CA1189087A - Method of refining a vegetable oil - Google Patents

Method of refining a vegetable oil

Info

Publication number: CA1189087A
Authority: CA; Canada
Prior art keywords: oil; vegetable oil; gum; membrane; water
Prior art date: 1981-11-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000415848A

Other languages

English (en)

French (fr)

Inventor

Yoshihiko Mutoh

Kazuo Matsuda

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Asahi Kasei Corp

Nisshin Oillio Group Ltd

Original Assignee

Nisshin Oil Mills Ltd

Asahi Kasei Kogyo KK

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-11-30

Filing date

1982-11-18

Publication date

1985-06-18

1982-11-18 Application filed by Nisshin Oil Mills Ltd, Asahi Kasei Kogyo KK filed Critical Nisshin Oil Mills Ltd

1985-06-18 Application granted granted Critical

1985-06-18 Publication of CA1189087A publication Critical patent/CA1189087A/en

Status Expired legal-status Critical Current

Links

235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 90
239000008158 vegetable oil Substances 0.000 title claims abstract description 90
238000000034 method Methods 0.000 title claims abstract description 45
238000007670 refining Methods 0.000 title claims description 8
239000012528 membrane Substances 0.000 claims abstract description 160
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 86
239000011148 porous material Substances 0.000 claims abstract description 42
238000003756 stirring Methods 0.000 claims abstract description 13
239000002253 acid Substances 0.000 claims description 16
239000012466 permeate Substances 0.000 claims description 4
210000004379 membrane Anatomy 0.000 description 135
239000003921 oil Substances 0.000 description 93
235000019198 oils Nutrition 0.000 description 93
238000001914 filtration Methods 0.000 description 55
239000007788 liquid Substances 0.000 description 32
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 24
230000000694 effects Effects 0.000 description 22
239000000203 mixture Substances 0.000 description 22
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 18
239000012510 hollow fiber Substances 0.000 description 17
230000001965 increasing effect Effects 0.000 description 16
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
230000004087 circulation Effects 0.000 description 15
-1 polyethylene Polymers 0.000 description 12
239000000377 silicon dioxide Substances 0.000 description 12
239000007864 aqueous solution Substances 0.000 description 10
239000003960 organic solvent Substances 0.000 description 10
239000010499 rapseed oil Substances 0.000 description 10
MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 description 9
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 9
BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 9
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 8
238000000108 ultra-filtration Methods 0.000 description 8
239000002033 PVDF binder Substances 0.000 description 7
229920002981 polyvinylidene fluoride Polymers 0.000 description 7
208000005156 Dehydration Diseases 0.000 description 6
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
230000000052 comparative effect Effects 0.000 description 6
229920001577 copolymer Polymers 0.000 description 6
230000018044 dehydration Effects 0.000 description 6
238000006297 dehydration reaction Methods 0.000 description 6
239000000463 material Substances 0.000 description 6
238000000605 extraction Methods 0.000 description 5
229920000642 polymer Polymers 0.000 description 5
235000011121 sodium hydroxide Nutrition 0.000 description 5
239000000243 solution Substances 0.000 description 5
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
239000004743 Polypropylene Substances 0.000 description 4
DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 4
238000009826 distribution Methods 0.000 description 4
229920001155 polypropylene Polymers 0.000 description 4
150000003839 salts Chemical class 0.000 description 4
239000007787 solid Substances 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
239000004698 Polyethylene Substances 0.000 description 3
235000019486 Sunflower oil Nutrition 0.000 description 3
239000013626 chemical specie Substances 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
239000010419 fine particle Substances 0.000 description 3
238000005259 measurement Methods 0.000 description 3
235000006408 oxalic acid Nutrition 0.000 description 3
229920000573 polyethylene Polymers 0.000 description 3
239000004810 polytetrafluoroethylene Substances 0.000 description 3
229940058401 polytetrafluoroethylene Drugs 0.000 description 3
235000012424 soybean oil Nutrition 0.000 description 3
239000003549 soybean oil Substances 0.000 description 3
239000000126 substance Substances 0.000 description 3
239000002600 sunflower oil Substances 0.000 description 3
229930195735 unsaturated hydrocarbon Natural products 0.000 description 3
230000000007 visual effect Effects 0.000 description 3
ATHHXGZTWNVVOU-UHFFFAOYSA-N N-methylformamide Chemical compound CNC=O ATHHXGZTWNVVOU-UHFFFAOYSA-N 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
239000002202 Polyethylene glycol Substances 0.000 description 2
235000019485 Safflower oil Nutrition 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
238000009835 boiling Methods 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
238000000576 coating method Methods 0.000 description 2
239000012141 concentrate Substances 0.000 description 2
239000000356 contaminant Substances 0.000 description 2
