JP2648516B2 - 立体異性体の分離法 - Google Patents

立体異性体の分離法

Info

Publication number
JP2648516B2
JP2648516B2 JP1194925A JP19492589A JP2648516B2 JP 2648516 B2 JP2648516 B2 JP 2648516B2 JP 1194925 A JP1194925 A JP 1194925A JP 19492589 A JP19492589 A JP 19492589A JP 2648516 B2 JP2648516 B2 JP 2648516B2
Authority
JP
Japan
Prior art keywords
group
polysaccharide
carrier
separation
separating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP1194925A
Other languages
English (en)
Japanese (ja)
Other versions
JPH0358943A (ja
Inventor
佳男 岡本
耕一 畑田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DAISERU KAGAKU KOGYO KK
Original Assignee
DAISERU KAGAKU KOGYO KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DAISERU KAGAKU KOGYO KK filed Critical DAISERU KAGAKU KOGYO KK
Priority to JP1194925A priority Critical patent/JP2648516B2/ja
Priority to US07/646,726 priority patent/US5202433A/en
Priority to PCT/JP1990/000743 priority patent/WO1991002006A1/fr
Priority to DE69030649T priority patent/DE69030649T2/de
Priority to EP90908633A priority patent/EP0436722B1/fr
Publication of JPH0358943A publication Critical patent/JPH0358943A/ja
Application granted granted Critical
Publication of JP2648516B2 publication Critical patent/JP2648516B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/29—Chiral phases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B57/00—Separation of optically-active compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/786—Separation; Purification; Stabilisation; Use of additives by membrane separation process, e.g. pervaporation, perstraction, reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B15/00—Preparation of other cellulose derivatives or modified cellulose, e.g. complexes
    • C08B15/05—Derivatives containing elements other than carbon, hydrogen, oxygen, halogens or sulfur
    • C08B15/06—Derivatives containing elements other than carbon, hydrogen, oxygen, halogens or sulfur containing nitrogen, e.g. carbamates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B3/00—Preparation of cellulose esters of organic acids
    • C08B3/08—Preparation of cellulose esters of organic acids of monobasic organic acids with three or more carbon atoms, e.g. propionate or butyrate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B31/00—Preparation of derivatives of starch
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/006—Heteroglycans, i.e. polysaccharides having more than one sugar residue in the main chain in either alternating or less regular sequence; Gellans; Succinoglycans; Arabinogalactans; Tragacanth or gum tragacanth or traganth from Astragalus; Gum Karaya from Sterculia urens; Gum Ghatti from Anogeissus latifolia; Derivatives thereof
    • C08B37/0087—Glucomannans or galactomannans; Tara or tara gum, i.e. D-mannose and D-galactose units, e.g. from Cesalpinia spinosa; Tamarind gum, i.e. D-galactose, D-glucose and D-xylose units, e.g. from Tamarindus indica; Gum Arabic, i.e. L-arabinose, L-rhamnose, D-galactose and D-glucuronic acid units, e.g. from Acacia Senegal or Acacia Seyal; Derivatives thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Materials Engineering (AREA)
  • Biochemistry (AREA)
  • Analytical Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Emergency Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP1194925A 1989-07-27 1989-07-27 立体異性体の分離法 Expired - Fee Related JP2648516B2 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP1194925A JP2648516B2 (ja) 1989-07-27 1989-07-27 立体異性体の分離法
US07/646,726 US5202433A (en) 1989-07-27 1990-06-07 Polysaccharide derivatives as separating agents
PCT/JP1990/000743 WO1991002006A1 (fr) 1989-07-27 1990-06-07 Derives de polysaccharides et agent separateur
DE69030649T DE69030649T2 (de) 1989-07-27 1990-06-07 Polysaccharide derivate sowie trennmittel
EP90908633A EP0436722B1 (fr) 1989-07-27 1990-06-07 Derives de polysaccharides et agent separateur

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1194925A JP2648516B2 (ja) 1989-07-27 1989-07-27 立体異性体の分離法

Publications (2)

Publication Number Publication Date
JPH0358943A JPH0358943A (ja) 1991-03-14
JP2648516B2 true JP2648516B2 (ja) 1997-09-03

Family

ID=16332627

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1194925A Expired - Fee Related JP2648516B2 (ja) 1989-07-27 1989-07-27 立体異性体の分離法

Country Status (5)

