PL417293A1 - New oxysalt in the triple system of cobalt, phosphorus and chromium oxides and method for producing new oxysalts in the triple system of cobalt, phosphorus and chromium oxides - Google Patents
New oxysalt in the triple system of cobalt, phosphorus and chromium oxides and method for producing new oxysalts in the triple system of cobalt, phosphorus and chromium oxidesInfo
- Publication number
- PL417293A1 PL417293A1 PL417293A PL41729316A PL417293A1 PL 417293 A1 PL417293 A1 PL 417293A1 PL 417293 A PL417293 A PL 417293A PL 41729316 A PL41729316 A PL 41729316A PL 417293 A1 PL417293 A1 PL 417293A1
- Authority
- PL
- Poland
- Prior art keywords
- cobalt
- phosphorus
- oxide
- chromium
- new
- Prior art date
Links
- UOUJSJZBMCDAEU-UHFFFAOYSA-N chromium(3+);oxygen(2-) Chemical class [O-2].[O-2].[O-2].[Cr+3].[Cr+3] UOUJSJZBMCDAEU-UHFFFAOYSA-N 0.000 title abstract 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title abstract 3
- 229910017052 cobalt Inorganic materials 0.000 title abstract 3
- 239000010941 cobalt Substances 0.000 title abstract 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 title abstract 3
- 229910052698 phosphorus Inorganic materials 0.000 title abstract 3
- 239000011574 phosphorus Substances 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 abstract 6
- QDOXWKRWXJOMAK-UHFFFAOYSA-N dichromium trioxide Chemical compound O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 abstract 4
- 238000002156 mixing Methods 0.000 abstract 4
- 238000000137 annealing Methods 0.000 abstract 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 abstract 2
- 238000001665 trituration Methods 0.000 abstract 2
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 abstract 1
- -1 cobalt (II) oxide-phosphorus (V) -chromium (III) oxide Chemical group 0.000 abstract 1
- XLJKHNWPARRRJB-UHFFFAOYSA-N cobalt(2+) Chemical compound [Co+2] XLJKHNWPARRRJB-UHFFFAOYSA-N 0.000 abstract 1
- ZOTKGJBKKKVBJZ-UHFFFAOYSA-L cobalt(2+);carbonate Chemical compound [Co+2].[O-]C([O-])=O ZOTKGJBKKKVBJZ-UHFFFAOYSA-L 0.000 abstract 1
- IUYLTEAJCNAMJK-UHFFFAOYSA-N cobalt(2+);oxygen(2-) Chemical compound [O-2].[Co+2] IUYLTEAJCNAMJK-UHFFFAOYSA-N 0.000 abstract 1
- 229910000001 cobalt(II) carbonate Inorganic materials 0.000 abstract 1
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(II) oxide Inorganic materials [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 abstract 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 abstract 1
- 239000008188 pellet Substances 0.000 abstract 1
- 235000021317 phosphate Nutrition 0.000 abstract 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 abstract 1
- 239000002243 precursor Substances 0.000 abstract 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
Przedmiotem zgłoszenia jest nowa oksysól w trójskładnikowym układzie tlenków kobaltu, fosforu i chromu, w którym układ trójskładnikowy oznacza tlenek kobaltu(II)-tlenek fosforu(V)-tlenek chromu(III), o wzorze sumarycznym CoCr2P4O14. Zgłoszenie zawiera też sposób wytwarzania nowej oksysoli, polegający na mieszaniu odpowiednich związków, ujednorodnianiu, wygrzewaniu i chłodzeniu otrzymanych mieszanin, który charakteryzuje się tym, że miesza się węglan kobaltu(II), wodoroortofosforan(V) amonu i tlenek chromu(III) lub inne prekursory tlenków kobaltu(II), fosforu(V) i chromu(III) w stosunku molowym takim, że w przeliczeniu na składniki układu trójskładnikowego tlenków zawartość zarówno tlenku kobaltu(II), jak i tlenku chromu(III), wynosi 25,00% molowych, natomiast zawartość tlenku fosforu(V) wynosi 50,00% molowych. Otrzymaną mieszaninę reagentów ujednorodnia się przez ucieranie, a następnie wygrzewa się w temperaturach od 350 do 1100°C, schładza i uciera otrzymując produkt o wzorze sumarycznym CoCr2P4O14. Korzystnie mieszaninę wygrzewa się przez 100 godzin, w pięciu etapach, przy czym po każdym etapie próbkę schładza