SU1165230A3 - Способ получени диметил-( @ -цианимидо)-карбоната - Google Patents

Способ получени диметил-( @ -цианимидо)-карбоната Download PDF

Info

Publication number: SU1165230A3
Authority: SU; USSR - Soviet Union
Prior art keywords: carbonate; cyanimido; cyanamide; substituted; alcohol
Prior art date: 1981-07-08

Application number

SU823462947A

Other languages

English (en)

Russian (ru)

Inventor

Йенко Бране

Липовшек Франц

Линдич Зденка

Йерай Франц

Original Assignee

Лек,Товарна Фармацевтских Ин@Кемичних Изделков Н.Сол.,О.,(Фирма)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-07-08

Filing date

1982-07-08

Publication date

1985-06-30

1982-07-08 Application filed by Лек,Товарна Фармацевтских Ин@Кемичних Изделков Н.Сол.,О.,(Фирма) filed Critical Лек,Товарна Фармацевтских Ин@Кемичних Изделков Н.Сол.,О.,(Фирма)

1985-06-30 Application granted granted Critical

1985-06-30 Publication of SU1165230A3 publication Critical patent/SU1165230A3/ru

Links

238000000034 method Methods 0.000 title claims abstract description 10
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 title description 6
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 12
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 8
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 7
XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 claims abstract description 6
238000006243 chemical reaction Methods 0.000 claims abstract description 5
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 4
KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 claims abstract description 4
229910052801 chlorine Inorganic materials 0.000 claims abstract description 4
239000000460 chlorine Substances 0.000 claims abstract description 4
230000003993 interaction Effects 0.000 claims abstract description 4
239000007864 aqueous solution Substances 0.000 claims abstract description 3
150000001298 alcohols Chemical class 0.000 claims abstract 2
238000001816 cooling Methods 0.000 claims abstract 2
150000002825 nitriles Chemical class 0.000 claims 2
238000004519 manufacturing process Methods 0.000 claims 1
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
238000003786 synthesis reaction Methods 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
JMANVNJQNLATNU-UHFFFAOYSA-N oxalonitrile Chemical compound N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 description 2
239000000243 solution Substances 0.000 description 2
-1 4-methyl-5-imidazolyl Chemical group 0.000 description 1
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
241000124033 Salix Species 0.000 description 1
239000000739 antihistaminic agent Substances 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
229910052794 bromium Inorganic materials 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
238000005660 chlorination reaction Methods 0.000 description 1
229960001380 cimetidine Drugs 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000013078 crystal Substances 0.000 description 1
ATDGTVJJHBUTRL-UHFFFAOYSA-N cyanogen bromide Chemical compound BrC#N ATDGTVJJHBUTRL-UHFFFAOYSA-N 0.000 description 1
125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000000284 extract Substances 0.000 description 1
238000011065 in-situ storage Methods 0.000 description 1
RMAHPRNLQIRHIJ-UHFFFAOYSA-N methyl carbamimidate Chemical compound COC(N)=N RMAHPRNLQIRHIJ-UHFFFAOYSA-N 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
239000012071 phase Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
239000011734 sodium Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

SU823462947A 1981-07-08 1982-07-08 Способ получени диметил-( @ -цианимидо)-карбоната SU1165230A3 (ru)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
YU169081A YU42018B (en)	1981-07-08	1981-07-08	Process for preparing dimethyl -(n-cyanimido) carbonate

Publications (1)

Publication Number	Publication Date
SU1165230A3 true SU1165230A3 (ru)	1985-06-30

Family

ID=25555201

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SU823462947A SU1165230A3 (ru)	1981-07-08	1982-07-08	Способ получени диметил-( @ -цианимидо)-карбоната

Country Status (6)

Country	Link
CH (1)	CH653013A5 (de)
DD (1)	DD202534A5 (de)
DE (1)	DE3225249C2 (de)
HU (1)	HU185722B (de)
SU (1)	SU1165230A3 (de)
YU (1)	YU42018B (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4123608C1 (de) *	1991-07-17	1992-07-02	Skw Trostberg Ag, 8223 Trostberg, De
WO2003057680A1 (en) *	2001-12-28	2003-07-17	Nippon Carbide Kogyo Kabushiki Kaisha	Process for producing 2-cyanoimino-1,3-thiazolidine
DE10321269A1 (de) *	2003-05-13	2004-12-02	Bayer Cropscience Ag	Verfahren zur Herstellung von Dimethylcyanimidocarbonat

