description 6
- 239000010955 niobium Substances 0.000 description 6
- 230000001186 cumulative effect Effects 0.000 description 5
- 238000010586 diagram Methods 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000395 magnesium oxide Substances 0.000 description 4
- -1 organic acid salt Chemical class 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 3
- 239000012298 atmosphere Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000000635 electron micrograph Methods 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229910052758 niobium Inorganic materials 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 238000005498 polishing Methods 0.000 description 3
- 229910052715 tantalum Inorganic materials 0.000 description 3
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- ZKATWMILCYLAPD-UHFFFAOYSA-N niobium pentoxide Chemical compound O=[Nb](=O)O[Nb](=O)=O ZKATWMILCYLAPD-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000011163 secondary particle Substances 0.000 description 2
- 239000006104 solid solution Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 1
- 229910020684 PbZr Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 150000002611 lead compounds Chemical class 0.000 description 1
- VJPLIHZPOJDHLB-UHFFFAOYSA-N lead titanium Chemical compound [Ti].[Pb] VJPLIHZPOJDHLB-UHFFFAOYSA-N 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 230000015654 memory Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002715 modification method Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000001272 pressureless sintering Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000009774 resonance method Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 150000003609 titanium compounds Chemical class 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 150000003755 zirconium compounds Chemical class 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Insulating Materials (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58245766A JPS60141674A (ja) | 1983-12-29 | 1983-12-29 | 透光性強誘電体磁器の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58245766A JPS60141674A (ja) | 1983-12-29 | 1983-12-29 | 透光性強誘電体磁器の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60141674A true JPS60141674A (ja) | 1985-07-26 |
| JPH0469109B2 JPH0469109B2 (2) | 1992-11-05 |
Family
ID=17138483
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58245766A Granted JPS60141674A (ja) | 1983-12-29 | 1983-12-29 | 透光性強誘電体磁器の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60141674A (2) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6311523A (ja) * | 1986-07-02 | 1988-01-19 | Natl Inst For Res In Inorg Mater | 易焼結性圧電セラミツクス粉末の製造法 |
-
1983
- 1983-12-29 JP JP58245766A patent/JPS60141674A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6311523A (ja) * | 1986-07-02 | 1988-01-19 | Natl Inst For Res In Inorg Mater | 易焼結性圧電セラミツクス粉末の製造法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0469109B2 (2) | 1992-11-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP4234006B2 (ja) | スパッタリングターゲットおよび透明導電膜 | |
| GB2349272A (en) | Piezoelectric paste and piezoelectric film and piezoelectric part using the same | |
| CN101024573A (zh) | 多元铌酸钾钠系无铅压电陶瓷及其制备方法 | |
| US4990324A (en) | Method for producing two-component or three-component lead zirconate-titanate | |
| CN120483716A (zh) | 一种无铅压电钙钛矿陶瓷材料及其制备方法 | |
| JPS60141674A (ja) | 透光性強誘電体磁器の製造法 | |
| US5607632A (en) | Method of fabricating PLZT piezoelectric ceramics | |
| JPS6324950B2 (2) | ||
| JP3236641B2 (ja) | 複合強誘電性セラミックスの製造方法 | |
| WO1999064366A2 (en) | Method for producing sintered electroceramic materials from hydroxide and oxalate precursors | |
| JPS6335449A (ja) | 磁器組成物の製造方法 | |
| JPS62123018A (ja) | 高誘電体粉末の製造方法 | |
| JP3710100B2 (ja) | 酸化物圧電材料の製造方法 | |
| JPS6197159A (ja) | 圧電体薄膜製造用溶液及び圧電体薄膜の製造方法 | |
| JP4720004B2 (ja) | 結晶配向セラミックスの製造方法 | |
| JPS60141675A (ja) | 透光性強誘電体磁器の製造方法 | |
| US3532628A (en) | Piezoelectric ceramic material | |
| JPS5811385B2 (ja) | トウコウセイセラミツクスノ セイゾウホウホウ | |
| JP2607519B2 (ja) | 光学セラミックスの製造方法 | |
| CN1081016A (zh) | 铅系低温烧结弛豫铁电陶瓷瓷料组成及制备工艺 | |
| JPS62162670A (ja) | チタン酸ジルコン酸鉛焼結体の製法 | |
| JP3084401B1 (ja) | 高性能圧電セラミックスとその製造方法 | |
| CN117886601A (zh) | 一种高电致伸缩性能的钛酸钡基陶瓷及其制备方法 | |
| JPS58106703A (ja) | 透光性強誘電体セラミツクスの製造方法 | |
| JP2000203938A (ja) | 高性能圧電セラミックスおよびその製造方法 |