się wolno do temperatury pokojowej i uciera. Inny sposób wytwarzania oksysoli, polegający na mieszaniu odpowiednich związków, ujednorodnianiu, wygrzewaniu i chłodzeniu otrzymanych mieszanin, charakteryzuje się tym, że miesza się dwa fosforany(V): CrP3O9 i Co3Cr4P6O24 w stosunku molowym 2:1. Otrzymaną mieszaninę reagentów ujednorodnia się przez ucieranie, a następnie wygrzewa się w postaci pastylki w temperaturach od 950 do 1100°C, otrzymując produkt o wzorze sumarycznym CoCr2P4O14. Korzystnie mieszaninę wygrzewa się przez 52 godziny, w trzech etapach, przy czym po każdym etapie wygrzewania próbkę ochładza się wolno do temperatury pokojowej i uciera.The subject of the application is a new oxysol in a ternary cobalt, phosphorus and chromium oxides system, in which the ternary system is cobalt (II) oxide-phosphorus (V) -chromium (III) oxide, with the formula CoCr2P4O14. The application also contains a method of producing new oxysols, consisting of mixing appropriate compounds, homogenizing, annealing and cooling of the obtained mixtures, which is characterized by mixing cobalt (II) carbonate, ammonium hydrogenorthophosphate and chromium (III) oxide or other precursors cobalt (II), phosphorus (V) and chromium (III) oxides in a molar ratio such that, calculated as components of the ternary oxide system, the content of both cobalt (II) oxide and chromium (III) oxide is 25.00 mol% while the phosphorus (V) oxide content is 50.00 mol%. The resulting reagent mixture is homogenised by trituration, and then annealed at 350 to 1100 ° C, cooled and triturated to give the product of the total formula CoCr2P4O14. Preferably, the mixture is heated for 100 hours in five steps, after each step the sample is slowly cooled to room temperature and ground. Another method of producing oxysols, consisting of mixing appropriate compounds, homogenizing, annealing and cooling of the obtained mixtures, is characterized by mixing two phosphates (V): CrP3O9 and Co3Cr4P6O24 in a molar ratio of 2: 1. The resulting reagent mixture is homogenized by trituration, and then annealed in the form of a pellet at temperatures from 950 to 1100 ° C, to obtain the product with the total formula CoCr2P4O14. Preferably, the mixture is soaked for 52 hours in three stages, after which each sample is slowly cooled to room temperature and ground.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL417293A PL233232B1 (en) | 2016-05-24 | 2016-05-24 | New oxysalt in the triple system of cobalt, phosphorus and chromium oxides and method for producing new oxysalts in the triple system of cobalt, phosphorus and chromium oxides |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL417293A PL233232B1 (en) | 2016-05-24 | 2016-05-24 | New oxysalt in the triple system of cobalt, phosphorus and chromium oxides and method for producing new oxysalts in the triple system of cobalt, phosphorus and chromium oxides |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL417293A1 true PL417293A1 (en) | 2017-12-04 |
| PL233232B1 PL233232B1 (en) | 2019-09-30 |
Family
ID=60473105
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL417293A PL233232B1 (en) | 2016-05-24 | 2016-05-24 | New oxysalt in the triple system of cobalt, phosphorus and chromium oxides and method for producing new oxysalts in the triple system of cobalt, phosphorus and chromium oxides |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL233232B1 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL449246A1 (en) * | 2024-07-16 | 2026-01-19 | Zachodniopomorski Uniwersytet Technologiczny W Szczecinie | A new chemical compound in a ternary system of cobalt, phosphorus and chromium oxides and a method for its production |
-
2016
- 2016-05-24 PL PL417293A patent/PL233232B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL233232B1 (en) | 2019-09-30 |
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