PL417897A1 - New type phases of restricted solid solutions doped with d- and f-electron metal ions and method for producing the type phases of restricted solid solutions doped with d- and f-electron metal ions - Google Patents

New type phases of restricted solid solutions doped with d- and f-electron metal ions and method for producing the type phases of restricted solid solutions doped with d- and f-electron metal ions

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Publication number
PL417897A1
PL417897A1 PL417897A PL41789716A PL417897A1 PL 417897 A1 PL417897 A1 PL 417897A1 PL 417897 A PL417897 A PL 417897A PL 41789716 A PL41789716 A PL 41789716A PL 417897 A1 PL417897 A1 PL 417897A1
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PL
Poland
Prior art keywords
metal ions
solid solutions
electron metal
mol
type phases
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PL417897A
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Polish (pl)
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PL231517B1 (en
Inventor
Marta Pawlikowska
Elżbieta Tomaszewicz
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Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
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Priority to PL417897A priority Critical patent/PL231517B1/en
Publication of PL417897A1 publication Critical patent/PL417897A1/en
Publication of PL231517B1 publication Critical patent/PL231517B1/en

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Abstract

Przedmiotem zgłoszenia są nowe fazy typu ograniczonych roztworów stałych dotowanych jonami d- i f-elektronowego metalu, które charakteryzują się tym, że metal d-elektronowy stanowi mangan lub kobalt, metal f-elektronowy stanowi neodym o ogólnym wzorze Ca0,9934-3xM0,0066 xNd2x(MoO4)1-3x(WO4)3x, gdzie 0 < x ? 0,25, M oznacza Mn lub Co, a oznacza wakancje w sieci krystalicznej. Zgłoszenie zawiera też sposób wytwarzania faz typu ograniczonych roztworów stałych dotowanych jonami d- i f-elektronowego metalu według wynalazku, polegający na mieszaniu, ujednorodnianiu, wygrzewaniu i chłodzeniu, charakteryzuje się tym, że molibdenian(VI) wapnia w ilości większej niż lub równej 49,00% molowego, a mniejszej niż 100,00% molowego miesza się z wolframianem(VI) neodymu(III) w ilości większej niż 0% molowego a mniejszej niż lub równej 50,00% molowego oraz molibdenianem(VI) manganu(II) lub molibdenianem(VI) kobaltu(II) w ilości równej 1,00% molowego, po czym mieszaniny praży się w temperaturze od 900 do 1170°C, następnie chłodzi otrzymując produkt o ogólnym wzorze, Ca0,9934-3xM0,0066 xNd2x(MoO4)1-3x(WO4)3x, gdzie 0 < x ? 0,25, M oznacza Mn lub Co, a oznacza wakancje w sieci krystalicznej.The subject of the application are new phases of the type of limited solid solutions subsidized with d- and f-electron metal ions, which are characterized in that the d-electron metal is manganese or cobalt, the f-electron metal is a neodymium with the general formula Ca0.9934-3xM0.0066 xNd2x (MoO4) 1-3x (WO4) 3x, where 0 <x? 0.25, M is Mn or Co, and means vacancies in the crystal lattice. The application also contains a method for producing phases of the type of limited solid solutions subsidized with d- and f-electron metal ions according to the invention, consisting in mixing, homogenization, heating and cooling, characterized in that calcium molybdate in an amount greater than or equal to 49, 00 mol% and less than 100.00 mol% is mixed with neodymium (III) tungstate in an amount greater than 0 mol% and less than or equal to 50.00 mol% and manganese (II) molybdate or cobalt (II) molybdate in an amount equal to 1.00 mol%, after which the mixtures are calcined at 900 to 1170 ° C, then cooled to give the product of the general formula, Ca0.9934-3xM0.0066 xNd2x (MoO4) 1-3x (WO4) 3x, where 0 <x? 0.25, M is Mn or Co, and means vacancies in the crystal lattice.

PL417897A 2016-07-11 2016-07-11 New type phases of restricted solid solutions doped with d- and f-electron metal ions and method for producing the type phases of restricted solid solutions doped with d- and f-electron metal ions PL231517B1 (en)

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PL417897A PL231517B1 (en) 2016-07-11 2016-07-11 New type phases of restricted solid solutions doped with d- and f-electron metal ions and method for producing the type phases of restricted solid solutions doped with d- and f-electron metal ions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL417897A PL231517B1 (en) 2016-07-11 2016-07-11 New type phases of restricted solid solutions doped with d- and f-electron metal ions and method for producing the type phases of restricted solid solutions doped with d- and f-electron metal ions

Publications (2)

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PL417897A1 true PL417897A1 (en) 2018-01-15
PL231517B1 PL231517B1 (en) 2019-03-29

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PL417897A PL231517B1 (en) 2016-07-11 2016-07-11 New type phases of restricted solid solutions doped with d- and f-electron metal ions and method for producing the type phases of restricted solid solutions doped with d- and f-electron metal ions

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