239000002385 cottonseed oil Substances 0.000 description 2
235000012343 cottonseed oil Nutrition 0.000 description 2
238000009792 diffusion process Methods 0.000 description 2
238000005265 energy consumption Methods 0.000 description 2
229910052731 fluorine Inorganic materials 0.000 description 2
125000001153 fluoro group Chemical group F* 0.000 description 2
235000011187 glycerol Nutrition 0.000 description 2
229920001903 high density polyethylene Polymers 0.000 description 2
239000004700 high-density polyethylene Substances 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
229920001223 polyethylene glycol Polymers 0.000 description 2
229920001343 polytetrafluoroethylene Polymers 0.000 description 2
229920005989 resin Polymers 0.000 description 2
239000011347 resin Substances 0.000 description 2
235000005713 safflower oil Nutrition 0.000 description 2
239000003813 safflower oil Substances 0.000 description 2
239000008159 sesame oil Substances 0.000 description 2
235000011803 sesame oil Nutrition 0.000 description 2
BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 1
235000003301 Ceiba pentandra Nutrition 0.000 description 1
244000146553 Ceiba pentandra Species 0.000 description 1
241000973252 Diagramma Species 0.000 description 1
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
229920000219 Ethylene vinyl alcohol Polymers 0.000 description 1
VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 1
FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
229920000305 Nylon 6,10 Polymers 0.000 description 1
235000019482 Palm oil Nutrition 0.000 description 1
235000004347 Perilla Nutrition 0.000 description 1
244000124853 Perilla frutescens Species 0.000 description 1
229920002367 Polyisobutene Polymers 0.000 description 1
239000004721 Polyphenylene oxide Substances 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
235000019774 Rice Bran oil Nutrition 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
150000001299 aldehydes Chemical class 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
239000004327 boric acid Substances 0.000 description 1
239000010495 camellia oil Substances 0.000 description 1
239000004359 castor oil Substances 0.000 description 1
235000019438 castor oil Nutrition 0.000 description 1
UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 1
239000004927 clay Substances 0.000 description 1
239000003240 coconut oil Substances 0.000 description 1
235000019864 coconut oil Nutrition 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
235000005687 corn oil Nutrition 0.000 description 1
239000002285 corn oil Substances 0.000 description 1
230000007547 defect Effects 0.000 description 1
230000002950 deficient Effects 0.000 description 1
229940113088 dimethylacetamide Drugs 0.000 description 1
FDPIMTJIUBPUKL-UHFFFAOYSA-N dimethylacetone Natural products CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 1
238000005315 distribution function Methods 0.000 description 1
239000000839 emulsion Substances 0.000 description 1
229920000840 ethylene tetrafluoroethylene copolymer Polymers 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000013213 extrapolation Methods 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
235000021588 free fatty acids Nutrition 0.000 description 1
ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
230000005484 gravity Effects 0.000 description 1
239000010460 hemp oil Substances 0.000 description 1
150000004677 hydrates Chemical class 0.000 description 1
230000036571 hydration Effects 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
238000009434 installation Methods 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
229910021645 metal ion Inorganic materials 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
238000000465 moulding Methods 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
239000004006 olive oil Substances 0.000 description 1
235000008390 olive oil Nutrition 0.000 description 1
239000002540 palm oil Substances 0.000 description 1
YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical compound CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 description 1
150000003904 phospholipids Chemical class 0.000 description 1
239000000049 pigment Substances 0.000 description 1
229920002492 poly(sulfone) Polymers 0.000 description 1
229920002239 polyacrylonitrile Polymers 0.000 description 1
229920001083 polybutene Polymers 0.000 description 1
229920000098 polyolefin Polymers 0.000 description 1
229920006380 polyphenylene oxide Polymers 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
229920000915 polyvinyl chloride Polymers 0.000 description 1
239000004800 polyvinyl chloride Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
102000004196 processed proteins & peptides Human genes 0.000 description 1
108090000765 processed proteins & peptides Proteins 0.000 description 1
230000005855 radiation Effects 0.000 description 1
239000008165 rice bran oil Substances 0.000 description 1
238000007127 saponification reaction Methods 0.000 description 1
239000007858 starting material Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1
150000003464 sulfur compounds Chemical class 0.000 description 1
BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
239000002383 tung oil Substances 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1
239000001993 wax Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis

Landscapes

Life Sciences & Earth Sciences (AREA)
Chemical & Material Sciences (AREA)
Microbiology (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Fats And Perfumes (AREA)