1981
- 1981-07-08 YU YU169081A patent/YU42018B/xx unknown
1982
- 1982-07-05 CH CH409082A patent/CH653013A5/de not_active IP Right Cessation
- 1982-07-06 DE DE19823225249 patent/DE3225249C2/de not_active Expired
- 1982-07-08 DD DD24151382A patent/DD202534A5/de not_active IP Right Cessation
- 1982-07-08 SU SU823462947A patent/SU1165230A3/ru active
- 1982-07-08 HU HU222982A patent/HU185722B/hu not_active IP Right Cessation

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
1. Европейский Патент А1 0014064, кл. С 07 С 125/08, 1978. *

Also Published As

Publication number	Publication date
DE3225249C2 (de)	1983-12-29
HU185722B (en)	1985-03-28
YU42018B (en)	1988-04-30
DD202534A5 (de)	1983-09-21
YU169081A (en)	1983-04-30
CH653013A5 (de)	1985-12-13
DE3225249A1 (de)	1983-05-26

Similar Documents

Publication	Publication Date	Title
SU628822A3 (ru)	1978-10-15	Способ получени хлоргидрата 4 -эпи-6 оксиадриамицина
GARBRECHT	1959	Synthesis of Amides of Lysergic Acid1
SU1165230A3 (ru)	1985-06-30	Способ получени диметил-( @ -цианимидо)-карбоната
SU973019A3 (ru)	1982-11-07	Способ получени N-галогеналкил-N-нитрозокарбамоилазида
Kato et al.	1967	Studies on ketene and its derivatives—XIII: Synthesis of β-aminocrotonamide and the structure of its pyrolysed product
Wang	1974	Synthesis and properties of N-acetimidoyl derivatives of glycine and sarcosine
SU1556537A3 (ru)	1990-04-07	Способ получени 4-бензилокси-3-пирролин-2-он-1-ил-ацетамида
Elmoghayer et al.	1982	Reactions with heterocyclic β-enaminoesters: A novel synthesis of 2-amino-3-ethoxycarbonyl-(4 H)-pyrans
Shozda et al.	1967	Derivatives of azidosulfonic acid. Halides, amides, and salts
JPS5867676A (ja)	1983-04-22	シメチジンの新しい結晶変異体およびその製造方法
US5395945A (en)	1995-03-07	Synthesis of 3,3-dinitroazetidine
SU1470179A3 (ru)	1989-03-30	Способ получени тетрамовой кислоты
SU914556A1 (ru)	1982-03-23	СПОСОБ ПОЛУЧЕНИЯ 5,6-ДИОКСИМОВ 2-(п-К-ФЕНАЦИЛИДЕН)-З-ОКСОПИПЕРАЗИНА1
US4534895A (en)	1985-08-13	1-Azidomethyl-3,5,7-trinitro-1,3,5,7-tetrazacyclooctane and synthesis thereof via azidation with acetyl azide
US5214222A (en)	1993-05-25	Nitrocubanes
US4579954A (en)	1986-04-01	Cimetidine monohydrate
Hovius et al.	1983	Intramolecular sulfonamide-carboxamide rearrangement
SU1735276A1 (ru)	1992-05-23	Способ получени диалкоксиаминов
Lombardo et al.	1972	Identification of photoaldrin chlorohydrin as a photoalteration product of dieldrin
Procopiou et al.	2003	Synthesis of (R)-α-benzylmethionine: a novel rearrangement during alkylation of the Seebach (R)-methionine oxazolidinone
SU1455610A1 (ru)	1991-08-23	Способ получени 6-арил-5-окси-2,3-дигидропиридазин-3-онов
SU454203A1 (ru)	1974-12-25	Способ получени нитрилов карбоновых кислот
SU1092157A1 (ru)	1984-05-15	Способ получени @ -алкилизофталимидов
SU1007557A3 (ru)	1983-03-23	Способ получени производных 2-метил-2-оксипропилпиперазин-1-карбоксилата
SU1114677A1 (ru)	1984-09-23	Способ получени бензо-2,1,3-тиадиазола