Country Link
US (1) US5202433A (fr)
EP (1) EP0436722B1 (fr)
JP (1) JP2648516B2 (fr)
DE (1) DE69030649T2 (fr)
WO (1) WO1991002006A1 (fr)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69222904T2 (de) * 1991-02-28 1998-02-26 Daicel Chem Neue polysaccharidverbindung und trennmittel
WO1992015635A1 (fr) * 1991-03-04 1992-09-17 Daicel Chemical Industries, Ltd. Derive de polysaccharide, sa production et agent separateur
US5543506A (en) * 1992-06-25 1996-08-06 Daicel Chemical Industries, Ltd. Polysaccharide derivative and separating agent
US5514818A (en) * 1993-09-17 1996-05-07 Daicel Chemical Industries, Ltd. Resolution of stereoisomers of aliphatic epoxides
JP3426702B2 (ja) * 1993-09-17 2003-07-14 ダイセル化学工業株式会社 脂肪族エポキシド類の立体異性体の分割方法
US5679572A (en) * 1993-09-22 1997-10-21 Daicel Chemical Industries, Ltd. Separation of chiral compounds on polysaccharide supports
JPH07260762A (ja) * 1994-03-17 1995-10-13 Daicel Chem Ind Ltd 高速液体クロマトグラフィー用充填剤及びその製造法
DE19613990A1 (de) * 1996-04-09 1997-10-16 Wolff Walsrode Ag Thermoplastischer Werkstoff bestehend aus aliphatischen Carbamidsäurederivaten von Polysacchariden und niedermolekularen Harnstoffderivaten sowie ein Verfahren zu dessen Herstellung und Verwendung desselben
US6224775B1 (en) * 1997-09-08 2001-05-01 Villanova University Method of separating chemical mixtures
JP4320065B2 (ja) * 1997-10-23 2009-08-26 ダイセル化学工業株式会社 光学異性体分離法
AU6864798A (en) * 1998-03-16 1999-10-11 Chiral Technologies, Inc. Chiral separations of pyrimidines
FR2786774B1 (fr) * 1998-12-03 2003-04-04 Univ Droit D Economie Et Des S Esters chiraux de polysaccharides, l'un de leurs procedes de preparation et leurs applications dans l'obtention d'acides optiquement enrichis ou la chromatographie chirale
JP2000297103A (ja) * 1999-04-16 2000-10-24 Daicel Chem Ind Ltd キチン誘導体の製造方法
CZ304734B6 (cs) 2000-07-21 2014-09-10 Gilead Sciences, Inc. Způsob přípravy 9-[2-(fosfonomethoxy)propyl]adeninu a 9-[2-(fosfonomethoxy)ethyl]adeninu
US6736967B2 (en) * 2001-06-07 2004-05-18 Daicel Chemical Industries, Ltd. Separating agent for enantiomeric isomers
KR100938207B1 (ko) * 2001-07-06 2010-01-22 다이셀 가가꾸 고교 가부시끼가이샤 신규한 광학이성체 분리용 분리제 및 그 제조 방법
US7265106B2 (en) * 2003-05-09 2007-09-04 Vela Aquisition Corporation Method for isolating (R)-tofisopam
US20060128955A1 (en) * 2003-05-09 2006-06-15 Vela Pharmaceuticals, Inc. Method of isolating (R)-tofisopam
EP1749018B1 (fr) 2004-04-23 2014-10-22 Expedeon Limited Procedes et kits pour stabiliser, proteger et solubiliser des proteines
CN101769906B (zh) * 2009-01-07 2012-07-04 北京英力科技发展有限公司 一种用于检测内酰胺基镁盐含量的衍生化方法
GB0912485D0 (en) 2009-07-17 2009-08-26 Polytherics Ltd Improved conjugation method
WO2011158935A1 (fr) * 2010-06-18 2011-12-22 ダイセル化学工業株式会社 Agent séparateur pour isomères optiques
CN118125909B (zh) * 2024-03-18 2024-07-19 宏济堂制药(商河)有限公司 一种连续工业化制备左旋麝香酮的方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1472040A (fr) * 1965-06-16 1967-03-10 Centre Nat Rech Scient Procédé de préparation de polymères à groupements optiquement actifs, polymères obtenus et leurs applications
JPS60142930A (ja) * 1983-12-28 1985-07-29 Daicel Chem Ind Ltd 分離剤
JPS60226832A (ja) * 1984-04-02 1985-11-12 Daicel Chem Ind Ltd 多糖の脂肪族エステルを含む分離剤
JPH0680081B2 (ja) * 1984-04-11 1994-10-12 ダイセル化学工業株式会社 多糖類誘導体
JPH0655765B2 (ja) * 1984-04-20 1994-07-27 ダイセル化学工業株式会社 セルロース誘導体
JPS61233633A (ja) * 1985-04-03 1986-10-17 Univ Osaka 多糖のハロゲン置換芳香族カルバメート誘導体を有効成分とする分離剤
JPH0680082B2 (ja) * 1985-05-07 1994-10-12 ダイセル化学工業株式会社 多糖の芳香族カルバメ−ト誘導体
JPS62135450A (ja) * 1985-07-31 1987-06-18 Teijin Ltd 光学活性なベ−タ遮断薬の製造方法
JPH0653763B2 (ja) * 1985-08-26 1994-07-20 ダイセル化学工業株式会社 セルロ−ス系カルバメ−ト誘導体
JPH0813844B2 (ja) * 1986-03-20 1996-02-14 ダイセル化学工業株式会社 多糖のアルキル置換フエニルカルバメ−ト誘導体
US4861872A (en) * 1986-03-20 1989-08-29 Daicel Chemical Industries, Ltd. Alkyl-phenylcarbamate derivative of polysaccharide
US4912205A (en) * 1986-03-20 1990-03-27 Daicel Chemical Industries, Ltd. Alkyl-substituted phenylcarbamate derivative of polysaccharide
DE3715576A1 (de) * 1987-05-09 1988-11-24 Wella Ag Neue makromolekulare, oberflaechenaktive, quaternaere n-substituierte chitosanderivate sowie kosmetisches mittel auf der basis dieser neuen chitosanderivate
US4912094B1 (en) * 1988-06-29 1994-02-15 Ribi Immunochem Research Inc. Modified lipopolysaccharides and process of preparation

Also Published As

Publication number Publication date
US5202433A (en) 1993-04-13
EP0436722A4 (en) 1993-03-03
DE69030649T2 (de) 1997-08-21
JPH0358943A (ja) 1991-03-14
DE69030649D1 (de) 1997-06-12
EP0436722B1 (fr) 1997-05-07
WO1991002006A1 (fr) 1991-02-21
EP0436722A1 (fr) 1991-07-17

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