CA000415848A 1981-11-30 1982-11-18 Method of refining a vegetable oil Expired CA1189087A (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
JP56-190660		1981-11-30
JP19066081A JPS5950718B2 (ja)	1981-11-30	1981-11-30	植物性油の膜による精製方法

Publications (1)

Publication Number	Publication Date
CA1189087A true CA1189087A (en)	1985-06-18

Family

ID=16261778

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000415848A Expired CA1189087A (en)	1981-11-30	1982-11-18	Method of refining a vegetable oil

Country Status (3)

Country	Link
JP (1)	JPS5950718B2 (ja)
CA (1)	CA1189087A (ja)
DE (1)	DE3244007C2 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5286886A (en) *	1988-06-21	1994-02-15	Van Den Bergh Foods Co., Division Of Conopco, Inc.	Method of refining glyceride oils
US5516924A (en) *	1988-06-21	1996-05-14	Van Den Bergh Foods Co., Division Of Conopco, Inc.	Method of refining glyceride oils
US6797172B2 (en) *	2000-05-24	2004-09-28	The Texas A&M University System	Degumming of edible oils by ultrafiltration

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6022906A (ja) *	1983-07-18	1985-02-05	Asahi Chem Ind Co Ltd	多孔質膜の洗浄方法
GB8423229D0 (en) *	1984-09-14	1984-10-17	Unilever Plc	Treating triglyceride oil
GB8914603D0 (en) *	1989-06-26	1989-08-16	Unilever Plc	Method for refining virgin olive oil
JPH0774353B2 (ja) *	1991-08-26	1995-08-09	日清製油株式会社	食用油の製造法
FR2760756B1 (fr) *	1997-03-17	2003-09-19	Richard De Nyons	Procede de production des huiles vegetales hypoallergeniques
JP2000219886A (ja)	1999-02-01	2000-08-08	Masatoshi Matsumura	植物油（バージン油）又は植物性廃油のディーゼルエンジン用燃料化精製方法及び装置
DE50002182D1 (de) *	2000-07-22	2003-06-18	Hubert Tippkoetter	Verfahren zur Behandlung von gebrauchten Pflanzenölen
ATE354627T1 (de) *	2002-10-31	2007-03-15	Carapelli Firenze S P A	Verfahren zur physikalischen behandlung von olivenöl
DE102006023990B4 (de) *	2006-05-22	2008-07-03	Chmiel, Horst, Prof. Dr.-Ing.	Entfernung von hydrophilen Substanzen aus Ölen mittels Membranen
DE102006060107A1 (de) *	2006-12-08	2008-06-12	Westfalia Separator Ag	Verfahren zur Abscheidung von Feststoffen aus einem fließfähigen Produkt
DE102007016157A1 (de)	2007-04-02	2008-10-09	Bayer Technology Services Gmbh	Verfahren zur Trennung von Produktgemischen aus Umesterungsreaktionen

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB1509543A (en) *	1974-05-16	1978-05-04	Unilever Ltd	Purification process
GB1564402A (en) *	1975-11-13	1980-04-10	Unilever Ltd	Purification process
GB2014184B (en) *	1978-01-10	1982-05-19	Asahi Chemical Ind	Method of separating oil from oil-containing liquid

1981
- 1981-11-30 JP JP19066081A patent/JPS5950718B2/ja not_active Expired
1982
- 1982-11-18 CA CA000415848A patent/CA1189087A/en not_active Expired
- 1982-11-27 DE DE19823244007 patent/DE3244007C2/de not_active Expired

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5286886A (en) *	1988-06-21	1994-02-15	Van Den Bergh Foods Co., Division Of Conopco, Inc.	Method of refining glyceride oils
US5516924A (en) *	1988-06-21	1996-05-14	Van Den Bergh Foods Co., Division Of Conopco, Inc.	Method of refining glyceride oils
US6797172B2 (en) *	2000-05-24	2004-09-28	The Texas A&M University System	Degumming of edible oils by ultrafiltration

Also Published As

Publication number	Publication date
DE3244007C2 (de)	1986-06-12
DE3244007A1 (de)	1983-06-01
JPS5950718B2 (ja)	1984-12-10
JPS5893798A (ja)	1983-06-03

Legal Events

Date	Code	Title	Description
2002-06-19	MKEC	Expiry (correction)
2002-11-18	MKEX	Expiry

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JP2886579B2 (ja)	1999-04-26	酵素の精製方法
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CA1189087A - Method of refining a vegetable oil - Google Patents

Info

Links

Classifications

Landscapes

Applications Claiming Priority (2)

Publications (1)

Family

ID=16261778

Family Applications (1)

Country Status (3)

Cited By (3)

Families Citing this family (11)

Family Cites Families (3)

Cited By (3)

Also Published As

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